CN104777277A - Equipment for measuring mass of medicinal powder during heating process - Google Patents
Equipment for measuring mass of medicinal powder during heating process Download PDFInfo
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- CN104777277A CN104777277A CN201510114981.7A CN201510114981A CN104777277A CN 104777277 A CN104777277 A CN 104777277A CN 201510114981 A CN201510114981 A CN 201510114981A CN 104777277 A CN104777277 A CN 104777277A
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- baking oven
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- level acquisition
- axostylus axostyle
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Abstract
The invention discloses equipment for measuring the mass of medicinal powder during the heating process. The equipment can online detect the mass change of medicinal powder during the heating process synchronously without being affected by the exterior environment. The equipment is capable of collecting the gas in a baking oven and precisely measuring the mass loss of medicinal powder during the heating process without being affected by the air flow in the baking oven. The equipment comprises a baking oven, an installation rack, an electronic weighing device arranged on the bottom of the baking oven, a gas sampling device, and a volume compensation device, wherein the gas sampling device and the volume compensation device are arranged on the baking oven.
Description
Technical field
The present invention relates to a kind of medicinal powder heating quality measuring equipment, be specifically related to a kind ofly on-line synchronous to detect the measuring equipment of medicinal powder heating quality.
Background technology
In current existing technology, usually adopt and measure the mass change of medicinal powder in heating process with the following method: first medicinal powder will be put into baking oven and heat, after a period of time to be heated, medicinal powder is taken out, and after being cooled to room temperature; Then by the medicinal powder quality of balance measurement after heating, thus the change of heating forward and backward medicinal powder quality is obtained.On the other hand, in order to analyze in medicinal powder heating process the gas discharging/decompose; In the process of heating medicinal powder, extract the gas in baking oven by air pump, thus gather the gas decomposed in medicinal powder thermal decomposition gasification.
In current this measurement medicinal powder heating process, not only efficiency is low for the method for mass change, and when medicinal powder is by taking out in baking oven, cooling, in the process measured in balance again, medicinal powder high and low temperature alternative, ambient humidity changes, from air, absorbing moisture etc. during as shifted out to have an impact to the accuracy of the data of reality, causing the mass loss that measurement data is difficult in authentic and valid reaction medicinal powder heating process.
In addition, due in the process of heating medicinal powder, extract the gas in baking oven by air pump, gather the gas decomposed in medicinal powder thermal decomposition gasification, so just will form air flowing in baking oven; And the weighing precision of electronic weighing device (as electronic balance) is high, and mass change amount in medicinal powder heating process this is just very little, the air flowing of baking oven will have influence on the weighing accuracy of electronic weighing device, especially for Powdered medicinal powder such as medicinal powder, the impact by air flowing is larger; Thus the mass loss causing measurement data to be difficult in authentic and valid reaction medicinal powder heating process.
Summary of the invention
The object of the invention is to overcome deficiency of the prior art, providing a kind of medicinal powder heating quality measuring equipment, it on-line synchronous can not only detect the change of medicinal powder heating quality, avoids the impact by external environment; And can have and while gas, effectively avoid causing measurement data to be difficult to the problem of the mass loss in authentic and valid reaction medicinal powder heating process because forming air flowing in baking oven in collection baking oven.
Technical scheme of the present invention is:
A kind of medicinal powder heating quality measuring equipment, comprises baking oven, erecting frame, is arranged on the electronic weighing device bottom baking oven, be arranged on the gas sampling assembly on baking oven and volume compensation device; Described volume compensation device comprises and being arranged on baking oven side and the horizontally-guided cover be connected with oven ncavity, slidably be arranged on the compensation cylinder in horizontally-guided cover, overlap between medial surface on described horizontally-guided cover medial surface, at compensation cylinder and horizontally-guided and be provided with the first O-ring seal; Described gas sampling assembly comprises the level acquisition cylinder body be arranged on erecting frame, coaxially be arranged on the passing axostylus axostyle in level acquisition cylinder body and at least two piston bodies be slidably arranged in level acquisition cylinder body, and be connected by connecting axostylus axostyle between adjacent two-piston body, be also provided with pneumatophore between adjacent two-piston body; One end of level acquisition cylinder body is connected with oven ncavity, the other end is provided with dodges through hole, one end of described passing axostylus axostyle is connected with near the piston body of dodging through hole, the other end is through dodging through hole, and be positioned at outside level acquisition cylinder body, pass axostylus axostyle to be provided with along passing the axially extended main air guide channel of axostylus axostyle, and main air guide channel extends toward piston body direction, and through each connection axostylus axostyle; One end of this main air guide channel toward extension, and passing axostylus axostyle outside level acquisition cylinder body forms porting, and the other end is closed; Each connection axostylus axostyle lateral surface is respectively equipped with the radial direction through hole be connected with main air guide channel, and the inner chamber of each pneumatophore is connected with corresponding radial direction through hole respectively; Described level acquisition cylinder body lateral surface is provided with at least one sampling through hole be communicated with level acquisition inner chamber of cylinder block, and is provided with the seal plug that can take out in sampling through hole; On described passing axostylus axostyle, be positioned at inside level acquisition cylinder body and be provided with positive stop, when interior positive stop is resisted against on the level acquisition cylinder body end face of dodging through hole place, each piston body is positioned at level acquisition cylinder interior, and level acquisition cylinder body between adjacent two-piston body has the sampling through hole described in respectively;
Described level acquisition cylinder body and horizontally-guided cover are positioned at the relative both sides of baking oven, and level acquisition cylinder body and horizontally-guided overlap coaxial setting, coupling shaft rod member is provided with between described compensation cylinder and the close piston body compensating cylinder, one end of this coupling shaft rod member is connected with the end face compensating cylinder, and the other end is connected with piston body end face; Described erecting frame is provided with the promotion cylinder for pushing piston body.
This programme heats medicinal powder by baking oven, and carrys out the change of on-line synchronous detection medicinal powder heating quality by electronic weighing device, thus avoids the impact by external environment, effectively improves measurement efficiency and measurement accuracy.On the other hand, this case gathers the gas in the baking oven in baking oven heating process by gas sampling assembly, thus gathers the gas decomposed in medicinal powder thermal decomposition gasification; And in gas collecting process, the volume compensation device of this programme will carry out isopyknic compensation to oven ncavity simultaneously, avoid because in baking oven, gas is removed, and cause baking oven internal gas pressure to reduce, ensure to adopt in process at gas, air pressure in baking oven keeps stable, so just can effectively avoid forming air stream in baking oven in gas collecting process; Thus this programme can effectively be avoided causing measurement data to be difficult to the problem of the mass loss in authentic and valid reaction medicinal powder heating process because forming air flowing in baking oven.
As preferably, the internal diameter of level acquisition cylinder body is identical with the external diameter compensating cylinder.
As preferably, pneumatophore comprises the Air sac cover being set in and connecting on axostylus axostyle, and the two ends of Air sac cover respectively be connected axostylus axostyle lateral surface and be tightly connected.
As preferably, electronic weighing device comprises electronic balance, be arranged on the pallet in baking oven, to be arranged on baking oven bottom surface and the bar through hole be positioned at immediately below pallet, be arranged on the vertical support bar of support plate immediately below bar through hole and connecting trays and support plate, vertical support bar is through bar through hole.
As preferably, pass on axostylus axostyle, be positioned at outside level acquisition cylinder body and be provided with outer positive stop, and when outer positive stop leans against on the level acquisition cylinder body end face of dodging through hole place, piston body adjacent with passing axostylus axostyle in each piston body is positioned at level acquisition cylinder body, and all the other piston bodies are positioned at the baking oven outside level acquisition cylinder body.
As preferably, be provided with thermopair in pallet, described baking oven bottom surface is provided with through wires hole, and is provided with seal rubber sleeve in through wires hole, and the signal wire of described thermopair is through seal rubber sleeve.
As preferably, baking oven is provided with the temperature sensor of the temperature for detecting oven ncavity.
The invention has the beneficial effects as follows: on-line synchronous can not only detect the change of medicinal powder heating quality, avoid the impact by external environment; And can have and while gas, effectively avoid causing measurement data to be difficult to the problem of the mass loss in authentic and valid reaction medicinal powder heating process because forming air flowing in baking oven in collection baking oven.
Accompanying drawing explanation
Fig. 1 is a kind of structural representation of the present invention.
Fig. 2 is a kind of cross-sectional view before gas sampling assembly of the present invention does not gather gas.
Fig. 3 is a kind of cross-sectional view after gas sampling assembly of the present invention completes gas collecting.
In figure: baking oven 1, gas sampling assembly 2, piston body 21, connect axostylus axostyle 22, pneumatophore 23, interior positive stop 24, pass axostylus axostyle 25, level acquisition cylinder body 26, outer positive stop 27, dodge through hole 28, seal plug 29, main air guide channel 210, radial direction through hole 211, porting 212, electronic weighing device 3, pallet 31, support plate 32, vertically support bar 33, thermopair 34, electronic balance 35, volume compensation device 4, horizontally-guided cover 41, compensation cylinder 42, first O-ring seal 43, connecting rod 5, erecting frame 6.
Embodiment
Below in conjunction with accompanying drawing and embodiment, the present invention is described in further detail:
As shown in Figure 1 and Figure 2, a kind of medicinal powder heating quality measuring equipment comprises baking oven 1, erecting frame 6, is arranged on the electronic weighing device 3 bottom baking oven, is arranged on the gas sampling assembly 2 on baking oven and volume compensation device 4.Oven ncavity is seal chamber.The side of baking oven is provided with sealed container door.Feet is provided with bottom baking oven.Baking oven is provided with the temperature sensor of the temperature for detecting oven ncavity.Baking oven is also provided with electric heater.
Electronic weighing device comprises electronic balance 35, be arranged on the pallet 31 in baking oven, to be arranged on baking oven bottom surface and the bar through hole be positioned at immediately below pallet, to be arranged on the vertical support bar 33 of support plate 32 immediately below bar through hole and connecting trays and support plate.Vertical support bar is through bar through hole.Thermopair 34 is provided with in pallet.Baking oven bottom surface is provided with through wires hole, and is provided with seal rubber sleeve in through wires hole.The signal wire of thermopair is through seal rubber sleeve.Electronic balance is positioned at below baking oven.
Volume compensation device 4 comprises and to be arranged on baking oven side and the horizontally-guided be connected with oven ncavity overlaps 41, is slidably arranged on the compensation cylinder 42 in horizontally-guided cover.On horizontally-guided cover medial surface, between compensation cylinder and orienting sleeve medial surface, be provided with the first O-ring seal 43.
Gas sampling assembly 2 comprises the level acquisition cylinder body 26 be arranged on erecting frame, coaxially be arranged on the passing axostylus axostyle 25 in level acquisition cylinder body and four piston bodies 21 be slidably arranged in level acquisition cylinder body, and be connected by connecting axostylus axostyle 22 between adjacent two-piston body, be also provided with pneumatophore 23 between adjacent two-piston body.Connection axostylus axostyle and piston body are coaxially arranged.Four piston bodies are equally spaced.One end of level acquisition cylinder body is connected with oven ncavity, and the other end is provided with dodges through hole 28.The one end of passing axostylus axostyle is connected with near the piston body of dodging through hole, and the other end through dodging through hole, and is positioned at outside level acquisition cylinder body.Pass axostylus axostyle to be provided with along passing the axially extended main air guide channel 210 of axostylus axostyle, and main air guide channel extends toward piston body direction, and through each connection axostylus axostyle.One end of this main air guide channel toward extension, and passing axostylus axostyle outside level acquisition cylinder body forms porting 212, and the other end is closed.Each connection axostylus axostyle lateral surface is respectively equipped with the radial direction through hole 211 be connected with main air guide channel.The inner chamber of each pneumatophore is connected with corresponding radial direction through hole respectively.Pneumatophore comprises and is set in the Air sac cover connected on axostylus axostyle, and the two ends of Air sac cover respectively be connected axostylus axostyle lateral surface and be tightly connected.
Level acquisition cylinder body lateral surface is provided with three sampling through holes be communicated with level acquisition inner chamber of cylinder block, and is provided with the seal plug 29 that can take out in sampling through hole.Be threaded connection between seal plug and sampling through hole.Three sampling through holes are equally spaced.Pass on axostylus axostyle, be positioned at inside level acquisition cylinder body and be provided with positive stop 24.Interior positive stop is near piston body.Pass on axostylus axostyle, be positioned at outside level acquisition cylinder body and be provided with outer positive stop 27.As shown in Figure 3, when interior positive stop is resisted against on the level acquisition cylinder body end face of dodging through hole place, each piston body is positioned at level acquisition cylinder interior, and level acquisition cylinder body between adjacent two-piston body has the sampling through hole described in respectively.As shown in Figure 2, when outer positive stop leans against on the level acquisition cylinder body end face of dodging through hole place, piston body adjacent with passing axostylus axostyle in each piston body is positioned at level acquisition cylinder body, and all the other piston bodies are positioned at the baking oven outside level acquisition cylinder body.
Level acquisition cylinder body and horizontally-guided cover are positioned at the relative both sides of baking oven, and level acquisition cylinder body and horizontally-guided overlap coaxial setting.The internal diameter gathering cylinder body is identical with the external diameter compensating cylinder.Compensate cylinder and be provided with connecting rod 5 between the piston body compensating cylinder.One end of this connecting rod is connected with the end face compensating cylinder, and the other end is connected with piston body end face.Connecting rod is coaxially arranged with compensation cylinder.Erecting frame is provided with the promotion cylinder for pushing piston body.Promotion cylinder is horizontally disposed with, and the piston rod promoting cylinder is connected with the passing axostylus axostyle be positioned at outside level acquisition cylinder body.
The concrete use procedure of medicinal powder heating quality measuring equipment of the present invention is as follows:
First, as shown in Figure 1, piston body is driven to move in baking oven by promoting cylinder, dodge on the collection cylinder body end face at through hole place until outer positive stop leans against, the piston body be now connected with passing axostylus axostyle in each piston body is positioned at and gathers cylinder body, and all the other piston bodies are positioned at the baking oven gathered outside cylinder body;
Medicinal powder to be measured is placed in pallet; Electronic balance is placed on immediately below support plate, and support plate is placed on the weighing platform at electronic balance top; Now pallet is placed on electronic balance by vertical support bar and support plate.
The second, baking oven heats, thus carrys out the change of on-line synchronous detection material heating quality by electronic balance.
In baking oven heating process, when needs gather gas in baking oven:
A, driving piston body to move in collection cylinder body by promoting cylinder, compensating cylinder simultaneously and moving in baking oven; Till interior positive stop is resisted against on the collection cylinder body end face of dodging through hole place, now each piston body is positioned at collection cylinder interior, as shown in Figure 3.
Due at piston body in collection cylinder body while movement, compensating cylinder will toward the interior movement of baking oven; Gather in the process of gas in baking oven at gas sampling assembly like this, by being moved in baking oven cavity, to gather cylinder body inner volume (this volume is the former piston body be placed in baking oven cavity, the volume sum of connecting link and the gas between adjacent two-piston body) identical with the volume moving to the compensation cylinder in baking oven cavity; Thus in gas collecting process, volume compensation device will carry out isopyknic compensation to oven ncavity simultaneously, thus avoid the air pressure of the oven ncavity above dividing plate to reduce, air pressure in baking oven is remained unchanged, like this when the upper and lower cavity connects of baking oven, can avoid forming air stream in baking oven, ensure the authentic and valid of measurement data.
3rd, collecting bag of the prior art (such as vacuum bag etc.) can be adopted to collect the gas sample gathered in gas sampling assembly, and concrete operations are as follows:
Gas in collecting bag is discharged, the seal plug in each sampling through hole is taken off, and will; The sack of collecting bag docks with corresponding sampling through hole;
Then, inflated in each pneumatophore from porting, main air guide channel and radial direction through hole by air pump, pneumatophore is expanded, thus the gas between adjacent two-piston body is discharged in collecting bag by through hole of sampling.
Claims (7)
1. a medicinal powder heating quality measuring equipment, is characterized in that, comprises baking oven (1), erecting frame (6), is arranged on the electronic weighing device (3) bottom baking oven, is arranged on the gas sampling assembly (2) on baking oven and volume compensation device (4);
Described volume compensation device comprises and being arranged on baking oven side and the horizontally-guided cover (41) be connected with oven ncavity, slidably be arranged on the compensation cylinder (42) in horizontally-guided cover, overlap between medial surface on described horizontally-guided cover medial surface, at compensation cylinder and horizontally-guided and be provided with the first O-ring seal;
Described gas sampling assembly comprises the level acquisition cylinder body (26) be arranged on erecting frame, coaxially be arranged on the passing axostylus axostyle (25) in level acquisition cylinder body and at least two piston bodies (21) be slidably arranged in level acquisition cylinder body, and be connected by connecting axostylus axostyle (22) between adjacent two-piston body, be also provided with pneumatophore (23) between adjacent two-piston body; One end of level acquisition cylinder body is connected with oven ncavity, the other end is provided with dodges through hole (28), one end of described passing axostylus axostyle is connected with near the piston body of dodging through hole, the other end is through dodging through hole, and be positioned at outside level acquisition cylinder body, pass axostylus axostyle to be provided with along passing the axially extended main air guide channel (210) of axostylus axostyle, and main air guide channel extends toward piston body direction, and through each connection axostylus axostyle; One end of this main air guide channel toward extension, and passing axostylus axostyle outside level acquisition cylinder body forms porting (212), and the other end is closed; Each connection axostylus axostyle lateral surface is respectively equipped with the radial direction through hole (211) be connected with main air guide channel, and the inner chamber of each pneumatophore is connected with corresponding radial direction through hole respectively; Described level acquisition cylinder body lateral surface is provided with at least one sampling through hole be communicated with level acquisition inner chamber of cylinder block, and is provided with the seal plug (29) that can take out in sampling through hole; On described passing axostylus axostyle, be positioned at inside level acquisition cylinder body and be provided with positive stop (24), when interior positive stop is resisted against on the level acquisition cylinder body end face of dodging through hole place, each piston body is positioned at level acquisition cylinder interior, and level acquisition cylinder body between adjacent two-piston body has the sampling through hole described in respectively;
Described level acquisition cylinder body and horizontally-guided cover are positioned at the relative both sides of baking oven, and level acquisition cylinder body and horizontally-guided overlap coaxial setting, connecting rod (5) is provided with between described compensation cylinder and the close piston body compensating cylinder, one end of this connecting rod is connected with the end face compensating cylinder, and the other end is connected with piston body end face; Described erecting frame is provided with the promotion cylinder for pushing piston body.
2. a kind of medicinal powder heating quality measuring equipment according to claim 1, is characterized in that, the internal diameter of described collection cylinder body is identical with the external diameter compensating cylinder.
3. a kind of medicinal powder heating quality measuring equipment according to claim 1, it is characterized in that, described pneumatophore comprises the Air sac cover be set on connecting link, and the two ends of Air sac cover are tightly connected with connecting link lateral surface respectively.
4. a kind of medicinal powder heating quality measuring equipment according to claim 1 or 2 or 3, described electronic weighing device comprises electronic balance (35), be arranged on the pallet (31) in baking oven, to be arranged on baking oven bottom surface and the bar through hole be positioned at immediately below pallet, be arranged on the vertical support bar (33) of support plate (32) immediately below bar through hole and connecting trays and support plate, vertical support bar is through bar through hole.
5. a kind of medicinal powder heating quality measuring equipment according to claim 1 or 2 or 3, it is characterized in that, on described passing axostylus axostyle, be positioned to gather outside cylinder body and be provided with outer positive stop (27), and when outer positive stop leans against on the collection cylinder body end face of dodging through hole place, piston body adjacent with passing axostylus axostyle in each piston body is positioned at and gathers cylinder body, and all the other piston bodies are positioned at the baking oven gathered outside cylinder body.
6. a kind of medicinal powder heating quality measuring equipment according to claim 1 or 2 or 3, it is characterized in that, be provided with thermopair (35) in described pallet, described baking oven bottom surface is provided with through wires hole, and being provided with seal rubber sleeve in through wires hole, the signal wire of described thermopair is through seal rubber sleeve.
7. a kind of medicinal powder heating quality measuring equipment according to claim 1 or 2 or 3, it is characterized in that, described baking oven is provided with the temperature sensor of the temperature for detecting oven ncavity.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510114981.7A CN104777277B (en) | 2015-03-17 | 2015-03-17 | A kind of medicated powder heating quality measures equipment |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510114981.7A CN104777277B (en) | 2015-03-17 | 2015-03-17 | A kind of medicated powder heating quality measures equipment |
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| Publication Number | Publication Date |
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| CN104777277A true CN104777277A (en) | 2015-07-15 |
| CN104777277B CN104777277B (en) | 2016-09-14 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201510114981.7A Expired - Fee Related CN104777277B (en) | 2015-03-17 | 2015-03-17 | A kind of medicated powder heating quality measures equipment |
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Citations (7)
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| US4266423A (en) * | 1979-10-01 | 1981-05-12 | Hobart Corporation | Use of acid as an analysis aid in salted meat samples |
| US5983711A (en) * | 1997-12-29 | 1999-11-16 | Arizona Instrument Corporation | Temperature controlled gravimetric moisture analyzer and method therefor |
| EP0965832A2 (en) * | 1998-06-12 | 1999-12-22 | Troxler Electronic Laboratories, Inc. | Method and apparatus for analyzing asphalt content |
| US20050048661A1 (en) * | 2003-08-25 | 2005-03-03 | Droit Jimmy L. | Methods and apparatus for analyzing materials |
| CN202599780U (en) * | 2012-04-13 | 2012-12-12 | 东华大学 | Industrial or city sewage sludge bound water form and content measuring device |
| CN103674767A (en) * | 2013-11-18 | 2014-03-26 | 西安近代化学研究所 | Device for measuring heating mass loss rate of explosive powder |
| CN204086064U (en) * | 2014-08-22 | 2015-01-07 | 中国农业科学院农产品加工研究所 | A kind of performance analysis device of material volatile matter |
-
2015
- 2015-03-17 CN CN201510114981.7A patent/CN104777277B/en not_active Expired - Fee Related
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4266423A (en) * | 1979-10-01 | 1981-05-12 | Hobart Corporation | Use of acid as an analysis aid in salted meat samples |
| US5983711A (en) * | 1997-12-29 | 1999-11-16 | Arizona Instrument Corporation | Temperature controlled gravimetric moisture analyzer and method therefor |
| EP0965832A2 (en) * | 1998-06-12 | 1999-12-22 | Troxler Electronic Laboratories, Inc. | Method and apparatus for analyzing asphalt content |
| US20050048661A1 (en) * | 2003-08-25 | 2005-03-03 | Droit Jimmy L. | Methods and apparatus for analyzing materials |
| CN202599780U (en) * | 2012-04-13 | 2012-12-12 | 东华大学 | Industrial or city sewage sludge bound water form and content measuring device |
| CN103674767A (en) * | 2013-11-18 | 2014-03-26 | 西安近代化学研究所 | Device for measuring heating mass loss rate of explosive powder |
| CN204086064U (en) * | 2014-08-22 | 2015-01-07 | 中国农业科学院农产品加工研究所 | A kind of performance analysis device of material volatile matter |
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