CN104801419A - Strong magnetic purification separation device for raw material liquid in chemical industry production - Google Patents
Strong magnetic purification separation device for raw material liquid in chemical industry production Download PDFInfo
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- CN104801419A CN104801419A CN201510162917.6A CN201510162917A CN104801419A CN 104801419 A CN104801419 A CN 104801419A CN 201510162917 A CN201510162917 A CN 201510162917A CN 104801419 A CN104801419 A CN 104801419A
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Abstract
The invention discloses a strong magnetic purification separation device for raw material liquid in chemical industry production. The strong magnetic purification separation device comprises a solid-liquid separator, a strong magnetic adsorption device, connecting pipes, a distillation box, a condenser and a material liquid collecting tank, wherein a liquid inlet pipe is arranged on the side wall of the solid-liquid separator; the pipe orifice of the liquid inlet pipe is connected with the strong magnetic adsorption device; the pipe orifice of a liquid outlet pipe is connected with a filtration membrane assembly through the connecting pipe; the bottom of the filtration membrane assembly is connected with the distillation box through the connecting pipe; an electrical heater is arranged at the bottom of the distillation box; an air pipe is arranged at the top of the distillation box; a liquid outlet is further formed in the side wall of the distillation box; an exhaust fan is arranged on the air pipe; the tail end of the air pipe is connected with the condenser; the condenser is connected with the material liquid collecting tank through the connecting pipe. The strong magnetic purification separation device for the raw material liquid in chemical industry production is simple in structure, convenient to use, good in purification effect, high in separating efficiency and low in cost, and can treat effective material liquid and other material liquid conveniently.
Description
Technical field
The present invention relates to purification separation device technique field, be specially a kind of Chemical Manufacture Central Plains feed liquid strong magnetic purification separation device.
Background technology
In the production of industrial chemicals liquid, often into catalyst dust can be brought in industrial chemicals liquid, and in the storage and transportation of industrial chemicals liquid, also can be mixed into the iron rust of container and pipeline, wet goods impurity, therefore, purified treatment must be carried out to industrial chemicals liquid, just can reach production energy-conservation, efficiently, free of contamination object, the purification separation device of existing work production Central Plains feed liquid is due to complex structure, unilaterally can only remove the impurity in industrial chemicals liquid, all adopt common screen pack to carry out impurity screening, make inferior separating effect, purification efficiency is low, such as coarse separation device carries out purified treatment to industrial chemicals liquid, Coalescence filter core in device is mainly to be separated into master between liquid and liquid, can only mechanical admixture in filtering industrial chemicals liquid or oiliness impurity, because removal of impurities is single, thus change is impracticable, and for process after feed liquid process aspect be also a difficult problem, so we have proposed a kind of good separating effect, the Chemical Manufacture Central Plains feed liquid purification separation device that purification efficiency is high.
Summary of the invention
The object of the present invention is to provide a kind of Chemical Manufacture Central Plains feed liquid strong magnetic purification separation device, to solve the problem proposed in above-mentioned background technology.
For achieving the above object, the invention provides following technical scheme: a kind of Chemical Manufacture Central Plains feed liquid strong magnetic purification separation device, comprise solid-liquid separator, strong magnetic adsorption device, tube connector, distillation case, condenser and feed liquid collecting tank, the side, lower end of described solid-liquid separator is provided with blow-off pipe, upper end one sidewall of described solid-liquid separator is provided with drain pipe, another sidewall is provided with feed tube, the mouth of pipe place of described feed tube connects strong magnetic adsorption device, and described strong magnetic adsorption device is positioned at the inside of solid-liquid separator, described strong magnetic adsorption device comprises the installation frame body for installing strong bar magnet and forms strong bar magnet by neodymium iron boron rod core and stainless steel surrounding layer, described strong bar magnet is arranged on the inside of installation frame body, the bottom of described solid-liquid separator is also provided with a screen pack, the mouth of pipe of described drain pipe is connected with filter membrane component by tube connector, described filter membrane component comprises screen cloth film, filter film, milipore filter and NF membrane, described screen cloth film, filter film, milipore filter and NF membrane are according to order from top to bottom successively compact siro spinning technology, the bottom of described filter membrane component connects distillation case by tube connector, the bottom of described distillation case is provided with electric heater, top is provided with breather pipe, the sidewall of described distillation case is also provided with liquid outlet, described breather pipe is provided with exhaust fan, the end of described breather pipe connects condenser, described condenser connects feed liquid collecting tank by tube connector.
Preferably, the rectangular inside being arranged on installation frame body of described strong bar magnet, described strong bar magnet is provided with five rows, and one to arrange the quantity that can arrange be five to eight, and described strong bar magnet is perpendicular to the direction of feed liquor stream.
Preferably, the inside of described electric heater is provided with electrical heating wire.
Preferably, described electrical heating wire is the inside that corrugated is laid on electric heater.
Preferably, the sidewall of described distillation case is also provided with temperature sensor, and described temperature sensor is electrically connected with a controller, and the control output end of described controller is electrically connected electric heater.
Preferably, the pore size of described screen pack is 0.1 to 0.5 micron.
Preferably, the pore size of described milipore filter is 0.001 to 0.02 micron, and the pore size of described NF membrane is 1 to 3 nanometer.
Compared with prior art, the invention has the beneficial effects as follows: this Chemical Manufacture Central Plains feed liquid strong magnetic purification separation apparatus structure is simple, easy to use, by being provided with the continuous extraction process adopting ultrafiltration and nanofiltration to combine, especially have employed nanofiltration, effective removal is a large amount of, and oneself knows in industrial chemicals liquid and retains all active ingredient of industrial chemicals liquid while impurity completely usually, and to its efficient concentration, thus while not affecting and extracting active principle in industrial chemicals liquid, significantly reduce the volume of industrial chemicals liquid, effective other invalid impurity having purified industrial chemicals liquid, by being provided with strong magnetic adsorption device, wherein, strong bar magnet is provided with five rows, one to arrange the quantity that can arrange be five to eight, make the magnetic force strong ten times than common permanent-magnet material, can iron content effectively in inspiration liquid or containing aluminium impurity, and can recycle, reduce operating cost, quantity makes its absorption affinity play better more, adsorption function is stronger, by utilizing the boiling point of different material different, distil(l) is carried out to the industrial chemicals liquid after filtering, and obtain required feed liquid by condenser condenses, good purification of the present invention, separative efficiency is high, cost is low, and to effective feed liquid and other feed liquid process convenience.
Accompanying drawing explanation
Fig. 1 is structural representation of the present invention;
Fig. 2 is the structural representation of filter membrane component of the present invention.
In figure: 1 solid-liquid separator, 2 drain pipes, 3 screen packs, 4 feed tubes, the last 5 magnetic adsorption device, 51 installation frame body, the last 52 bar magnet, 6 tube connectors, 7 filter membrane components, 71 screen cloth films, 72 filter films, 73 milipore filters, 74 NF membrane, 8 distillation case, 9 liquid outlets, 10 exhaust fans, 11 condensers, 12 feed liquid collecting tanks, 13 blow-off pipes, 14 temperature sensors, 15 breather pipes, 16 electric heaters, 17 controllers, 18 electrical heating wires.
Detailed description of the invention
Below in conjunction with the accompanying drawing in the embodiment of the present invention, be clearly and completely described the technical scheme in the embodiment of the present invention, obviously, described embodiment is only the present invention's part embodiment, instead of whole embodiments.Based on the embodiment in the present invention, those of ordinary skill in the art, not making the every other embodiment obtained under creative work prerequisite, belong to the scope of protection of the invention.
Refer to Fig. 1-2, the invention provides a kind of technical scheme: a kind of Chemical Manufacture Central Plains feed liquid strong magnetic purification separation device, comprise solid-liquid separator 1, strong magnetic adsorption device 5, tube connector 6, distillation case 8, condenser 11 and feed liquid collecting tank 12, the side, lower end of solid-liquid separator 1 is provided with blow-off pipe 13, upper end one sidewall of solid-liquid separator 1 is provided with drain pipe 2, another sidewall is provided with feed tube 4, the mouth of pipe place of feed tube 4 connects strong magnetic adsorption device 5, and strong magnetic adsorption device 5 is positioned at the inside of solid-liquid separator 1, strong magnetic adsorption device 5 comprises the installation frame body 51 for installing strong bar magnet 52 and forms strong bar magnet 52 by neodymium iron boron rod core and stainless steel surrounding layer, strong bar magnet 52 is arranged on the inside of installation frame body 51, the rectangular inside being arranged on installation frame body 51 of strong bar magnet 52, strong bar magnet 52 is provided with five rows, one to arrange the quantity that can arrange be five to eight, make the magnetic force strong ten times than common permanent-magnet material, can iron content effectively in inspiration liquid or containing aluminium impurity, and can recycle, reduce operating cost, quantity makes its absorption affinity play better more, adsorption function is stronger, and strong bar magnet 52 is perpendicular to the direction of feed liquor stream, the bottom of solid-liquid separator 1 is also provided with a screen pack 3, the pore size of screen pack 3 is 0.1 to 0.5 micron, the mouth of pipe of drain pipe 4 is connected with filter membrane component 7 by tube connector 6, filter membrane component 7 comprises screen cloth film 71, filter film 72, milipore filter 73 and NF membrane 74, screen cloth film 71, filter film 72, milipore filter 73 and NF membrane 74 are according to order from top to bottom successively compact siro spinning technology, the pore size of milipore filter 73 is 0.001 to 0.02 micron, the pore size of NF membrane 74 is 1 to 3 nanometer, the bottom of filter membrane component 7 connects distillation case 8 by tube connector 6, the bottom of distillation case 8 is provided with electric heater 16, the inside of electric heater 16 is provided with electrical heating wire 18, electrical heating wire 18 is laid on the inside of electric heater 16 in corrugated, the sidewall of distillation case 8 is also provided with temperature sensor 14, temperature sensor 14 is electrically connected with a controller 17, the control output end of controller 17 is electrically connected electric heater 16, the top top of distillation case 8 is provided with breather pipe 15, the sidewall of distillation case 8 is also provided with liquid outlet 9, breather pipe 15 is provided with exhaust fan 10, the end of breather pipe 15 connects condenser 11, condenser 11 connects feed liquid collecting tank 12 by tube connector 6.
Operation principle: industrial chemicals liquid enters solid-liquid separator 1 by feed tube 4, feed tube 4 connects strong magnetic adsorption device 5, industrial chemicals liquid first passes through strong magnetic adsorption device 5, iron content a large amount of in industrial chemicals liquid or absorbed containing the impurity of aluminium, then the decline of industrial chemicals liquid is full of the bottom of solid-liquid separator 1, liquid level is rising submergence screen pack 3 gradually, wherein be greater than separated the getting off of solid particle of 0.1 to 0.5 micron and fall into the bottom of solid-liquid separator 1, industrial chemicals liquid continues upwards to stretch to the top of solid-liquid separator 1, then discharge from drain pipe 2, and enter in filter membrane component 7, by milipore filter 73 and the NF membrane 74 of setting, effective removal is a large amount of, and oneself knows in industrial chemicals liquid and retains all active ingredient of industrial chemicals liquid while impurity completely usually, and to its efficient concentration, thus while not affecting and extracting active principle in industrial chemicals liquid, significantly reduce the volume of industrial chemicals liquid, and the industrial chemicals liquid after making it filter enters distillation case 8 by tube connector 6, now open electric heater 16 to heat distillation case 8, enter according to the boiling point difference of the different material in different industrial chemicals liquid and carry out separation and Extraction, low-boiling feed liquid, air-flow is formed after heating, condenser 11 is entered under the effect of exhaust fan 10, by condenser 11 condensation carried out to it and flow into feed liquid collecting tank 12 by tube connector 6, electric heater 16 is electrically connected controller 17, and the lateral wall of distillation case 8 is provided with temperature sensor 14, the heating-up temperature in distillation case 8 can be changed in real time, thus accurately can carry out purification separation to industrial chemicals liquid, structure of the present invention is simple, easy to use, by being provided with the continuous extraction process adopting ultrafiltration and nanofiltration to combine, especially have employed nanofiltration, effective removal is a large amount of, and oneself knows in industrial chemicals liquid and retains all active ingredient of industrial chemicals liquid while impurity completely usually, and to its efficient concentration, thus while not affecting and extracting active principle in industrial chemicals liquid, significantly reduce the volume of industrial chemicals liquid, effective other invalid impurity having purified industrial chemicals liquid, by being provided with strong magnetic adsorption device 5, wherein, strong bar magnet 52 is provided with five rows, one to arrange the quantity that can arrange be five to eight, make the magnetic force strong ten times than common permanent-magnet material, can iron content effectively in inspiration liquid or containing aluminium impurity, and can recycle, reduce operating cost, quantity makes its absorption affinity play better more, adsorption function is stronger, by utilizing the boiling point of different material different, distil(l) is carried out to the industrial chemicals liquid after filtering, thus obtain required feed liquid, good purification of the present invention, separative efficiency is high, cost is low, effectively other process can be carried out to waste liquid by the blow-off pipe 13 arranged.
Although illustrate and describe embodiments of the invention, for the ordinary skill in the art, be appreciated that and can carry out multiple change, amendment, replacement and modification to these embodiments without departing from the principles and spirit of the present invention, scope of the present invention is by claims and equivalents thereof.
Claims (7)
1. a Chemical Manufacture Central Plains feed liquid strong magnetic purification separation device, comprise solid-liquid separator (1), strong magnetic adsorption device (5), tube connector (6), distillation case (8), condenser (11) and feed liquid collecting tank (12), the side, lower end of described solid-liquid separator (1) is provided with blow-off pipe (13), upper end one sidewall of described solid-liquid separator (1) is provided with drain pipe (2), another sidewall is provided with feed tube (4), it is characterized in that: the mouth of pipe place of described feed tube (4) connects strong magnetic adsorption device (5), and described strong magnetic adsorption device (5) is positioned at the inside of solid-liquid separator (1), described strong magnetic adsorption device (5) comprises the installation frame body (51) for installing strong bar magnet (52) and forms strong bar magnet (52) by neodymium iron boron rod core and stainless steel surrounding layer, described strong bar magnet (52) is arranged on the inside of installation frame body (51), the bottom of described solid-liquid separator (1) is also provided with a screen pack (3), the mouth of pipe of described drain pipe (4) is connected with filter membrane component (7) by tube connector (6), described filter membrane component (7) comprises screen cloth film (71), filter film (72), milipore filter (73) and NF membrane (74), described screen cloth film (71), filter film (72), milipore filter (73) and NF membrane (74) are according to order from top to bottom successively compact siro spinning technology, the bottom of described filter membrane component (7) connects distillation case (8) by tube connector (6), the bottom of described distillation case (8) is provided with electric heater (16), top is provided with breather pipe (15), the sidewall of described distillation case (8) is also provided with liquid outlet (9), described breather pipe (15) is provided with exhaust fan (10), the end of described breather pipe (15) connects condenser (11), described condenser (11) connects feed liquid collecting tank (12) by tube connector (6).
2. a kind of Chemical Manufacture Central Plains feed liquid according to claim 1 strong magnetic purification separation device, it is characterized in that: the described rectangular inside being arranged on installation frame body (51) of strong bar magnet (52), described strong bar magnet (52) is provided with five rows, one to arrange the quantity that can arrange be five to eight, and described strong bar magnet (52) is perpendicular to the direction of feed liquor stream.
3. a kind of Chemical Manufacture Central Plains feed liquid according to claim 1 strong magnetic purification separation device, is characterized in that: the inside of described electric heater (16) is provided with electrical heating wire (18).
4. a kind of Chemical Manufacture Central Plains feed liquid according to claim 3 strong magnetic purification separation device, is characterized in that: described electrical heating wire (18) is laid on the inside of electric heater (16) in corrugated.
5. a kind of Chemical Manufacture Central Plains feed liquid according to claim 1 strong magnetic purification separation device, it is characterized in that: the sidewall of described distillation case (8) is also provided with temperature sensor (14), described temperature sensor (14) is electrically connected with a controller (17), and the control output end of described controller (17) is electrically connected electric heater (16).
6. a kind of Chemical Manufacture Central Plains feed liquid according to claim 1 strong magnetic purification separation device, is characterized in that: the pore size of described screen pack (3) is 0.1 to 0.5 micron.
7. a kind of Chemical Manufacture Central Plains feed liquid according to claim 1 strong magnetic purification separation device, is characterized in that: the pore size of described milipore filter (73) is 0.001 to 0.02 micron, the pore size of described NF membrane (74) is 1 to 3 nanometer.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510162917.6A CN104801419A (en) | 2015-04-09 | 2015-04-09 | Strong magnetic purification separation device for raw material liquid in chemical industry production |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510162917.6A CN104801419A (en) | 2015-04-09 | 2015-04-09 | Strong magnetic purification separation device for raw material liquid in chemical industry production |
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| CN104801419A true CN104801419A (en) | 2015-07-29 |
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| CN201510162917.6A Pending CN104801419A (en) | 2015-04-09 | 2015-04-09 | Strong magnetic purification separation device for raw material liquid in chemical industry production |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113292590A (en) * | 2021-05-21 | 2021-08-24 | 江西国化实业有限公司 | Separation device for preparing trimethylsilyl trifluoromethanesulfonate and using method |
-
2015
- 2015-04-09 CN CN201510162917.6A patent/CN104801419A/en active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113292590A (en) * | 2021-05-21 | 2021-08-24 | 江西国化实业有限公司 | Separation device for preparing trimethylsilyl trifluoromethanesulfonate and using method |
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Application publication date: 20150729 |
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