CN104724936A - Decorative glass making technology - Google Patents

Decorative glass making technology Download PDF

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Publication number
CN104724936A
CN104724936A CN201310715197.2A CN201310715197A CN104724936A CN 104724936 A CN104724936 A CN 104724936A CN 201310715197 A CN201310715197 A CN 201310715197A CN 104724936 A CN104724936 A CN 104724936A
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CN
China
Prior art keywords
sodium
grams
glass
ammonium
hydrogen fluoride
Prior art date
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Pending
Application number
CN201310715197.2A
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Chinese (zh)
Inventor
黄淼
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Individual
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Individual
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Priority to CN201310715197.2A priority Critical patent/CN104724936A/en
Publication of CN104724936A publication Critical patent/CN104724936A/en
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Classifications

    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C15/00Surface treatment of glass, not in the form of fibres or filaments, by etching

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Cosmetics (AREA)
  • Detergent Compositions (AREA)

Abstract

The invention relates to the field of frosted glass manufacture and especially relates to a decorative glass making technology. The decorative glass making technology comprises the following steps of crushing ammonium fluoride, ammonium hydrogen fluoride, magnesium hydrogen fluoride, aluminum hydrogen fluoride, oxalic acid, sodium acetate, sodium silicate, ammonium fluoroborate, sodium fluoroborate, Al2O3 and SiO2, sodium dodecyl sulfate, cellulose MCC, sodium hexametaphosphate and sodium polyacrylate according to a certain weight ratio, carrying out stirring to obtain a uniform mixture, carrying out an intense agitation reaction process on the mixture to obtain paste with appropriate denseness, continuously feeding frosting paste through a sunned screen printing plate of 100 meshes by 75<o> of a resin adhesive plate and to plane glass, after 3min, carrying out drip washing on the surface of the glass by water and carrying out airing to obtain frosted accidented 3D patterns of the glass.

Description

A kind of manufacture craft of ambetti
Technical field
The present invention relates to the making of glass frosting, refer in particular to a kind of manufacture craft of ambetti.
Background technology
Current glass solid pattern processing technology power consumption is large, and technical difficulty is large, and the pattern line of machine carve is stiff, not nature.
Summary of the invention
The object of the invention is to overcome the deficiencies in the prior art, a kind of manufacture craft of ambetti be provided:
For achieving the above object, technical formula production craft step provided by the invention is as follows: technical formula production craft step provided by the invention is as follows: a, get ammonium fluoride, ammonium bifluoride, hydrogen fluoride magnesium, hydrogen fluoride aluminium main raw material, then adds a small amount of ionic strength adjustor (oxalic acid, sodium-acetate, water glass, ammonium borofluoride and Sodium tetrafluoroborate) and viscosity-controlling agent (Al 2o 3and SiO 2), tensio-active agent (sodium laurylsulfonate, Mierocrystalline cellulose MCC, Sodium hexametaphosphate 99 % and poly-Sodium Propionate) is for subsequent use; B, get institute standby material ammonium fluoride 16%, ammonium bifluoride 16%, hydrogen fluoride magnesium 13% by weight percentage, hydrogen fluoride aluminium 13% is main raw material, then adds a small amount of ionic strength adjustor (oxalic acid 3%, sodium-acetate 2%, water glass 2%, ammonium borofluoride 2% and Sodium tetrafluoroborate 2%) and viscosity-controlling agent (Al 2o 314% and SiO 214%), tensio-active agent (sodium laurylsulfonate 1%, Mierocrystalline cellulose MCC1%, Sodium hexametaphosphate 99 0.5% and poly-Sodium Propionate 0.5%); C, get b crushing material, stir, dry; D, get c gained mixture and to be placed in Stirring still sealing stirring 25 minutes; The frosting powder be stirred and technical hydrochloric acid are carried out hybrid reaction by 1: 1 and obtains frosted liquid, the time of hybrid reaction is 50 hours, and frosted liquid 10 1 100 order conventional screen or nylon net filter are obtained even emulsus frosted liquid; Its weight proportion following (in 100 grams): emulsus frosted liquid 35 grams, 6 grams, the acetone of 99 %, polyacrylic resin 5 grams, white sugar 7 grams, barium carbonate 45 grams, nonpolar 2 grams, alicyclic organic compounds acetic acid third fat; E, by ripe for the reaction of the gained d mixture strong stirring paste suitable to denseness, f, with 75 0the poly-money resin offset plate continuous net of crossing of silk-screen plate that e gains frosting cream has been shone in 10O object on flat glass, after 3 minutes, use water wash clean glass surface, namely airing obtains glass frosting stereo concave-convex pattern.
Positive effect of the present invention is: technique is simple, processes, does not have dust pollution, do not have waste water,waste gas and industrial residue to discharge under normal temperature.
Embodiment
Below invention is further elaborated, technical formula production craft step provided by the invention is as follows: a, get ammonium fluoride, ammonium bifluoride, hydrogen fluoride magnesium, hydrogen fluoride aluminium main raw material, then adds a small amount of ionic strength adjustor (oxalic acid, sodium-acetate, water glass, ammonium borofluoride and Sodium tetrafluoroborate) and viscosity-controlling agent (Al 2o 3and SiO 2), tensio-active agent (sodium laurylsulfonate, Mierocrystalline cellulose MCC, Sodium hexametaphosphate 99 % and poly-Sodium Propionate) is for subsequent use; B, get institute standby material ammonium fluoride 16%, ammonium bifluoride 16%, hydrogen fluoride magnesium 13% by weight percentage, hydrogen fluoride aluminium 13% is main raw material, then adds a small amount of ionic strength adjustor (oxalic acid 3%, sodium-acetate 2%, water glass 2%, ammonium borofluoride 2% and Sodium tetrafluoroborate 2%) and viscosity-controlling agent (Al 2o 314% and SiO 214%), tensio-active agent (sodium laurylsulfonate 1%, Mierocrystalline cellulose MCC1%, Sodium hexametaphosphate 99 0.5% and poly-Sodium Propionate 0.5%); C, get b crushing material, stir, dry; D, get c gained mixture and to be placed in Stirring still sealing stirring 25 minutes; The frosting powder be stirred and technical hydrochloric acid are carried out hybrid reaction by 1: 1 and obtains frosted liquid, the time of hybrid reaction is 50 hours, and frosted liquid 10 1 100 order conventional screen or nylon net filter are obtained even emulsus frosted liquid; Its weight proportion following (in 100 grams): emulsus frosted liquid 35 grams, 6 grams, the acetone of 99 %, polyacrylic resin 5 grams, white sugar 7 grams, barium carbonate 45 grams, nonpolar 2 grams, alicyclic organic compounds acetic acid third fat; E, by ripe for the reaction of the gained d mixture strong stirring paste suitable to denseness, f, with 75 0the poly-money resin offset plate continuous net of crossing of silk-screen plate that e gains frosting cream has been shone in 10O object on flat glass, after 3 minutes, use water wash clean glass surface, namely airing obtains glass frosting stereo concave-convex pattern.

Claims (4)

1. the technique of an ambetti makes, it is characterized in that: technical formula production craft step provided by the invention is as follows: a, get ammonium fluoride, ammonium bifluoride, hydrogen fluoride magnesium, hydrogen fluoride aluminium main raw material, then add a small amount of ionic strength adjustor (oxalic acid, sodium-acetate, water glass, ammonium borofluoride and Sodium tetrafluoroborate) and viscosity-controlling agent (Al 2o 3and SiO 2), tensio-active agent (sodium laurylsulfonate, Mierocrystalline cellulose MCC, Sodium hexametaphosphate 99 % and poly-Sodium Propionate) is for subsequent use.
2. according to right 1, it is characterized in that: b, get institute standby material ammonium fluoride 16%, ammonium bifluoride 16%, hydrogen fluoride magnesium 13% by weight percentage, hydrogen fluoride aluminium 13% is main raw material, then adds a small amount of ionic strength adjustor (oxalic acid 3%, sodium-acetate 2%, water glass 2%, ammonium borofluoride 2% and Sodium tetrafluoroborate 2%) and viscosity-controlling agent (Al 2o 314% and SiO 214%), tensio-active agent (sodium laurylsulfonate 1%, Mierocrystalline cellulose MCC1%, Sodium hexametaphosphate 99 0.5% and poly-Sodium Propionate 0.5%).
3., according to right 1, it is characterized in that: c, get b crushing material, stir, dry; D, get c gained mixture and to be placed in Stirring still sealing stirring 25 minutes; The frosting powder be stirred and technical hydrochloric acid are carried out hybrid reaction by 1: 1 and obtains frosted liquid, the time of hybrid reaction is 50 hours, and frosted liquid 10 1 100 order conventional screen or nylon net filter are obtained even emulsus frosted liquid; Its weight proportion following (in 100 grams): emulsus frosted liquid 35 grams, 6 grams, the acetone of 99 %, polyacrylic resin 5 grams, white sugar 7 grams, barium carbonate 45 grams, nonpolar 2 grams, alicyclic organic compounds acetic acid third fat; E, by ripe for the reaction of the gained d mixture strong stirring paste suitable to denseness.
4. according to right 1, it is characterized in that: f, with 75 0the poly-money resin offset plate continuous net of crossing of silk-screen plate that e gains frosting cream has been shone in 10O object on flat glass, after 3 minute second, use water wash clean glass surface, namely airing obtains glass frosting stereo concave-convex pattern.
CN201310715197.2A 2013-12-23 2013-12-23 Decorative glass making technology Pending CN104724936A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201310715197.2A CN104724936A (en) 2013-12-23 2013-12-23 Decorative glass making technology

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201310715197.2A CN104724936A (en) 2013-12-23 2013-12-23 Decorative glass making technology

Publications (1)

Publication Number Publication Date
CN104724936A true CN104724936A (en) 2015-06-24

Family

ID=53449430

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201310715197.2A Pending CN104724936A (en) 2013-12-23 2013-12-23 Decorative glass making technology

Country Status (1)

Country Link
CN (1) CN104724936A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111233339A (en) * 2020-03-21 2020-06-05 郑州恒昊光学科技有限公司 Glass etching solution, high-alumina-silica glass etching method and high-alumina-silica glass with texture on surface
CN113501670A (en) * 2021-07-20 2021-10-15 海南海控特玻科技有限公司 Chemical strengthening and film-covering strengthening process for ultrathin high-aluminum glass

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111233339A (en) * 2020-03-21 2020-06-05 郑州恒昊光学科技有限公司 Glass etching solution, high-alumina-silica glass etching method and high-alumina-silica glass with texture on surface
CN111233339B (en) * 2020-03-21 2022-02-18 郑州恒昊光学科技有限公司 Glass etching solution, high-alumina-silica glass etching method and high-alumina-silica glass with texture on surface
CN113501670A (en) * 2021-07-20 2021-10-15 海南海控特玻科技有限公司 Chemical strengthening and film-covering strengthening process for ultrathin high-aluminum glass
CN113501670B (en) * 2021-07-20 2022-05-31 海南海控特玻科技有限公司 Chemical strengthening and film-covering strengthening process for ultrathin high-aluminum glass

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Application publication date: 20150624

WD01 Invention patent application deemed withdrawn after publication