CN104841162A - Cylindrical constant interface extraction pool - Google Patents
Cylindrical constant interface extraction pool Download PDFInfo
- Publication number
- CN104841162A CN104841162A CN201510202182.5A CN201510202182A CN104841162A CN 104841162 A CN104841162 A CN 104841162A CN 201510202182 A CN201510202182 A CN 201510202182A CN 104841162 A CN104841162 A CN 104841162A
- Authority
- CN
- China
- Prior art keywords
- interface
- liquid pool
- phase
- pool
- baffle plate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Sampling And Sample Adjustment (AREA)
Abstract
The invention belongs to the design of a cylindrical constant interface extraction pool. The cylindrical constant interface extraction pool is wholly made of organic glass and comprises a liquid pool (7), a liquid pool cover (4), interface baffle plates (5) (6), two-phase stirring paddles (9) (10) and a constant temperature water jacket (8). A liquid pool body equipped with the liquid pool cover is cylindrical. The liquid pool cover is provided with a stirring opening (3), a feeding opening (1) and a sampling opening (2). The liquid pool (7) is divided into inner and outer two layers, and the constant temperature water jacket (8) is arranged between the inner layer and the outer layer. The interface baffle plates (5) (6) are arranged at the two-phase interface place in the liquid pool (7). The interface baffle plates (5) (6) are formed by two semicircles, wherein one semicircle is fixed unmoved, and the other semicircle can rotate randomly around a shaft at different angles. Therefore, adjustment of the size of the contact area at the two-phase interface place can be realized favorably.
Description
Technical field
The invention belongs to separation technology field, relate to liquid solution abstraction technique, be specifically related to a kind of small-sized constant-interface abstraction device for extraction kinetics research.
Background technology
To be the two-phase that makes to stir respectively carry out mass transfer to constant-interface abstraction technology on a constant interface, material concentration is extracted by certain time interval sample analysis from two-phase, obtain dynamics data, it is the classical way of research liquid-liquid two-phase mass transfer, device used is constant-interface abstraction pool, also cries Lewis pond.In constant-interface abstraction pool, install one piece of interface baffle plate and two-phase separated, the interface of two-phase is in the fan-shaped space of this interface baffle plate, and each stirs respectively by the paddle rotated alone.The sectorial area changing interface baffle plate just can change the size of two-phase interface area.
Summary of the invention
Goal of the invention
According to the needs of liquid-liquid extraction dynamics research.The present invention aims to provide simple, the practical constant-interface abstraction pool of a kind of structure, and the concrete interface baffle plate solving current constant-interface abstraction pool regulates the problem of two-phase contact area.
Technical scheme
For achieving the above object, the invention provides following scheme.
A kind of cylinder type permanent boundary abstraction pool, comprises liquid pool, liquid pool lid, interface baffle plate, two-phase agitator, thermostatted water chuck.The liquid pool being provided with liquid pool lid is cylindrical shape, and liquid pool has covered stirring port, charge door and sample tap.Liquid pool is divided into inside and outside two-layer, inside and outside two-layer between be thermostatic water-jacket.Key is, in liquid pool, two-phase interface place is designed with interface baffle plate, and interface baffle plate is made up of two semicircles, and a semicircle maintains static, and another semicircle can arbitrarily pivot different angles, thus is conducive to the adjustment realizing two-phase interface place contact area size.
Invention effect
In technical scheme provided by the invention, in liquid pool, two-phase interface place design interface baffle plate is made up of two semicircles, and a semicircle maintains static, and another semicircle can arbitrarily pivot different angles.Thus be conducive to the adjustment realizing two-phase interface place contact area size.
Accompanying drawing explanation
Fig. 1 is the structural representation of cylinder type constant-interface abstraction device.
Fig. 2 is structural representation two-layer inside and outside liquid pool.
Fig. 3 is the structural representation of liquid pool lid.
Fig. 4 is the structural representation of interface baffle plate.
In figure, sequence number and title are respectively: (1) charge door (2) sample tap (3) stirring port (4) liquid pool lid (5) (6) interface baffle plate (7) liquid pool (8) thermostatic water-jacket (9) organic phase paddle (10) aqueous phase paddle
Detailed description of the invention
Below in conjunction with accompanying drawing of the present invention, technical scheme of the present invention is set forth further.
As shown in Figure 1, a kind of cylinder type constant-interface abstraction pool, comprises liquid pool (7), liquid pool lid (4), interface baffle plate (5) (6), two-phase paddle (9) (10), thermostatic water-jacket (8).
As shown in Figure 2, liquid pool (7) is divided into inside and outside two-layer, inside and outside two-layer between be thermostatic water-jacket (8), be used for the temperature of control extraction system.
As shown in Figure 3, liquid pool lid (4) there is stirring port (3), charge door (1) and sample tap (2), add two-phase liquid successively from charge door (1), gets upper phase analysis from sample tap (2).Stirring port (3) can add two-phase paddle (9) (10).
As shown in Figure 4, in liquid pool, two-phase interface place is designed with interface baffle plate (5) (6), and interface baffle plate (5) (6) are made up of two semicircles.This liquid pool inner boundary baffle plate (5) (6) semicircles maintain static, and another semicircle can arbitrarily pivot different angles.Thus be conducive to the adjustment realizing two-phase interface place contact area size.
Claims (3)
1. a cylinder type constant-interface abstraction pool, is characterized in that this cylinder type interface abstraction pool is the liquid-adding cell lid (7) of a cylindrical hollow, has interface baffle plate (5) (6) in liquid pool.
2. cylinder type constant-interface abstraction pool as claimed in claim 1, is characterized in that can adding two-phase liquid successively from charge door (1), gets upper phase analysis from sample tap (2).Can also add two-phase paddle (9) (10) from stirring port (3), organic phase stirs (9) oar and is placed in above the baffle plate of interface, and aqueous phase paddle (10) is placed in below the baffle plate of interface.
3. cylinder type constant-interface abstraction pool as claimed in claim 1, it is characterized in that interface baffle plate (5) (6) are made up of two semicircles, a semicircle maintains static, and another semicircle can arbitrarily pivot different angles.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510202182.5A CN104841162A (en) | 2015-04-24 | 2015-04-24 | Cylindrical constant interface extraction pool |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510202182.5A CN104841162A (en) | 2015-04-24 | 2015-04-24 | Cylindrical constant interface extraction pool |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104841162A true CN104841162A (en) | 2015-08-19 |
Family
ID=53841380
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510202182.5A Pending CN104841162A (en) | 2015-04-24 | 2015-04-24 | Cylindrical constant interface extraction pool |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104841162A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105241999A (en) * | 2015-11-10 | 2016-01-13 | 济南大学 | Novel extraction dynamics research method |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4787979A (en) * | 1985-12-24 | 1988-11-29 | Kernforschungszentrum Karlsruhe Gmbh | Liquid-liquid extraction process |
| CN2060687U (en) * | 1989-10-13 | 1990-08-22 | 钟盛华 | Extractor of multi-defection interface |
| CN2197119Y (en) * | 1994-09-06 | 1995-05-17 | 中国科学院长春应用化学研究所 | Pool with the fixed demarcated section of lawyer flow |
| CN200951328Y (en) * | 2006-06-23 | 2007-09-26 | 北京有色金属研究总院 | Extracting mass-transfer, and reactor for improving mass-transfer process externally |
| CN101402002A (en) * | 2008-11-06 | 2009-04-08 | 中国原子能科学研究院 | Constant interface extraction pool |
-
2015
- 2015-04-24 CN CN201510202182.5A patent/CN104841162A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4787979A (en) * | 1985-12-24 | 1988-11-29 | Kernforschungszentrum Karlsruhe Gmbh | Liquid-liquid extraction process |
| CN2060687U (en) * | 1989-10-13 | 1990-08-22 | 钟盛华 | Extractor of multi-defection interface |
| CN2197119Y (en) * | 1994-09-06 | 1995-05-17 | 中国科学院长春应用化学研究所 | Pool with the fixed demarcated section of lawyer flow |
| CN200951328Y (en) * | 2006-06-23 | 2007-09-26 | 北京有色金属研究总院 | Extracting mass-transfer, and reactor for improving mass-transfer process externally |
| CN101402002A (en) * | 2008-11-06 | 2009-04-08 | 中国原子能科学研究院 | Constant interface extraction pool |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105241999A (en) * | 2015-11-10 | 2016-01-13 | 济南大学 | Novel extraction dynamics research method |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Ouyang et al. | Research on the adsorption behavior of heavy metal ions by porous material prepared with silicate tailings | |
| Mu et al. | Microfluidics for manipulating cells | |
| KR20030035621A (en) | Method of manufacturing kit for isolating nucleic acids or biological materials, kit manufactured by the method, and apparatus using the kit | |
| CN104777011B (en) | A kind of Tidal Flat Sediments collection, ecological simulating apparatus in situ and its method | |
| CN203379905U (en) | Reagent tank and kit thereof | |
| CN104841162A (en) | Cylindrical constant interface extraction pool | |
| CN102703687A (en) | Temperature controllable device for selectively leaching minerals by bacteria | |
| Bendjeffal et al. | Adsorption and removal of hydroxychloroquine from aqueous media using Algerian kaolin: full factorial optimisation, kinetic, thermodynamic, and equilibrium studies | |
| CN104215497B (en) | Experimental device and method for extracting polycyclic aromatic hydrocarbons in enriched seawater | |
| US11173458B2 (en) | Integrated apparatus for mixing and separating fluid phases and method therefor | |
| Shi et al. | Environmental Applications of Electromembrane Extraction: A Review | |
| CN101402002A (en) | Constant interface extraction pool | |
| CN106290735A (en) | A kind of experimental provision for measuring liquid-liquid transfer coefficient | |
| CN208350447U (en) | A kind of multiple groups water sampling storage device | |
| CN202212029U (en) | High-voltage electrostatic continuous emulsion breaking device | |
| CN206038644U (en) | Experimental device for be used for surveing liquid mass transfer coefficient | |
| CN201668975U (en) | Miniature centrifugal extractor | |
| CN1996014B (en) | Array micro-fluidic chip device for use in drug metabolism screening | |
| CN111701277A (en) | Cylindrical constant interface extraction pool | |
| CN108728346A (en) | Intermittent gravity micro-flow chip hybridization device and method | |
| CN203507904U (en) | Fixed shaft stirrer | |
| CN209322535U (en) | Industrial wastewater magnetic-adsorption processing unit | |
| CN102689744B (en) | Reagent container | |
| CN202687114U (en) | Reagent container | |
| Pulito et al. | Antibody Array as a tool for screening of natural agents in Cancer chemoprevention |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| EXSB | Decision made by sipo to initiate substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20150819 |
|
| WD01 | Invention patent application deemed withdrawn after publication |