CN104849406A - Titanium dioxide slurry transmittance measurement and test method - Google Patents
Titanium dioxide slurry transmittance measurement and test method Download PDFInfo
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- CN104849406A CN104849406A CN201510239866.2A CN201510239866A CN104849406A CN 104849406 A CN104849406 A CN 104849406A CN 201510239866 A CN201510239866 A CN 201510239866A CN 104849406 A CN104849406 A CN 104849406A
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Abstract
The invention relates to a titanium dioxide slurry transmittance measurement and test method, comprising the specific steps of (1), connecting a silicone rubber pipe between a pressure control system and a slurry receiver, opening a compressed air valve, and adjusting a pressure gage to 0.3Mpa; (2) slowly pouring titanium dioxide slurry into a wide-mouth hopper until a filter screen is completely blocked; (3) measuring the volume of the filtered solution of the titanium dioxide slurry by using a measuring cylinder; (4) calculating, wherein 1 micrometer of filtration amount is equal to filtration milliliter quantity when the filter screen is completely blocked. The method has the advantages that a device is low in production cost, about 300 Yuan; the structure is simple, the operation is convenient, and the population is easy; faults cannot be generated in a use process, and maintenance charge is basically not needed by cleaning well.
Description
[technical field]
The present invention relates to production of polyester technical field of measurement and test, specifically, is that a kind of titania slurry transmitance measures method of testing.
[background technology]
In polyester semi-dulling chips production run, need to add in right amount through the titania of grinding, the fiber that aft-loaded airfoil is obtained has good extinction effect.
The quality of titania grinding effect, is directly connected to the quality of polyester semi-dulling chips melt.Each manufacturing enterprise has the titania slurry transmitance of reflection titania grinding effect to measure, but the mensuration of this project there is no unified detection method standard at present, sensing equipment is also mainly with being certainly made as master, the measurement result repeatability obtained is poor, and the measurement result size of each enterprise is at a distance of very large, without comparability, be not easy to exchange of technology and technology raising.
This titania slurry transmission detecting device, the sealing of slurry receiver part is reliable, and control pressurer system is stablized adjustable, and estimating precision is high, and measurement result is reproducible, can control titania grinding effect preferably.
[summary of the invention]
The object of the invention is to overcome the deficiencies in the prior art, provide a kind of titania slurry transmitance to measure method of testing.
The object of the invention is to be achieved through the following technical solutions:
A kind of titania slurry transmission detecting device, it is characterized in that, size X-over is connected on the instrument compressed air of factory, the small end of size X-over is connected with filtering pressure reducing valve group by two threaded connector of banjo connector G1/4, filtering pressure reducing valve group is connected with the ball valve of banjo connector G1/4 by two threaded connector of banjo connector G1/4, plastics tracheae is connected after plug-in type threaded connector is connected with ball valve, the other end inserts plug-in type threaded connector and is connected with stop valve, stop valve is connected plug-in type threaded connector and is connected with L-type plug-in type threaded connector by plastics tracheae, finally L-type plug-in type threaded connector be screwed into air nozzle and be connected with vacuum drawn threeway by 10mm silicone rubber tube.
Wide-mouth hopper, seal assembly, 1um stainless steel filter disc, wide-mouth triangular funnel, sealing-plug, bottle,suction, hopper, funnel clips clamp.Composition Suction filtration device, refers to assembling schematic diagram.
A kind of titania slurry transmitance measures method of testing, and its concrete steps are:
(1) silicone rubber tube between link pressure Force control system and slurry receiver, opens pressurized air valve, regulates tensimeter to 0.3Mpa;
(2) titania slurry is slowly poured in wide-mouth hopper, till filter screen blocks completely;
(3) the filtered solution volume of titania slurry is measured with graduated cylinder;
(4) calculate:
The milliliter number filtered when 1um filtrable volume=filter screen blocks completely.
Compared with prior art, good effect of the present invention is:
Because the sealing of this Suction filtration device receiver part is reliable, and pressure controllable is adjustable, and this device possesses:
The present invention has filled up the blank of this project detection method, and estimating precision is high, and measurement result is reproducible, can control titania grinding effect preferably.
Apparatus of the present invention cost of manufacture is low, at about 300 yuan;
Structure of the present invention is simple, easy to operate, is easy to promote;
Can not fault be produced in use procedure of the present invention, as long as carry out clean, basic Maintenance free expense.
[accompanying drawing explanation]
The schematic diagram of Fig. 1 slurry receiver of the present invention;
The schematic diagram of Fig. 2 control pressurer system of the present invention;
Being labeled as in accompanying drawing: 1 size X-over, 2 filtering pressure reducing valves, 3 ball valves, 4 plug-in type threaded connectors, 5 stop valves, 6 pressure idle joint, 7 plastics tracheaes, 8 pairs of threaded connectors, 9 silicone rubber tubes;
[embodiment]
A kind of titania slurry transmitance of the present invention is below provided to measure the embodiment of method of testing.
Embodiment 1
Refer to accompanying drawing 1, a kind of titania slurry transmission detecting device, it comprises control pressurer system, it is characterized in that, size X-over is connected on the instrument compressed air of factory, the small end of size X-over is connected with filtering pressure reducing valve group by two threaded connector of banjo connector G1/4, filtering pressure reducing valve group is connected with the ball valve of banjo connector G1/4 by two threaded connector of banjo connector G1/4, plastics tracheae is connected after plug-in type threaded connector is connected with ball valve, the other end inserts plug-in type threaded connector and is connected with stop valve, stop valve is connected plug-in type threaded connector and is connected with L-type plug-in type threaded connector by plastics tracheae, finally L-type plug-in type threaded connector be screwed into air nozzle and be connected with vacuum drawn threeway by 10mm silicone rubber tube.
Wide-mouth hopper, seal assembly, 1um stainless steel filter disc, wide-mouth triangular funnel, sealing-plug, bottle,suction, hopper, funnel clips clamp.Composition Suction filtration device, refers to assembling schematic diagram.
A kind of titania slurry transmitance measures method of testing:
(1) silicone rubber tube between link pressure Force control system and slurry receiver, opens pressurized air valve, regulates tensimeter to 0.3Mpa;
(2) titania slurry is slowly poured in wide-mouth hopper, till filter screen blocks completely;
(3) the filtered solution volume of titania slurry is measured with graduated cylinder;
(4) calculate:
The milliliter number filtered when 1um filtrable volume=filter screen blocks completely.
The above is only the preferred embodiment of the present invention; it should be pointed out that for those skilled in the art, without departing from the inventive concept of the premise; can also make some improvements and modifications, these improvements and modifications also should be considered within the scope of protection of the present invention.
Claims (2)
1. titania slurry transmitance measures a method of testing, and it is characterized in that, its concrete steps are:
(1) in titania slurry transmission detecting device, open pressurized air valve, regulate tensimeter to 0.3Mpa;
(2) titania slurry is slowly poured in wide-mouth hopper, till filter screen blocks completely;
(3) the filtered solution volume of titania slurry is measured with graduated cylinder;
(4) calculate:
The milliliter number filtered when 1um filtrable volume=filter screen blocks completely.
2. a kind of titania slurry transmitance as claimed in claim 1 measures method of testing, it is characterized in that, described titania slurry transmission detecting device, size X-over is connected on the instrument compressed air of factory, the small end of size X-over is connected with filtering pressure reducing valve group by two threaded connector of banjo connector G1/4, filtering pressure reducing valve group is connected with the ball valve of banjo connector G1/4 by two threaded connector of banjo connector G1/4, plastics tracheae is connected after plug-in type threaded connector is connected with ball valve, the other end inserts plug-in type threaded connector and is connected with stop valve, stop valve is connected plug-in type threaded connector and is connected with L-type plug-in type threaded connector by plastics tracheae, finally L-type plug-in type threaded connector be screwed into air nozzle and be connected with vacuum drawn threeway by 10mm silicone rubber tube.
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CN103149109A (en) * | 2013-03-10 | 2013-06-12 | 浙江佳宝新纤维集团有限公司 | Method for rapidly and efficiently measuring fiber grease |
CN203132943U (en) * | 2013-03-10 | 2013-08-14 | 浙江佳宝新纤维集团有限公司 | Rapid tester of fiber oil |
US9021865B1 (en) * | 2011-03-02 | 2015-05-05 | The United States Of America As Represented By The Secretary Of The Army | Apparatus and method for measuring permeation of contaminants through protective materials |
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CN1773246A (en) * | 2004-11-10 | 2006-05-17 | 中国石油化工股份有限公司 | Diffusion coefficient analyzer |
CN101504351A (en) * | 2009-03-06 | 2009-08-12 | 中国科学院武汉岩土力学研究所 | Sand bed seepage flow sludge plugging simulation apparatus |
CN201514365U (en) * | 2009-10-29 | 2010-06-23 | 艾丹 | Bubble-free diffusion cell |
US9021865B1 (en) * | 2011-03-02 | 2015-05-05 | The United States Of America As Represented By The Secretary Of The Army | Apparatus and method for measuring permeation of contaminants through protective materials |
CN202886235U (en) * | 2012-09-27 | 2013-04-17 | 苏州出入境检验检疫局检验检疫综合技术中心 | Transdermal absorption simulating device |
CN103149109A (en) * | 2013-03-10 | 2013-06-12 | 浙江佳宝新纤维集团有限公司 | Method for rapidly and efficiently measuring fiber grease |
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Application publication date: 20150819 |