CN104810545B - Phosphate lithium fast-ionic conductor material and preparation method thereof - Google Patents
Phosphate lithium fast-ionic conductor material and preparation method thereof Download PDFInfo
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- CN104810545B CN104810545B CN201410036348.6A CN201410036348A CN104810545B CN 104810545 B CN104810545 B CN 104810545B CN 201410036348 A CN201410036348 A CN 201410036348A CN 104810545 B CN104810545 B CN 104810545B
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- 239000000463 material Substances 0.000 title claims abstract description 70
- 239000010416 ion conductor Substances 0.000 title claims abstract description 20
- 238000002360 preparation method Methods 0.000 title claims abstract description 20
- TWQULNDIKKJZPH-UHFFFAOYSA-K trilithium;phosphate Chemical compound [Li+].[Li+].[Li+].[O-]P([O-])([O-])=O TWQULNDIKKJZPH-UHFFFAOYSA-K 0.000 title abstract description 7
- 239000000843 powder Substances 0.000 claims abstract description 83
- 239000011521 glass Substances 0.000 claims abstract description 57
- 238000000034 method Methods 0.000 claims abstract description 47
- 239000004020 conductor Substances 0.000 claims abstract description 23
- 229910021131 SiyP3−yO12 Inorganic materials 0.000 claims abstract description 11
- 238000010438 heat treatment Methods 0.000 claims description 36
- 238000001816 cooling Methods 0.000 claims description 32
- 238000000465 moulding Methods 0.000 claims description 21
- 238000010791 quenching Methods 0.000 claims description 18
- 238000000137 annealing Methods 0.000 claims description 16
- 230000008569 process Effects 0.000 claims description 15
- 230000000171 quenching effect Effects 0.000 claims description 13
- 238000000748 compression moulding Methods 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 4
- 239000006112 glass ceramic composition Substances 0.000 claims description 3
- 238000007569 slipcasting Methods 0.000 claims description 3
- 238000009987 spinning Methods 0.000 claims description 3
- 238000010345 tape casting Methods 0.000 claims description 3
- 238000005096 rolling process Methods 0.000 claims 1
- 150000002500 ions Chemical class 0.000 abstract description 22
- 238000007493 shaping process Methods 0.000 abstract 1
- 239000002241 glass-ceramic Substances 0.000 description 38
- 229910052744 lithium Inorganic materials 0.000 description 35
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 34
- 238000001035 drying Methods 0.000 description 33
- YBMRDBCBODYGJE-UHFFFAOYSA-N germanium oxide Inorganic materials O=[Ge]=O YBMRDBCBODYGJE-UHFFFAOYSA-N 0.000 description 27
- 238000002156 mixing Methods 0.000 description 27
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 26
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 24
- 238000001238 wet grinding Methods 0.000 description 24
- 229910019142 PO4 Inorganic materials 0.000 description 22
- 238000012360 testing method Methods 0.000 description 22
- 229910001416 lithium ion Inorganic materials 0.000 description 20
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 description 18
- 238000000498 ball milling Methods 0.000 description 18
- 239000007784 solid electrolyte Substances 0.000 description 18
- 239000002228 NASICON Substances 0.000 description 14
- 238000004321 preservation Methods 0.000 description 14
- 229910017677 NH4H2 Inorganic materials 0.000 description 13
- 229910021502 aluminium hydroxide Inorganic materials 0.000 description 13
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 description 13
- 229910001679 gibbsite Inorganic materials 0.000 description 13
- 238000000227 grinding Methods 0.000 description 13
- 239000007788 liquid Substances 0.000 description 13
- XGZVUEUWXADBQD-UHFFFAOYSA-L lithium carbonate Chemical compound [Li+].[Li+].[O-]C([O-])=O XGZVUEUWXADBQD-UHFFFAOYSA-L 0.000 description 13
- 229910052808 lithium carbonate Inorganic materials 0.000 description 13
- 229910052757 nitrogen Inorganic materials 0.000 description 12
- 230000000903 blocking effect Effects 0.000 description 11
- 229910052681 coesite Inorganic materials 0.000 description 11
- 229910052906 cristobalite Inorganic materials 0.000 description 11
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 11
- 239000010931 gold Substances 0.000 description 11
- 229910052737 gold Inorganic materials 0.000 description 11
- 239000000377 silicon dioxide Substances 0.000 description 11
- 229910052682 stishovite Inorganic materials 0.000 description 11
- 239000000126 substance Substances 0.000 description 11
- 229910052905 tridymite Inorganic materials 0.000 description 11
- 238000004364 calculation method Methods 0.000 description 10
- 238000004146 energy storage Methods 0.000 description 10
- 230000000052 comparative effect Effects 0.000 description 9
- 239000013078 crystal Substances 0.000 description 9
- 238000003754 machining Methods 0.000 description 9
- 238000003825 pressing Methods 0.000 description 9
- 239000012535 impurity Substances 0.000 description 8
- 238000001144 powder X-ray diffraction data Methods 0.000 description 8
- 239000000919 ceramic Substances 0.000 description 7
- 238000000354 decomposition reaction Methods 0.000 description 6
- 239000003792 electrolyte Substances 0.000 description 6
- 239000000156 glass melt Substances 0.000 description 6
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 4
- 239000013590 bulk material Substances 0.000 description 4
- 238000002425 crystallisation Methods 0.000 description 4
- 230000008025 crystallization Effects 0.000 description 4
- 239000007787 solid Substances 0.000 description 4
- 239000010935 stainless steel Substances 0.000 description 4
- 229910001220 stainless steel Inorganic materials 0.000 description 4
- 229910009496 Li1.5Al0.5Ge1.5 Inorganic materials 0.000 description 3
- 229910010293 ceramic material Inorganic materials 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 238000009792 diffusion process Methods 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 238000009776 industrial production Methods 0.000 description 3
- 229910001386 lithium phosphate Inorganic materials 0.000 description 3
- 238000005245 sintering Methods 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- JLDSOYXADOWAKB-UHFFFAOYSA-N aluminium nitrate Chemical compound [Al+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O JLDSOYXADOWAKB-UHFFFAOYSA-N 0.000 description 2
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 2
- 238000009694 cold isostatic pressing Methods 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 238000001125 extrusion Methods 0.000 description 2
- 238000007731 hot pressing Methods 0.000 description 2
- 239000011244 liquid electrolyte Substances 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 239000013500 performance material Substances 0.000 description 2
- -1 polytetrafluoroethylene Polymers 0.000 description 2
- 229920001343 polytetrafluoroethylene Polymers 0.000 description 2
- 239000004810 polytetrafluoroethylene Substances 0.000 description 2
- 238000012876 topography Methods 0.000 description 2
- 238000007514 turning Methods 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 229910000733 Li alloy Inorganic materials 0.000 description 1
- 229910010084 LiAlH4 Inorganic materials 0.000 description 1
- 229910010954 LiGe2(PO4)3 Inorganic materials 0.000 description 1
- 229910010951 LiH2 Inorganic materials 0.000 description 1
- 229910011122 LiM2(PO4)3 Inorganic materials 0.000 description 1
- 229910000857 LiTi2(PO4)3 Inorganic materials 0.000 description 1
- 229910003249 Na3Zr2Si2PO12 Inorganic materials 0.000 description 1
- 239000004677 Nylon Substances 0.000 description 1
- 238000002441 X-ray diffraction Methods 0.000 description 1
- JDZCKJOXGCMJGS-UHFFFAOYSA-N [Li].[S] Chemical compound [Li].[S] JDZCKJOXGCMJGS-UHFFFAOYSA-N 0.000 description 1
- 230000004913 activation Effects 0.000 description 1
- 150000004703 alkoxides Chemical class 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 229910052849 andalusite Inorganic materials 0.000 description 1
- 238000010923 batch production Methods 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 229910001598 chiastolite Inorganic materials 0.000 description 1
- 230000002860 competitive effect Effects 0.000 description 1
- 229910052593 corundum Inorganic materials 0.000 description 1
- 239000002178 crystalline material Substances 0.000 description 1
- 238000002484 cyclic voltammetry Methods 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- MNNHAPBLZZVQHP-UHFFFAOYSA-N diammonium hydrogen phosphate Chemical compound [NH4+].[NH4+].OP([O-])([O-])=O MNNHAPBLZZVQHP-UHFFFAOYSA-N 0.000 description 1
- 229910000388 diammonium phosphate Inorganic materials 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000012983 electrochemical energy storage Methods 0.000 description 1
- 238000003487 electrochemical reaction Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000007429 general method Methods 0.000 description 1
- 238000001453 impedance spectrum Methods 0.000 description 1
- 229910052850 kyanite Inorganic materials 0.000 description 1
- XIXADJRWDQXREU-UHFFFAOYSA-M lithium acetate Chemical compound [Li+].CC([O-])=O XIXADJRWDQXREU-UHFFFAOYSA-M 0.000 description 1
- 239000012280 lithium aluminium hydride Substances 0.000 description 1
- 229910000032 lithium hydrogen carbonate Inorganic materials 0.000 description 1
- WMFOQBRAJBCJND-UHFFFAOYSA-M lithium hydroxide Inorganic materials [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 description 1
- IIPYXGDZVMZOAP-UHFFFAOYSA-N lithium nitrate Inorganic materials [Li+].[O-][N+]([O-])=O IIPYXGDZVMZOAP-UHFFFAOYSA-N 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000007773 negative electrode material Substances 0.000 description 1
- 238000010899 nucleation Methods 0.000 description 1
- 230000006911 nucleation Effects 0.000 description 1
- 229920001778 nylon Polymers 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- 239000005486 organic electrolyte Substances 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- 239000004814 polyurethane Substances 0.000 description 1
- 229920002635 polyurethane Polymers 0.000 description 1
- 239000007774 positive electrode material Substances 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000007086 side reaction Methods 0.000 description 1
- 229910052851 sillimanite Inorganic materials 0.000 description 1
- 239000002203 sulfidic glass Substances 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 230000007704 transition Effects 0.000 description 1
- 229910001845 yogo sapphire Inorganic materials 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
- H01M10/056—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes
- H01M10/0561—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes the electrolyte being constituted of inorganic materials only
- H01M10/0562—Solid materials
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M2300/00—Electrolytes
- H01M2300/0017—Non-aqueous electrolytes
- H01M2300/0065—Solid electrolytes
- H01M2300/0068—Solid electrolytes inorganic
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
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- Chemical & Material Sciences (AREA)
- Physics & Mathematics (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- General Physics & Mathematics (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Secondary Cells (AREA)
- Glass Compositions (AREA)
Abstract
Description
Claims (16)
Priority Applications (1)
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CN201410036348.6A CN104810545B (en) | 2014-01-24 | 2014-01-24 | Phosphate lithium fast-ionic conductor material and preparation method thereof |
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CN201410036348.6A CN104810545B (en) | 2014-01-24 | 2014-01-24 | Phosphate lithium fast-ionic conductor material and preparation method thereof |
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CN104810545A CN104810545A (en) | 2015-07-29 |
CN104810545B true CN104810545B (en) | 2017-08-11 |
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Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
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CN110534681A (en) * | 2018-05-25 | 2019-12-03 | 浙江锋锂新能源科技有限公司 | Conduct the tubular ceramic film and preparation method thereof of ion |
CN109687019A (en) * | 2019-01-22 | 2019-04-26 | 广东天劲新能源科技股份有限公司 | A method of improving oxide solid electrolyte electric conductivity |
JP2021098643A (en) * | 2019-12-20 | 2021-07-01 | Dowaエレクトロニクス株式会社 | Amorphous lithium ion-conductive oxide powder and method for producing the same, and method for producing lithium ion-conductive powder having nasicon-type crystal structure |
CN112830466B (en) * | 2021-01-22 | 2022-11-15 | 中汽创智科技有限公司 | Phosphate fast ion conductor material, preparation method and application |
CN112786891A (en) * | 2021-01-29 | 2021-05-11 | 东莞维科电池有限公司 | Electrode material, electrode plate, preparation method of electrode plate and lithium ion battery |
CN113422108A (en) * | 2021-06-22 | 2021-09-21 | 万年县阿尔伯特新能源研究有限公司 | Novel LGSP solid electrolyte and preparation method thereof |
CN115425314B (en) * | 2022-07-27 | 2023-04-18 | 哈尔滨工业大学 | Method for recycling garnet type solid electrolyte by spinning method |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1925203A (en) * | 2005-08-31 | 2007-03-07 | 株式会社小原 | Lithium ion secondary battery and solid electrolyte therefor |
CN1949569A (en) * | 2005-10-13 | 2007-04-18 | 株式会社小原 | Lithium ion conductive solid electrolyte and method for manufacturing the same |
CN101174698A (en) * | 2006-10-31 | 2008-05-07 | 株式会社小原 | Lithium ion conductive solid electrolyte and a method for manufacturing the same |
CN102468486A (en) * | 2010-11-02 | 2012-05-23 | 三星Sdi株式会社 | Positive active material for lithium secondary battery and method of manufacturing same |
CN103165864A (en) * | 2011-12-13 | 2013-06-19 | 三星电子株式会社 | Protected anode and lithium air battery and all-solid battery including protected anode |
-
2014
- 2014-01-24 CN CN201410036348.6A patent/CN104810545B/en active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1925203A (en) * | 2005-08-31 | 2007-03-07 | 株式会社小原 | Lithium ion secondary battery and solid electrolyte therefor |
CN1949569A (en) * | 2005-10-13 | 2007-04-18 | 株式会社小原 | Lithium ion conductive solid electrolyte and method for manufacturing the same |
CN101174698A (en) * | 2006-10-31 | 2008-05-07 | 株式会社小原 | Lithium ion conductive solid electrolyte and a method for manufacturing the same |
CN102468486A (en) * | 2010-11-02 | 2012-05-23 | 三星Sdi株式会社 | Positive active material for lithium secondary battery and method of manufacturing same |
CN103165864A (en) * | 2011-12-13 | 2013-06-19 | 三星电子株式会社 | Protected anode and lithium air battery and all-solid battery including protected anode |
Non-Patent Citations (1)
Title |
---|
Study on lithium/air secondary batteries—Stability of NASICON-type lithium ion conducting glass–ceramics with water;Satoshi Hasegawa et al.;《Journal of Power Sources》;20080814;第189卷;第371-377页 * |
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CN104810545A (en) | 2015-07-29 |
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Address after: 338004 No. 608 Nan Yuan Road, hi tech Development Zone, Xinyu, Jiangxi Patentee after: Jiangxi Ganfeng lithium Technology Co.,Ltd. Address before: 338004 No. 608 Nan Yuan Road, hi tech Development Zone, Xinyu, Jiangxi Patentee before: JIANGXI GANFENG BATTERY TECHNOLOGY Co.,Ltd. |
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Address after: 338004 No. 608 Nan Yuan Road, hi tech Development Zone, Xinyu, Jiangxi Patentee after: Jiangxi Ganfeng lithium battery technology Co.,Ltd. Address before: 338004 No. 608 Nan Yuan Road, hi tech Development Zone, Xinyu, Jiangxi Patentee before: Jiangxi Ganfeng lithium Technology Co.,Ltd. |