CN104845705B - Accurate knitting machine oil composition and preparation method thereof - Google Patents
Accurate knitting machine oil composition and preparation method thereof Download PDFInfo
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- CN104845705B CN104845705B CN201510281703.0A CN201510281703A CN104845705B CN 104845705 B CN104845705 B CN 104845705B CN 201510281703 A CN201510281703 A CN 201510281703A CN 104845705 B CN104845705 B CN 104845705B
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- parts
- catalyst
- knitting machine
- machine oil
- adhesive
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- 238000009940 knitting Methods 0.000 title claims abstract description 28
- 239000010721 machine oil Substances 0.000 title claims abstract description 28
- 239000000203 mixture Substances 0.000 title claims abstract description 25
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 30
- 239000003054 catalyst Substances 0.000 claims abstract description 24
- 239000000853 adhesive Substances 0.000 claims abstract description 22
- 230000001070 adhesive effect Effects 0.000 claims abstract description 22
- 239000002199 base oil Substances 0.000 claims abstract description 20
- FBPFZTCFMRRESA-KVTDHHQDSA-N D-Mannitol Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-KVTDHHQDSA-N 0.000 claims abstract description 19
- 229930195725 Mannitol Natural products 0.000 claims abstract description 19
- 239000013530 defoamer Substances 0.000 claims abstract description 19
- 235000010355 mannitol Nutrition 0.000 claims abstract description 19
- 239000000594 mannitol Substances 0.000 claims abstract description 19
- 239000003760 tallow Substances 0.000 claims abstract description 18
- -1 alkyl Propanolamine Chemical compound 0.000 claims abstract description 13
- 239000000376 reactant Substances 0.000 claims description 32
- 238000003756 stirring Methods 0.000 claims description 32
- 238000006243 chemical reaction Methods 0.000 claims description 24
- 239000012535 impurity Substances 0.000 claims description 9
- 238000002156 mixing Methods 0.000 claims description 8
- KWSLGOVYXMQPPX-UHFFFAOYSA-N 5-[3-(trifluoromethyl)phenyl]-2h-tetrazole Chemical group FC(F)(F)C1=CC=CC(C2=NNN=N2)=C1 KWSLGOVYXMQPPX-UHFFFAOYSA-N 0.000 claims description 3
- 125000002091 cationic group Chemical group 0.000 claims description 3
- 229910001379 sodium hypophosphite Inorganic materials 0.000 claims description 3
- 239000000839 emulsion Substances 0.000 claims description 2
- 239000002518 antifoaming agent Substances 0.000 claims 1
- 239000003921 oil Substances 0.000 abstract description 5
- 239000004744 fabric Substances 0.000 abstract description 4
- 239000002994 raw material Substances 0.000 abstract description 3
- 230000000694 effects Effects 0.000 abstract description 2
- 125000000217 alkyl group Chemical group 0.000 description 6
- WUGQZFFCHPXWKQ-UHFFFAOYSA-N Propanolamine Chemical compound NCCCO WUGQZFFCHPXWKQ-UHFFFAOYSA-N 0.000 description 5
- 238000006555 catalytic reaction Methods 0.000 description 5
- 229920006243 acrylic copolymer Polymers 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000014121 butter Nutrition 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- ZZVUWRFHKOJYTH-UHFFFAOYSA-N diphenhydramine Chemical compound C=1C=CC=CC=1C(OCCN(C)C)C1=CC=CC=C1 ZZVUWRFHKOJYTH-UHFFFAOYSA-N 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000005461 lubrication Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000010705 motor oil Substances 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
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- Lubricants (AREA)
Abstract
The invention discloses a kind of accurate knitting machine oil composition and preparation method thereof, it is made of following component according to mass fraction：50 70 parts of base oil, 5 10 parts of tallow alkyl Propanolamine, 10 20 parts of mannitol, 5 10 parts of etherifying agent, 20 25 parts of catalyst, 59 parts of adhesive, 69 parts of defoamer.Inventive can more general machine oil stablize, and raw material easily obtain, and cost is low, and effect is good, meets the curing requirements of accurate knitting machine, by test, is compared with general machine oil, cost reduction 30% of the present invention, time cloth rate reduces by 70% caused by oil pollution.
Description
Technical field
The present invention relates to a kind of Industrial Oil, and in particular to a kind of precision knitting machine oil composition and its preparation side
Method.
Background technology
Requirement of the accurate knitting machine to machine oil is higher, and general machine oil, which meets high temperature, low temperature etc., can all draw machine oil characteristic
Some changes are played, for example mobility reduces, and clean-up performance is deteriorated etc., so knitting needle, sinker and cam box are not just had good
Good lubrication and protective effect, increase the consumption of knitting needle, influence the precision of knitting machine, or even can be made because of oil pollution on the contrary
The increase of Cheng Cibu rates, influences product quality；And the highly stable general each component price of knitting machine oil of performance is costly, work is produced
Skill is more complicated, and the production cycle is longer, and raw material is also relatively difficult to collect.
The content of the invention
Goal of the invention：The purpose of the invention is to make up the deficiencies in the prior art, there is provided one kind is used for accurate knitting
Engine oil base oil of machine and preparation method thereof.
Technical solution：A kind of precision knitting machine oil composition, is made of following component according to mass fraction：Base oil 50-
70 parts, 5-10 parts of tallow alkyl Propanolamine, 10-20 parts of mannitol, 5-10 parts of etherifying agent, 20-25 parts of catalyst, adhesive 5-9
Part, 6-9 parts of defoamer.
Preferably, the composition by following component by weight：60 parts of base oil, tallow alkyl third
8 parts of hydramine, 15 parts of mannitol, 6 parts of etherifying agent, 21 parts of catalyst, 7 parts of adhesive, 8 parts of defoamer.
Preferably, etherifying agent is cationic etherifying agent.
Preferably, catalyst is sodium hypophosphite.
Preferably, adhesive is AA emulsion.
A kind of preparation method of precision knitting machine oil composition, includes the following steps：
1）According to parts by weight by base oil, tallow alkyl Propanolamine, mannitol, etherifying agent input reaction kettle, carry out
30min is stirred, reaction kettle temperature control is 200-300 DEG C, mixing speed 1000-2000r/min, and during stirring progressively
Catalyst is added, catalyst is divided into three equal parts according to quality, first part adds when being carried out five minutes for stirring, and second part is to stir
Mix and added when carrying out 15 minutes, the 3rd part adds when being carried out 20 minutes for stirring, obtains reactant A;
2）Adhesive will be added in reactant A, stirred evenly, after temperature is increased to 100-200 DEG C of reaction 20-30min
Room temperature is stood, is eventually adding defoamer, obtains reactant B；
3）Reactant B filters off impurity, you can.
Beneficial effect：Accurate knitting machine oil in the present invention, the more general machine oil of performance is stablized, and raw material easily obtain,
Cost is low, and effect is good, meets the curing requirements of accurate knitting machine, and by test, time cloth rate drops significantly caused by oil pollution
It is low, improve the quality of product.
Embodiment
In the present invention, defoamer is commercially available, and etherifying agent is cationic etherifying agent, and catalyst is sodium hypophosphite, adhesive
For acrylic copolymer.
Embodiment 1
A kind of precision knitting machine oil composition, is made of following component according to mass fraction：50 parts of base oil, tallow alkyl
5 parts of Propanolamine, 10 parts of mannitol, 5 parts of etherifying agent, 20 parts of catalyst, 5 parts of adhesive, 6 parts of defoamer.
The specific preparation method of above-mentioned composition includes the following steps：
1）By in base oil, tallow alkyl Propanolamine, mannitol, etherifying agent input reaction kettle, 30min is stirred, instead
It is 200 DEG C, mixing speed 1000r/min to answer kettle temperature control, catalyst is divided into three equal parts according to quality, stirring carries out five minutes
When add first part, stirring carry out 15 minutes when add second part, stirring carry out 20 minutes when add the 3rd part, 30 points
Reaction terminates after clock, obtains reactant A；
2）Adhesive will be added in reactant A, stirred evenly, temperature is increased to stand after 100 DEG C of reaction 20min and is arrived
Room temperature, is eventually adding defoamer, is sufficiently stirred, and obtains reactant B；
3）Reactant B filters off impurity, you can.Industry sieve can be used by filtering impurity.
Embodiment 2
A kind of precision knitting machine oil composition, is made of following component according to mass fraction：50-70 parts of base oil, butter
10 parts of alkyl propanols amine, 20 parts of mannitol, 10 parts of etherifying agent, 25 parts of catalyst, 9 parts of adhesive, 9 parts of defoamer.
The specific preparation method of above-mentioned composition includes the following steps：
1）According to parts by weight by base oil, tallow alkyl Propanolamine, mannitol, etherifying agent input reaction kettle, carry out
30min is stirred, reaction kettle temperature control is 300 DEG C, mixing speed 2000r/min, and catalysis is gradually added during stirring
Agent, is divided into three equal parts, first part adds when being carried out five minutes for stirring, and second part carries out ten for stirring by catalyst according to quality
Added at five minutes, the 3rd part adds when being carried out 20 minutes for stirring, obtains reactant A；
2）Adhesive will be added in reactant A, stirred evenly, after temperature is increased to 100-200 DEG C of reaction 20-30min
Room temperature is stood, is eventually adding defoamer, obtains reactant B；
3）Reactant B filters off impurity, you can.
Embodiment 3
A kind of precision knitting machine oil composition, by following component by weight：60 parts of base oil, tallow alkyl
8 parts of Propanolamine, 15 parts of mannitol, 6 parts of etherifying agent, 21 parts of catalyst, 7 parts of adhesive, 8 parts of defoamer.
A kind of preparation method of precision knitting machine oil composition, includes the following steps：
1）According to parts by weight by base oil, tallow alkyl Propanolamine, mannitol, etherifying agent input reaction kettle, carry out
30min is stirred, reaction kettle temperature control is 300 DEG C, mixing speed 2000r/min, and catalysis is gradually added during stirring
Agent, is divided into three equal parts, first part adds when being carried out five minutes for stirring, and second part carries out ten for stirring by catalyst according to quality
Added at five minutes, the 3rd part adds when being carried out 20 minutes for stirring, obtains reactant A；
2）Adhesive will be added in reactant A, stirred evenly, temperature is increased to stand after 100 DEG C of reaction 25min and is arrived
Room temperature, is eventually adding defoamer, obtains reactant B；
3）Reactant B filters off impurity, you can.
Embodiment 4
A kind of precision knitting machine oil composition, is made of following component according to mass fraction：65 parts of base oil, tallow alkyl
8 parts of Propanolamine, 18 parts of mannitol, 9 parts of etherifying agent, 23 parts of catalyst, 7 parts of adhesive, 8 parts of defoamer.
A kind of preparation method of precision knitting machine oil composition, includes the following steps：
1）According to parts by weight by base oil, tallow alkyl Propanolamine, mannitol, etherifying agent input reaction kettle, carry out
30min is stirred, reaction kettle temperature control is 220 DEG C, mixing speed 1500r/min, and catalysis is gradually added during stirring
Agent, is divided into three equal parts, first part adds when being carried out five minutes for stirring, and second part carries out ten for stirring by catalyst according to quality
Added at five minutes, the 3rd part adds when being carried out 20 minutes for stirring, obtains reactant A；
2）Adhesive will be added in reactant A, stirred evenly, temperature is increased to stand after 180 DEG C of reaction 21min and is arrived
Room temperature, is eventually adding defoamer, obtains reactant B；
3）Reactant B filters off impurity, you can.
Embodiment 5
A kind of precision knitting machine oil composition, is made of following component according to mass fraction：55 parts of base oil, tallow alkyl
8 parts of Propanolamine, 12 parts of mannitol, 5 parts of etherifying agent, 23 parts of catalyst, 7 parts of adhesive, 8 parts of defoamer.
A kind of preparation method of precision knitting machine oil composition, includes the following steps：
1）According to parts by weight by base oil, tallow alkyl Propanolamine, mannitol, etherifying agent input reaction kettle, carry out
30min is stirred, reaction kettle temperature control is 290 DEG C, mixing speed 1900r/min, and catalysis is gradually added during stirring
Agent, is divided into three equal parts, first part adds when being carried out five minutes for stirring, and second part carries out ten for stirring by catalyst according to quality
Added at five minutes, the 3rd part adds when being carried out 20 minutes for stirring, obtains reactant A；
2）Adhesive will be added in reactant A, stirred evenly, stood after temperature is increased to 190 DEG C of reaction 20-30min
To room temperature, defoamer is eventually adding, obtains reactant B；
3）Reactant B filters off impurity, you can.
Embodiment 6
A kind of precision knitting machine oil composition, is made of following component according to mass fraction：68 parts of base oil, tallow alkyl
7 parts of Propanolamine, 11 parts of mannitol, 6 parts of etherifying agent, 21 parts of catalyst, 6 parts of adhesive, 7 parts of defoamer.
A kind of preparation method of precision knitting machine oil composition, includes the following steps：
1）According to parts by weight by base oil, tallow alkyl Propanolamine, mannitol, etherifying agent input reaction kettle, carry out
30min is stirred, reaction kettle temperature control is 200 DEG C, mixing speed 1000r/min, and catalysis is gradually added during stirring
Agent, is divided into three equal parts, first part adds when being carried out five minutes for stirring, and second part carries out ten for stirring by catalyst according to quality
Added at five minutes, the 3rd part adds when being carried out 20 minutes for stirring, obtains reactant A;
2）Adhesive will be added in reactant A, stirred evenly, temperature is increased to stand after 200 DEG C of reaction 30min and is arrived
Room temperature, is eventually adding defoamer, obtains reactant B；
3）Reactant B filters off impurity, you can.
By fabric test, compared with general machine oil, cost reduction 30% of the present invention, time cloth rate caused by oil pollution
Reduce by 70%.
Claims (3)
- A kind of 1. precision knitting machine oil composition, it is characterised in that：The composition is by following component according to mass parts numeral system Into：50-70 parts of base oil, 5-10 parts of tallow alkyl Propanolamine, 10-20 parts of mannitol, 5-10 parts of etherifying agent, catalyst 20-25 Part, 5-9 parts of adhesive, 6-9 parts of defoamer；The etherifying agent is cationic etherifying agent；The catalyst is sodium hypophosphite, The adhesive is AA emulsion.
- 2. precision knitting machine oil composition as claimed in claim 1, it is characterised in that：The composition is pressed by following component It is made according to parts by weight：60 parts of base oil, 8 parts of tallow alkyl Propanolamine, 15 parts of mannitol, 6 parts of etherifying agent, 21 parts of catalyst, 7 parts of adhesive, 8 parts of defoamer.
- A kind of 3. preparation method of accurate knitting machine oil composition as claimed in claim 1, it is characterised in that：Including following step Suddenly：1）According to parts by weight by base oil, tallow alkyl Propanolamine, mannitol, etherifying agent input reaction kettle, it is stirred 30min, reaction kettle temperature control is 200-300 DEG C, mixing speed 1000-2000r/min, and is gradually added during stirring Catalyst, is divided into three equal parts by catalyst according to quality, and first part adds when being carried out five minutes for stirring, second part for stir into Added during row 15 minutes, the 3rd part adds when being carried out 20 minutes for stirring, obtains reactant A; 2）It will add in reactant A Enter adhesive, stir evenly, temperature is increased to stand after 100-200 DEG C of reaction 20-30min and arrives room temperature, is eventually adding defoaming Agent, obtains reactant B；3）Reactant B filters off impurity, you can.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510281703.0A CN104845705B (en) | 2015-05-28 | 2015-05-28 | Accurate knitting machine oil composition and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510281703.0A CN104845705B (en) | 2015-05-28 | 2015-05-28 | Accurate knitting machine oil composition and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN104845705A CN104845705A (en) | 2015-08-19 |
| CN104845705B true CN104845705B (en) | 2018-04-20 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510281703.0A Active CN104845705B (en) | 2015-05-28 | 2015-05-28 | Accurate knitting machine oil composition and preparation method thereof |
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| Country | Link |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101235336A (en) * | 2008-01-24 | 2008-08-06 | 益田润石（北京）化工有限公司 | High abrasion-resisting easy-cleaning knitting machine oil composition |
| CN104263478A (en) * | 2014-09-24 | 2015-01-07 | 中国石油化工股份有限公司 | Easy-to-clean antirust knitting machine oil composition and use thereof |
-
2015
- 2015-05-28 CN CN201510281703.0A patent/CN104845705B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101235336A (en) * | 2008-01-24 | 2008-08-06 | 益田润石（北京）化工有限公司 | High abrasion-resisting easy-cleaning knitting machine oil composition |
| CN104263478A (en) * | 2014-09-24 | 2015-01-07 | 中国石油化工股份有限公司 | Easy-to-clean antirust knitting machine oil composition and use thereof |
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| Publication number | Publication date |
|---|---|
| CN104845705A (en) | 2015-08-19 |
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| TR01 | Transfer of patent right |
Effective date of registration: 20210128 Address after: 251100 East Expressway, Qihe economic and Technological Development Zone, Dezhou City, Shandong Province Patentee after: Shandong Tenghui lubricating oil Technology Co.,Ltd. Address before: 212403 Zhenjiang Jurong City, Jiangsu Province, Jurong 18 town Jurong rabbit knitting factory Patentee before: JURONG SHENTU CRAFTS KNITTING MILL |
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| TR01 | Transfer of patent right |
Effective date of registration: 20240519 Address after: 253000, South 1, Industrial Road West Section, North Fangsi Industrial Park, Fangsi Town, Yucheng City, Dezhou City, Shandong Province Patentee after: Xuanbang Petrochemical Co.,Ltd. Country or region after: China Address before: 251100 East Expressway, Qihe economic and Technological Development Zone, Dezhou City, Shandong Province Patentee before: Shandong Tenghui lubricating oil Technology Co.,Ltd. Country or region before: China |
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