CN104744836A - Formula and process of butyl rubber film-covered gasket for detection - Google Patents

Formula and process of butyl rubber film-covered gasket for detection Download PDF

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Publication number
CN104744836A
CN104744836A CN201510096768.8A CN201510096768A CN104744836A CN 104744836 A CN104744836 A CN 104744836A CN 201510096768 A CN201510096768 A CN 201510096768A CN 104744836 A CN104744836 A CN 104744836A
Authority
CN
China
Prior art keywords
film
formula
parts
isoprene
gasket
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201510096768.8A
Other languages
Chinese (zh)
Inventor
田恒生
马正平
黄家萍
王荣祥
许冰
陶良锦
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
ANHUI HUAFENG PHARMACEUTICAL RUBBER Co Ltd
Original Assignee
ANHUI HUAFENG PHARMACEUTICAL RUBBER Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by ANHUI HUAFENG PHARMACEUTICAL RUBBER Co Ltd filed Critical ANHUI HUAFENG PHARMACEUTICAL RUBBER Co Ltd
Priority to CN201510096768.8A priority Critical patent/CN104744836A/en
Publication of CN104744836A publication Critical patent/CN104744836A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/02Elements
    • C08K3/04Carbon
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/02Elements
    • C08K3/06Sulfur
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/18Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/20Oxides; Hydroxides
    • C08K3/22Oxides; Hydroxides of metals
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/34Silicon-containing compounds
    • C08K3/346Clay
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/18Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/20Oxides; Hydroxides
    • C08K3/22Oxides; Hydroxides of metals
    • C08K2003/2237Oxides; Hydroxides of metals of titanium
    • C08K2003/2241Titanium dioxide

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

The invention discloses a formula and a process of a butyl rubber film-covered gasket for detection. The butyl rubber film-covered gasket is prepared from the following components in parts by weight: 100 parts of brominated butyl rubber, 85-95 parts of kaoline, 0.1 part of carbon black, 3 parts of titanium dioxide, 5-6 parts of PH value regulator and 0.1-0.3 part of sulfur. The process comprises the following production steps: step 1, dosing; step 2, rubber mixing; step 3, pre-molding; step 4, primary vulcanization; step 5, secondary vulcanization; step 6, edge removal; step 7, cleaning. On the basis of the traditional technique, the formula and the process of the rubber gasket are improved, and the surface of the rubber gasket is covered with a layer of inert film material to prevent the chemical reaction between the gasket and drugs, and therefore, the stability of a standard substance for detection is enhanced.

Description

A kind of formula and technique detecting use isoprene-isobutylene rubber overlay film pad
Technical field
The present invention relates to a kind of formula and technique of rubber sheet gasket, particularly relate to a kind of formula and the technique that detect use isoprene-isobutylene rubber overlay film pad.
Background technology
Detection isoprene-isobutylene rubber pad is formed by design for rubber formulation, directly contacts with testing standard product.It has unstable and the formula constituent complicacy of conventional polymer material, therefore, can by form and medicine generation chemical reactions such as absorption, absorption, infiltration, migrations, the result of these chemical reactions directly affects the stability of detection standard substance.Therefore, those skilled in the art needs a kind of new technical scheme badly and solves this problem.
Summary of the invention
Invent problem to be solved to be: provide a kind of and detect formula with isoprene-isobutylene rubber overlay film pad and technique, it has and prevents pad and medicine generation chemical reaction, the feature of the stability of enhancing detection standard substance.
Technical solution problem of the present invention adopts following technical scheme:
Detect the formula with isoprene-isobutylene rubber overlay film pad, be made up of by weight following component: brominated butyl rubber 100 parts, kaolin 85-95 part, carbon black 0.1 part, titanium dioxide 3 parts, pH value conditioning agent 5-6 part, sulphur 0.1-0.3 part.
Preferably, described pH value conditioning agent is activated magnesia.
Detect the technique with isoprene-isobutylene rubber overlay film pad, comprise following production stage:
Step one, by formula carry out various material preparation and put into the barrel of specifying, i.e. blending process;
Step 2, evenly mixing by material various in barrel, obtain sizing material, i.e. mixing process;
Step 3, as requested sizing material is made the film being convenient to sulfuration specified dimension weight, i.e. preform process;
Step 4, the film of the specified dimension weight made is put into mould do a sulfuration, i.e. a sulfidation;
After step 5, a sulfuration die sinking, film does not take out, and is directly placed on by mould material on film and carries out post cure, i.e. secondary sulfurizing course;
Step 6, through die-cut formation finished product, namely except crack approach;
Step 7, employing automatically cleaning clean rubber cushion, i.e. cleaning process;
Preferably, described mould material is the ETFE film of thickness 4mil.
The invention has the beneficial effects as follows: the present invention is on the basis of conventional art, improve the composition and engineering of rubber sheet gasket, and cover one deck inert coating material on the surface of rubber sheet gasket, prevent pad and medicine generation chemical reaction, strengthen the stability of detection standard substance.
Embodiment
Below in conjunction with specific embodiment, the present invention is described in further details.
Detect the formula with isoprene-isobutylene rubber overlay film pad, be made up of by weight following component: brominated butyl rubber 100 parts, kaolin 85-95 part, carbon black 0.1 part, titanium dioxide 3 parts, pH value conditioning agent 5-6 part, sulphur 0.1-0.3 part.
Embodiment 1:
Brominated butyl rubber 100 parts, kaolin 95 parts, carbon black 0.1 part, titanium dioxide 3 parts, pH value conditioning agent 6 parts, 0.3 part, sulphur.
Detect the technique with isoprene-isobutylene rubber overlay film pad, comprise following production stage:
Step one, by formula carry out various material preparation and put into the barrel of specifying, i.e. blending process;
Step 2, evenly mixing by material various in barrel, obtain sizing material, i.e. mixing process;
Step 3, as requested sizing material is made the film being convenient to sulfuration specified dimension weight, i.e. preform process;
Step 4, the film of the specified dimension weight made is put into mould do a sulfuration, i.e. a sulfidation;
After step 5, a sulfuration die sinking, film does not take out, and is directly placed on by mould material on film and carries out post cure, i.e. secondary sulfurizing course;
Step 6, through die-cut formation finished product, namely except crack approach;
Step 7, employing automatically cleaning clean rubber cushion, i.e. cleaning process;
As preferred embodiment, described mould material is the ETFE film of thickness 4mil.
The above; be only the present invention's preferably embodiment; but protection scope of the present invention is not limited thereto; anyly be familiar with those skilled in the art in the technical scope that the present invention discloses; be equal to according to technical scheme of the present invention and inventive concept thereof and replace or change, all should be encompassed within protection scope of the present invention.

Claims (4)

1. detect the formula with isoprene-isobutylene rubber overlay film pad, it is characterized in that, be made up of by weight following component: brominated butyl rubber 100 parts, kaolin 85-95 part, carbon black 0.1 part, titanium dioxide 3 parts, pH value conditioning agent 5-6 part, sulphur 0.1-0.3 part.
2. a kind of formula detected with isoprene-isobutylene rubber overlay film pad according to claim 1, it is characterized in that, described pH value conditioning agent is activated magnesia.
3. detect the technique with isoprene-isobutylene rubber overlay film pad, it is characterized in that, comprise following production stage:
Step one, by formula carry out various material preparation and put into the barrel of specifying, i.e. blending process;
Step 2, evenly mixing by material various in barrel, obtain sizing material, i.e. mixing process;
Step 3, as requested sizing material is made the film being convenient to sulfuration specified dimension weight, i.e. preform process;
Step 4, the film of the specified dimension weight made is put into mould do a sulfuration, i.e. a sulfidation;
After step 5, a sulfuration die sinking, film does not take out, and is directly placed on by mould material on film and carries out post cure, i.e. secondary sulfurizing course;
Step 6, through die-cut formation finished product, namely except crack approach;
Step 7, employing automatically cleaning clean rubber cushion, i.e. cleaning process.
4. a kind of technique detected with isoprene-isobutylene rubber overlay film pad according to claim 3, it is characterized in that, described mould material is the ETFE film of thickness 4mil.
CN201510096768.8A 2015-03-04 2015-03-04 Formula and process of butyl rubber film-covered gasket for detection Pending CN104744836A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510096768.8A CN104744836A (en) 2015-03-04 2015-03-04 Formula and process of butyl rubber film-covered gasket for detection

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510096768.8A CN104744836A (en) 2015-03-04 2015-03-04 Formula and process of butyl rubber film-covered gasket for detection

Publications (1)

Publication Number Publication Date
CN104744836A true CN104744836A (en) 2015-07-01

Family

ID=53585139

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201510096768.8A Pending CN104744836A (en) 2015-03-04 2015-03-04 Formula and process of butyl rubber film-covered gasket for detection

Country Status (1)

Country Link
CN (1) CN104744836A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107163311A (en) * 2017-06-27 2017-09-15 浙江欧尔赛斯科技有限公司 Concave surface natural rubber overlay film pad and its production technology
CN107351489A (en) * 2017-06-27 2017-11-17 浙江欧尔赛斯科技有限公司 The laminating pad of natural rubber, butyl rubber, membrane material and its production technology

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101427981A (en) * 2007-11-06 2009-05-13 江苏博生橡塑有限公司 Chlorinated butyl rubber bung for injection and method of producing the same
CN103146086A (en) * 2013-03-05 2013-06-12 江阴市鸿萌橡塑制品有限公司 Butyl rubber stopper for blood collection tube

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101427981A (en) * 2007-11-06 2009-05-13 江苏博生橡塑有限公司 Chlorinated butyl rubber bung for injection and method of producing the same
CN103146086A (en) * 2013-03-05 2013-06-12 江阴市鸿萌橡塑制品有限公司 Butyl rubber stopper for blood collection tube

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107163311A (en) * 2017-06-27 2017-09-15 浙江欧尔赛斯科技有限公司 Concave surface natural rubber overlay film pad and its production technology
CN107351489A (en) * 2017-06-27 2017-11-17 浙江欧尔赛斯科技有限公司 The laminating pad of natural rubber, butyl rubber, membrane material and its production technology
CN107163311B (en) * 2017-06-27 2019-05-28 浙江欧尔赛斯科技有限公司 Concave surface natural rubber overlay film gasket and its production technology
CN107351489B (en) * 2017-06-27 2019-07-26 浙江欧尔赛斯科技有限公司 The laminating gasket of natural rubber, butyl rubber, membrane material and its production technology

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Application publication date: 20150701