CN104745315A - Filter material back-flushing agent and preparation method thereof - Google Patents

Filter material back-flushing agent and preparation method thereof Download PDF

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Publication number
CN104745315A
CN104745315A CN201510066692.4A CN201510066692A CN104745315A CN 104745315 A CN104745315 A CN 104745315A CN 201510066692 A CN201510066692 A CN 201510066692A CN 104745315 A CN104745315 A CN 104745315A
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CN
China
Prior art keywords
ammonium chloride
hydrochloric acid
clear water
stirring
filter material
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Pending
Application number
CN201510066692.4A
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Chinese (zh)
Inventor
张峰
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Xi'an Hua Nuo Petro-Technology Development Corp Ltd
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Xi'an Hua Nuo Petro-Technology Development Corp Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Application filed by Xi'an Hua Nuo Petro-Technology Development Corp Ltd filed Critical Xi'an Hua Nuo Petro-Technology Development Corp Ltd
Priority to CN201510066692.4A priority Critical patent/CN104745315A/en
Publication of CN104745315A publication Critical patent/CN104745315A/en
Pending legal-status Critical Current

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Abstract

The invention provides a filter material back-flushing agent. The filter material back-flushing agent comprises the following components in parts by mass: 190-200 parts of clear water, 40-50 parts of hydrochloric acid, 10-20 parts of imidazoline, 25-35 parts of dodecyl dimethylbenzyl ammonium chloride, 10-20 parts of dodecyl trimethyl ammonium chloride, wherein the hydrochloric acid concentration is 8%-12%; the preparation method comprises the following steps: weighing the components in parst by mass, placing separately for later use; adding 70%-80% of the clear water in a mixer, stirring for 3-5 min; adding hydrochloric acid in the mixer, stirring for 12-18 min; adding imidazoline in the mixer and stirring for 12-18min; continuously adding dodecyl dimethylbenzyl ammonium chloride and dodecyl trimethyl ammonium chloride in the mixer, and adding the rest clear water, stirring for at least 20min, stopping stirring until the chemicals are uniformly mixed. Through the adoption of the filter material back-flushing agent, the oily matter and mechanical impurities on the surface of the filter material can be effectively removed; after the back-flushing agent permeates into the dirt, the dirt is loosened and falls off, and the bacteria under the dirt can be killed effectively to prevent the breeding of bacteria under the dirt, thereby prolonging the service life of the filter material; and the preparation method is simple and rapid; the production cost is low and the efficiency is high.

Description

A kind of filtrate recoil lotion and preparation method thereof
Technical field
The invention belongs to oilfield chemistry reagent preparing technical field, be specifically related to a kind of in disposing polluted water in oil the filtrate recoil lotion and preparation method thereof for Filter Back Washing.
Background technology
There are coarse filtration and essence filter two kinds of strainers in disposing polluted water in oil flow process, wherein coarse filtration mainly comprises the strainers such as quartz sand, nut-shell, fibrous nodules; Essence filter comprises PE millipore filter and fine filter.But strainer is in long operational process, owing to being subject to the pollution of sewage, filter effect is caused to be deteriorated, filter leaching material is even made to lose effect, filtrate after simultaneously being polluted can produce a large amount of bacteriums, sewage will be caused in sewage water filtration process to be subject to secondary pollution, injection water quality bacterium to be increased, finally pollutes stratum.
Therefore be necessary to develop a kind of filtrate recoil lotion, oils and the mechanical impurity of filter material surface can be removed, make dirty the loosening of dirt come off under realizing penetrating into dirt, effectively can kill the lower bacterium of dirt simultaneously, prevent growing, to extend the work-ing life of filtrate of the lower bacterium of dirt.
Summary of the invention
In order to solve above-mentioned prior art problem, the object of the present invention is to provide a kind of filtrate to recoil the preparation method of lotion, to recoil lotion with the filtrate preparing a kind of oils and mechanical impurity that effectively can remove filter material surface.
For achieving the above object, the technical solution used in the present invention is as follows:
A kind of filtrate recoil lotion, it is characterized in that, the component of being divided by following quality forms: clear water 190 ~ 200, hydrochloric acid 40 ~ 50, tetrahydroglyoxaline 10 ~ 20, dodecyl benzyl dimethyl ammonium chloride 25 ~ 35, Dodecyl trimethyl ammonium chloride 10 ~ 20.
Preferably, described concentration of hydrochloric acid is 8% ~ 12%.
Invention also provides the preparation method of this filtrate recoil lotion, it is characterized in that, comprise the steps:
Step one, divides by quality and takes each component, separated for subsequent use;
Step 2, add that clear water quality divides 70% ~ 80% in mixing tank, and start stirring, mixing speed is 100 ~ 150R/min, stirs 3 ~ 5min;
Step 3, adds hydrochloric acid in mixing tank, starts stirring, and mixing speed is 100 ~ 150R/min, stirs 12 ~ 18min;
Step 3, adds tetrahydroglyoxaline in mixing tank, starts stirring, and mixing speed is 100 ~ 150R/min, stirs 12 ~ 18min;
Step 4, add dodecyl benzyl dimethyl ammonium chloride and Dodecyl trimethyl ammonium chloride continuously in mixing tank, add the clear water that residual mass divides simultaneously, start and stir at least more than 20min, mixing speed is 100 ~ 150R/min, stirs until medicament mixes rear stopping.
Compared with prior art, the invention has the beneficial effects as follows:
1, the filtrate of this formula system recoil lotion is adopted effectively can to remove oils and the mechanical impurity of filter material surface, realization makes dirty the loosening of dirt come off under penetrating into dirt, effectively can kill the lower bacterium of dirt simultaneously, prevent growing, to extend the work-ing life of filtrate of the lower bacterium of dirt;
2, this preparation method is simple, quick, and production cost is low, efficiency is high.
Embodiment
In order to make technique means of the present invention, creation characteristic and reach object be easy to understand understand, set forth the present invention further below in conjunction with specific embodiment.
Embodiment 1:
The present embodiment provides a kind of filtrate recoil lotion, and its component of being divided by following quality forms: clear water 190, hydrochloric acid 40, tetrahydroglyoxaline 10, dodecyl benzyl dimethyl ammonium chloride 25, Dodecyl trimethyl ammonium chloride 10, and wherein concentration of hydrochloric acid is 8%.
The preparation method of this filtrate recoil lotion comprises the steps:
Step one, divides by quality and takes each component, separated for subsequent use;
Step 2, add that clear water quality divides 70% in mixing tank, and start stirring, mixing speed is 100R/min, stirs 3min;
Step 3, adds hydrochloric acid in mixing tank, starts stirring, and mixing speed is 100R/min, stirs 12min;
Step 3, adds tetrahydroglyoxaline in mixing tank, starts stirring, and mixing speed is 100R/min, stirs 12min;
Step 4, add dodecyl benzyl dimethyl ammonium chloride and Dodecyl trimethyl ammonium chloride continuously in mixing tank, add the clear water that residual mass divides simultaneously, start and stir at least more than 20min, mixing speed is 100R/min, stirs until medicament mixes rear stopping.
Embodiment 2
The present embodiment provides a kind of filtrate recoil lotion, and its component of being divided by following quality forms: clear water 195, hydrochloric acid 45, tetrahydroglyoxaline 15, dodecyl benzyl dimethyl ammonium chloride 30, Dodecyl trimethyl ammonium chloride 15, and wherein concentration of hydrochloric acid is 10%.
The preparation method of this filtrate recoil lotion comprises the steps:
Step one, divides by quality and takes each component, separated for subsequent use;
Step 2, add that clear water quality divides 77% in mixing tank, and start stirring, mixing speed is 130R/min, stirs 5min;
Step 3, adds hydrochloric acid in mixing tank, starts stirring, and mixing speed is 130R/min, stirs 15min;
Step 3, adds tetrahydroglyoxaline in mixing tank, starts stirring, and mixing speed is 130R/min, stirs 15min;
Step 4, add dodecyl benzyl dimethyl ammonium chloride and Dodecyl trimethyl ammonium chloride continuously in mixing tank, add the clear water that residual mass divides simultaneously, start and stir at least more than 20min, mixing speed is 130R/min, stirs until medicament mixes rear stopping.
Embodiment 3
The present embodiment provides a kind of filtrate recoil lotion, and its component of being divided by following quality forms: clear water 200, hydrochloric acid 50, tetrahydroglyoxaline 50, dodecyl benzyl dimethyl ammonium chloride 35, Dodecyl trimethyl ammonium chloride 20, and wherein concentration of hydrochloric acid is 12%.
The preparation method of this filtrate recoil lotion comprises the steps:
Step one, divides by quality and takes each component, separated for subsequent use;
Step 2, add that clear water quality divides 80% in mixing tank, and start stirring, mixing speed is 150R/min, stirs 4min;
Step 3, adds hydrochloric acid in mixing tank, starts stirring, and mixing speed is 150R/min, stirs 13min;
Step 3, adds tetrahydroglyoxaline in mixing tank, starts stirring, and mixing speed is 150R/min, stirs 13min;
Step 4, add dodecyl benzyl dimethyl ammonium chloride and Dodecyl trimethyl ammonium chloride continuously in mixing tank, add the clear water that residual mass divides simultaneously, start and stir at least more than 20min, mixing speed is 150R/min, stirs until medicament mixes rear stopping.
More than show and describe ultimate principle of the present invention, principal character and advantage; the technician of the industry should understand; the present invention is not restricted to the described embodiments; description in above-described embodiment and specification sheets is only and the present invention and principle thereof is described; the present invention also has various changes and modifications without departing from the spirit and scope of the present invention, and the improvement of these changes all falls in the claimed scope of the invention.Application claims protection domain is defined by appending claims and equivalent thereof.

Claims (5)

1. a filtrate recoil lotion, it is characterized in that, the component of being divided by following quality forms: clear water 190 ~ 200, hydrochloric acid 40 ~ 50, tetrahydroglyoxaline 10 ~ 20, dodecyl benzyl dimethyl ammonium chloride 25 ~ 35, Dodecyl trimethyl ammonium chloride 10 ~ 20.
2. a kind of filtrate recoil lotion according to claim 1, it is characterized in that, the component of being divided by following quality forms: clear water 195, hydrochloric acid 45, tetrahydroglyoxaline 15, dodecyl benzyl dimethyl ammonium chloride 30, Dodecyl trimethyl ammonium chloride 15.
3. a kind of filtrate recoil lotion according to claim 1, it is characterized in that, described concentration of hydrochloric acid is 8% ~ 12%.
4. a kind of filtrate recoil lotion according to claim 3, it is characterized in that, described concentration of hydrochloric acid is 10%.
5. a preparation method for filtrate recoil lotion, is characterized in that, comprise the steps:
Step one, divides by quality and takes each component, separated for subsequent use;
Step 2, add that clear water quality divides 70% ~ 80% in mixing tank, and start stirring, mixing speed is 100 ~ 150R/min, stirs 3 ~ 5min;
Step 3, adds hydrochloric acid in mixing tank, starts stirring, and mixing speed is 100 ~ 150R/min, stirs 12 ~ 18min;
Step 3, adds tetrahydroglyoxaline in mixing tank, starts stirring, and mixing speed is 100 ~ 150R/min, stirs 12 ~ 18min;
Step 4, add dodecyl benzyl dimethyl ammonium chloride and Dodecyl trimethyl ammonium chloride continuously in mixing tank, add the clear water that residual mass divides simultaneously, start and stir at least more than 20min, mixing speed is 100 ~ 150R/min, stirs until medicament mixes rear stopping.
CN201510066692.4A 2015-02-09 2015-02-09 Filter material back-flushing agent and preparation method thereof Pending CN104745315A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510066692.4A CN104745315A (en) 2015-02-09 2015-02-09 Filter material back-flushing agent and preparation method thereof

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Application Number Priority Date Filing Date Title
CN201510066692.4A CN104745315A (en) 2015-02-09 2015-02-09 Filter material back-flushing agent and preparation method thereof

Publications (1)

Publication Number Publication Date
CN104745315A true CN104745315A (en) 2015-07-01

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6288263B1 (en) * 1999-06-16 2001-09-11 The Dow Chemical Company Intermediates for the preparation of N-[2-(carboxymethoxy)ethyl]-N-(carboxymethyl)glycine
CN101328451A (en) * 2008-07-31 2008-12-24 中国石油天然气股份有限公司 Sewage filter cleaning agent and preparation thereof
CN103820232A (en) * 2014-01-22 2014-05-28 天津清正然化工科技有限公司 Filtering material cleaning agent for oilfield sewage filtering system

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6288263B1 (en) * 1999-06-16 2001-09-11 The Dow Chemical Company Intermediates for the preparation of N-[2-(carboxymethoxy)ethyl]-N-(carboxymethyl)glycine
CN101328451A (en) * 2008-07-31 2008-12-24 中国石油天然气股份有限公司 Sewage filter cleaning agent and preparation thereof
CN103820232A (en) * 2014-01-22 2014-05-28 天津清正然化工科技有限公司 Filtering material cleaning agent for oilfield sewage filtering system

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