CN104789158B - Environmental-protection pure natural essential oil vamp balosam is stuck with paste and is pasted the fragrant footwear of work with this balosam - Google Patents
Environmental-protection pure natural essential oil vamp balosam is stuck with paste and is pasted the fragrant footwear of work with this balosam Download PDFInfo
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- CN104789158B CN104789158B CN201510111856.0A CN201510111856A CN104789158B CN 104789158 B CN104789158 B CN 104789158B CN 201510111856 A CN201510111856 A CN 201510111856A CN 104789158 B CN104789158 B CN 104789158B
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- 239000000341 volatile oil Substances 0.000 title claims abstract description 58
- 239000003094 microcapsule Substances 0.000 claims abstract description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 19
- 229920000858 Cyclodextrin Polymers 0.000 claims abstract description 16
- 238000003756 stirring Methods 0.000 claims abstract description 14
- 244000215068 Acacia senegal Species 0.000 claims abstract description 13
- 229920000084 Gum arabic Polymers 0.000 claims abstract description 13
- 235000010489 acacia gum Nutrition 0.000 claims abstract description 13
- 239000000205 acacia gum Substances 0.000 claims abstract description 13
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- 235000007164 Oryza sativa Nutrition 0.000 claims abstract description 10
- 235000009566 rice Nutrition 0.000 claims abstract description 10
- 229920002907 Guar gum Polymers 0.000 claims abstract description 9
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- 239000004744 fabric Substances 0.000 claims abstract description 7
- 239000001116 FEMA 4028 Substances 0.000 claims abstract description 6
- WHGYBXFWUBPSRW-FOUAGVGXSA-N beta-cyclodextrin Chemical compound OC[C@H]([C@H]([C@@H]([C@H]1O)O)O[C@H]2O[C@@H]([C@@H](O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O3)[C@H](O)[C@H]2O)CO)O[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@@H]3O[C@@H]1CO WHGYBXFWUBPSRW-FOUAGVGXSA-N 0.000 claims abstract description 6
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- 238000000034 method Methods 0.000 claims abstract description 5
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- HFHDHCJBZVLPGP-UHFFFAOYSA-N schardinger α-dextrin Chemical compound O1C(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(O)C2O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC2C(O)C(O)C1OC2CO HFHDHCJBZVLPGP-UHFFFAOYSA-N 0.000 description 10
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- WQZGKKKJIJFFOK-PQMKYFCFSA-N alpha-D-mannose Chemical group OC[C@H]1O[C@H](O)[C@@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-PQMKYFCFSA-N 0.000 description 1
- 230000003064 anti-oxidating effect Effects 0.000 description 1
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- 239000003440 toxic substance Substances 0.000 description 1
- 238000009423 ventilation Methods 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
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Landscapes
- Footwear And Its Accessory, Manufacturing Method And Apparatuses (AREA)
Abstract
Pure natural essential oil vamp balosam is stuck with paste and is pasted the fragrant footwear of work with this balosam, and balosam is stuck with paste and is made up of the raw material of following weight parts: sticky rice flour 1 part, gum arabic 1.3 ~ 1.6 parts, guar gum 1.8 ~ 2.4 parts, pure water 64 parts, beta-cyclodextrin 6 parts, natural essential oil 1 part.Its making method is: be heated to 100 ~ 120 DEG C with sticky rice flour and pure water uniform stirring and obtain glutinous paste; By gum arabic, beta-cyclodextrin is poured in pure water in proportion and is stirred, and is warmed up to 60 DEG C, then pour into natural essential oil uniform stirring 4 hours essential oil clathrate; Guar gum is poured in essential oil clathrate and stirs, then glutinous paste poured into wherein stir.The vamp of fragrant footwear and setting cloth and shoe lining are stuck with paste with balosam of the present invention and are bonded; The middle level natural palm skin of the middle end of fragrant footwear fixes essential oil microcapsules, and the essential oil microcapsules in vamp of the present invention and by the fragrant molecule of lasting release that rubs at middle the end.Pure natural environment protection of the present invention without chemical pollution, environmental health.
Description
Technical field
The present invention relates to and delay essential oil volatilization and the Environmental-protection pure natural essential oil vamp balosam that stops essential oil and chemical glue that chemical reaction occurs again is stuck with paste, also relate to the fragrant footwear pasting work with this natural essential oil balosam.
Background technology
Modern science proves, the fragrance of pure natural essential oil volatilization is containing the trace unit number being of value to HUMAN HEALTH.The nasal membrane of people secretes a kind of immunoglobulin A, hears the fragrant content that can improve albumin A and strengthens human body disease resistance, reduce the pathogenetic probability of disease by nasal cavity.Pure natural essential oil can be absorbed by skin in blood, and participates in the biochemical reaction of whole body.Essential oil is not as chemicals in Remained mass, and their by urinating, be perspired and exhaling and discharging, and the time of discharge needs 3 ~ 6 hours.Essential oil also has antisepsis and anti-inflammation, deodorizing corrosion-preventing, neuralgia, rheumatism, spasmolytic, removing toxic substances, anti-melancholy, and sedation-analgesia is aid digestion, Eradicates phlegm, and skin care promotes circulation, promotes the effects such as wound healing.Modern shoe industry is want essential oil or spices to be attached in shoe industry to go very much, but owing to being subject to technical limitation, applies also immature.Major Difficulties has two, and one is to control essential oil volatilization; Two is that essential oil and chemical glue chemical reaction can occur, and produces a kind of objectionable impurities affecting Fertility of being plasticizer.In existing footwear art, have essential oil, spices are placed in the end, some placement shoe-pads, what have puts in sole groove or glue air bag, or to be directly pressed into by essence molecule by High Temperature High Pressure or to be injected in footwear material or to add in glue.But these technology not can solve the pollution again of essential oil or spices, and the problem of essential oil and chemical industry glue chemical reaction again.The problem that essential oil slowly volatilizees can not be controlled simultaneously.Some perfuming technology also may can change the normal configuration of shoes.And above-mentioned various problem will be solved, just must in conjunction with modern crafts (mechanised equipment, microcapsule essence technology) exploitation of innovation technology, reduce a part of ancient technique, the footwear made are made namely not change profile, do not change the Rational structure of footwear, really make natural environmental-protective, the fragrant footwear of pure natural essential oil that fragrance is lasting yet.
Summary of the invention
The technical problem to be solved in the present invention is, develops a kind of essential oil that delays and slowly to volatilize and the Environmental-protection pure natural essential oil vamp balosam that prevents essential oil and chemical glue from chemical reaction occurring again is stuck with paste; The fragrant footwear pasting work with this balosam are provided simultaneously.As much as possible reduce and use chemical materials, stop to use containing toluene class Chemicals, reduce environmental pollution, protection workman life security, produce the fragrant footwear of Environmental-protection pure natural essential oil of favourable consumer health.
For achieving the above object, utilize gum arabic, guar gum, sticky rice flour, cyclodextrin acting in conjunction point all needs pure water and the interactional characteristic of energy, has invented the vamp balosam paste that the same viscosity of the yellow glue of a kind of existing chemical industry has carried out again essential oil microcapsules inclusion.The technical solution used in the present invention is, a kind of Environmental-protection pure natural essential oil vamp balosam is stuck with paste, and is made up of: sticky rice flour 1 part the raw material of following weight parts, gum arabic 1.3 ~ 1.6 parts, guar gum 1.8 ~ 2.4 parts, pure water 64 parts, beta-cyclodextrin 6 parts, natural essential oil 1 part.
The operation steps of making method of the present invention is as follows:
A. sticky rice flour 1 part, pure water 4 parts, uniform stirring is without bulk; Be heated to 100 ~ 120 degree, stir to obtain glutinous paste;
B. by gum arabic 1.3 ~ 1.6 parts, beta-cyclodextrin 6 parts is poured in 60 parts of pure water and is stirred, and is warming up to 60 ~ 65 DEG C, is poured into by 1 part of natural essential oil, and uniform stirring 4 hours, obtains essential oil clathrate, i.e. essential oil microcapsules.
C. guar gum 1.8 ~ 2.4 parts is poured in essential oil clathrate and stir, then the glutinous paste of 100 ~ 120 DEG C is poured into wherein stir, obtain environmental-friendly natural essential oil vamp balosam and stick with paste.
With the shoes that the essential oil microcapsules that above-mentioned Environmental-protection pure natural essential oil vamp balosam is stuck with paste and prepared by aforesaid method makes, shoes comprise vamp, the middle end, the large end.Stick with paste bonding vamp and setting cloth and shoe lining with pure natural environment protection essential oil vamp balosam, then dry.The middle end, divides three layers, base fabric high temperature laminating in bottom waterproof membrane, and organic solvent when stoping vamp and large primer to close in glue invades; Middle level is that natural palm skin fixes essential oil microcapsules enhancing ventilation property, and upper strata is ventilative middle base fabric.Three layers of combination high frequency are pressed into middle base plate.Whole shoes chemical glue useless.
The beneficial effect that the technology of the present invention is brought, without the volatilization of toxic organic compound in a glue, protection workman and human consumer healthy, reduce environmental pollution; Two is that adhesive strength pure natural vamp balosam is stuck with paste and the yellow glue of chemical industry does not have difference; Three is that pure natural vamp balosam paste has good water-absorbent and drainage, the moisture that pin in footwear produces can be discharged outside footwear in time, make in footwear dry and comfortable, ventilative; Four volatilizations effectively alleviating fragrant molecule, working lipe can reach more than 1 year; Five is overcome the impact of essential oil by temperature and light; Six is carry the time grown and stored; Seven accessibility used, what can be put into footwear appoints conjunction position.In vamp microcapsule and at middle the end microcapsule all make microcapsules by friction and discharge fragrant molecule.
Scientific basis of the present invention is as follows:
One, microcapsule essence technology microcapsule essence technology is a kind of film forming material solid or the coated and fine particle that formed of liquid.General particle is in micron and millimeter scope.Essential oil all has the fast feature of volatility, and be heated especially and can accelerate volatilization, its application is restricted.Microcapsule essence technology can overcome this shortcoming.The advantage of microcapsule essence technology is as follows: the essential oil after micro encapsulation can protect its distinctive fragrance and fragrance matter to avoid directly being heated, the impact of light and temperature and shadow plays deterioration by oxidation.Avoid effective constituent to lose because of volatilization, effectively can control the slow releasing of fragrance matter, improve the accessibility storing, transport and apply.The wall material of microcapsulary has: xanthan gum, gelatin, carrageenin, gum arabic, soybean protein, carboxymethyl cellulose, ethyl cellulose, methylcellulose gum etc.
Two, cyclodextrin cyclodextrin can store and never degenerate for many years as starch.Cyclodextrin, originally as natural product, has nontoxic, biodegradable, the not easily advantage of the moisture absorption and caking.Cyclodextrin is a kind of microcapsule formed on a molecular scale as coating material, is also to apply the wider physical method preparing microcapsule in recent years.
The inclusion principle of cyclodextrin is; There are hydrophobic lipophilic effect and spatial volume matching effect in the hollow cave of cyclodextrin, and has suitable size, shape and hydrophobic molecule and forms stable inclusion compound by the effect of non covalent bond.Spices pigment and the sizeable molecule of VITAMIN equimolecular all can form inclusion compound with cyclodextrin.The reaction forming inclusion compound generally can only be carried out when water exists.When cyclodextrin is water-soluble, the annular center cavity of cyclodextrin is also occupied by water molecules, when adding nonpolar foreign molecules (essential oil), because hydrophobic cavity is more easily combined with nonpolar foreign molecules, these moisture are replaced by foreign molecules very soon, form more stable inclusion compound.
Three, gum arabic is a kind of food thickener of natural safety non-toxic, and be the natural gum of natural coagulation in atmosphere, gum arabic is good water-soluble dietary fibre, is applied to healthcare products, candy and beverage.Gum arabic has solubility, and the colloid adding 5 ~ 8% in water solubilization can reach capacity, and the blending ratio of gum arabic and water can reach 60%, has very high viscosity when high-content.Gum arabic has good film forming characteristics, and be medically used for volatile oil or other liquid as microcapsule membrane-forming agent, changing into powder type can extend flavor quality, and anti-oxidation, be also used as the carrier for essence drying product of founding.
Four, guar gum, after removing the peel the endosperm position drying and crushing after degerming by fabaceous seed, obtains after the pressurized hydrolysis that adds water by drying and crushing after the alcohol settling centrifugation of 20%.Guar gum main component to be molecular weight be 5 ~ 800,000 the polygalactomannan that combines of glycosidic linkage, the high molecular hydrocolloid polyose be made up of semi-lactosi and seminose, dispersion forms viscous fluid in the hot water or in cold water, the water-soluble viscosity of 1% is about 4 ~ 5Pa.s, for natural gum viscosity is the highest, water-soluble is neutral.Owing to having very high wetting ability, cohesiveness, be therefore widely used in the food industry, as cold drink flour products, beverage etc.
Five, sticky rice flour is a kind of food materials, be difficult to water-soluble at normal temperatures, but when being heated to 80 ~ 95 DEG C, starch molecule crystallizing field hydrogen bond is cut off, and crystalline texture is damaged, and to make free-water be easy to infiltrate starch molecule inner, and therefore temperature its solubleness higher is also larger.The essence of sticky rice flour gelatinization is that water molecules enters microlitic structure, breaks the association situation of starch molecule, starch molecule or its congeries height aquation and form gel, and it is very strong that sticky rice flour belongs to amylopectin viscosity, very strong to the viscosity of fiber band hair body and cotton class especially.
Claims (3)
1. Environmental-protection pure natural essential oil vamp balosam is stuck with paste, and is made up of: sticky rice flour 1 part, gum arabic 1.3 ~ 1.6 parts, guar gum 1.8 ~ 2.4 parts, pure water 64 parts, beta-cyclodextrin 6 parts, natural essential oil 1 part the raw material of following weight parts.
2. the making method of Environmental-protection pure natural essential oil vamp balosam paste, the steps include:
A. sticky rice flour 1 part, pure water 4 parts, uniform stirring is without bulk; Be heated to 100 ~ 120 DEG C, stir to obtain glutinous paste;
B. by gum arabic 1.3 ~ 1.6 parts, beta-cyclodextrin 6 parts is poured in 60 parts of pure water and is stirred, and is warmed up to 60 ~ 65 DEG C, is poured into by 1 part of natural essential oil, and uniform stirring 4 hours, obtains essential oil clathrate, i.e. essential oil microcapsules;
C. guar gum 1.8 ~ 2.4 parts is poured in essential oil clathrate and stir, then the glutinous paste of 100 ~ 120 DEG C is poured into wherein stir, obtain environmental-friendly natural essential oil vamp balosam and stick with paste.
3. with the fragrant footwear that the essential oil microcapsules that Environmental-protection pure natural essential oil vamp balosam described in claim 1 is stuck with paste and prepared by claim 2 makes, fragrant footwear comprise upper of a shoe, the middle end, the large end, it is characterized in that: vamp and setting cloth and shoe lining Environmental-protection pure natural essential oil balosam are stuck with paste and bonded, and then dry; The middle end, divides three layers, base fabric high temperature laminating in bottom waterproof membrane, and organic solvent when stoping vamp and large primer to close in glue invades; Middle level is that natural palm skin fixes essential oil microcapsules, and upper strata is ventilative middle base fabric; The middle end is pressed into high frequency after three layers of combination.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510111856.0A CN104789158B (en) | 2015-03-16 | 2015-03-16 | Environmental-protection pure natural essential oil vamp balosam is stuck with paste and is pasted the fragrant footwear of work with this balosam |
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| CN201510111856.0A CN104789158B (en) | 2015-03-16 | 2015-03-16 | Environmental-protection pure natural essential oil vamp balosam is stuck with paste and is pasted the fragrant footwear of work with this balosam |
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| CN104789158B true CN104789158B (en) | 2016-03-16 |
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| CN105996288B (en) * | 2016-06-22 | 2017-07-18 | 周贤良 | The preparation method that environmental protection removes foot odour health-care functional shoe |
| CN107280142A (en) * | 2017-05-31 | 2017-10-24 | 苏州峰佳医疗科技有限公司 | Foot orthopedic insoles and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102008149A (en) * | 2011-01-08 | 2011-04-13 | 石国明 | Method for manufacturing deodorant shoe and deodorant shoe |
| CN102408946A (en) * | 2011-10-24 | 2012-04-11 | 日照日纳功能材料科技有限公司 | High temperature resistant essence |
| CN102925075A (en) * | 2012-11-09 | 2013-02-13 | 宁波雅特化工科技发展有限公司 | Biology starch-base solid gum and preparation method thereof |
| CN102952274A (en) * | 2012-08-01 | 2013-03-06 | 湖北工业大学 | Arabic gum component grading method as well as product thereby and application of product |
| CN103666368A (en) * | 2013-12-21 | 2014-03-26 | 栾晓健 | Natural adhesive |
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Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102008149A (en) * | 2011-01-08 | 2011-04-13 | 石国明 | Method for manufacturing deodorant shoe and deodorant shoe |
| CN102408946A (en) * | 2011-10-24 | 2012-04-11 | 日照日纳功能材料科技有限公司 | High temperature resistant essence |
| CN102952274A (en) * | 2012-08-01 | 2013-03-06 | 湖北工业大学 | Arabic gum component grading method as well as product thereby and application of product |
| CN102925075A (en) * | 2012-11-09 | 2013-02-13 | 宁波雅特化工科技发展有限公司 | Biology starch-base solid gum and preparation method thereof |
| CN103666368A (en) * | 2013-12-21 | 2014-03-26 | 栾晓健 | Natural adhesive |
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