CN104710650B - The preparation method of environmental protective type chemical mixed aid - Google Patents

The preparation method of environmental protective type chemical mixed aid Download PDF

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Publication number
CN104710650B
CN104710650B CN201510108769.XA CN201510108769A CN104710650B CN 104710650 B CN104710650 B CN 104710650B CN 201510108769 A CN201510108769 A CN 201510108769A CN 104710650 B CN104710650 B CN 104710650B
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grams
auxiliary agent
powder
mixed aid
stearic acid
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CN201510108769.XA
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CN104710650A (en
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张维宽
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Ruian Haobang New Material Technology Co.,Ltd.
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Rui'an City Hao Bang Rubber-Plastics Material Co Ltd
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  • Compositions Of Macromolecular Compounds (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)
  • Manufacture Of Porous Articles, And Recovery And Treatment Of Waste Products (AREA)
  • Processing And Handling Of Plastics And Other Materials For Molding In General (AREA)

Abstract

The preparation method of environmental protective type chemical mixed aid disclosed by the invention, it is characterised in that comprise the following steps:Auxiliary agent powder is subjected to fine crushing, powder particle size is controlled in 2,000 5000 mesh;The auxiliary agent powder of fine crushing and appropriate stearic acid powder are added to homogenizer together, mixer rotating speed is in more than 1000r/min, until all powders are sufficiently mixed and into sticky matter;Sticky matter cooled and solidified is into solid;Solid is put into comminutor and is granulated, mixed aid particle is formed after granulation;

Description

The preparation method of environmental protective type chemical mixed aid
Technical field
The present invention relates to a kind of preparation method of environmental protective type chemical mixed aid.
Background technology
, it is necessary to largely use auxiliary chemicals in plastics chemical industry, the species of auxiliary chemicals is various, a kind of auxiliary chemicals A kind of usually purposes, and often different plastic rubber products need to add a variety of auxiliary chemicals, a variety of auxiliary chemicals need to mix Use, the general character of auxiliary chemicals is all mostly powder, and the problem of thus bringing is a lot, wherein most importantly environmental protection is asked Topic.During the use of auxiliary chemicals, it is necessary first to be added to by required counterweight one or more different auxiliary agent powders close In mill and aniseed(Refer to rubber raw materials)Mix and be kneaded, using inconvenience, labor strength is big, this mistake Have substantial amounts of dust in journey to produce, it is estimated that more than the 20% of auxiliary agent total amount can be accounted for by becoming the auxiliary agent powder of dust escape, make to help Agent materials are inaccurate, and the addition of auxiliary agent often has a significant impact to the quality of plastic, rubber product, although the big portion of dust The dust collection equipment that branch is matched somebody with somebody by workshop, which is taken away, to be caused to waste, but also fraction can seriously pollute environment, and environmental protection is difficult to reach Mark, worker even if produce its health with mouth mask also can be adversely effected.Moreover, powder auxiliary agent is in transport, handling Dust can be all produced Deng during, influences environment, in addition, the auxiliary agent of various a multitude of names is stacked upon, space is big, Stacking pressure cost;Further, auxiliary agent powder is difficult to be well mixed with aniseed in aniseed, poor dispersion, then can easily make production Plastic rubber product physical property is unstable, quality defect.
The content of the invention
The present invention is adopted the following technical scheme that to realize:
The preparation method of environmental protective type chemical mixed aid, it is characterised in that comprise the following steps:1. by all kinds of auxiliary powders Expect to carry out fine crushing respectively, the powder particle size after fine crushing is controlled in 2000-5000 mesh;2. by the institute of above-mentioned fine crushing There are kind of auxiliary agent powder and appropriate stearic acid powder to be added to homogenizer together, control the rotating speed of mixer in 1000r/min More than, until all powders are sufficiently mixed and into sticky matters;3. sticky matter cooled and solidified is into solid;4. above-mentioned solid is put It is granulated into comminutor, mixed aid particle is formed after granulation;5. mixed aid particle is put on screen cloth and carries out sub-sieve, Particle diameter 2-6mm is qualified finished product, and prepared by mixed aid completes.
In above-mentioned technical proposal, fine crushing is carried out to auxiliary agent powder first, it is therefore an objective to meet different auxiliary agent powders rear More preferable in continuous process to complete to bond, then the high-speed stirred together with appropriate stearic acid powder, various during high-speed stirred Powder is mixed, simultaneously as friction produces temperature, in the range of temperature reaches 50-80 degree, stearic acid powder is fused into For liquid oily, then all powders are sufficiently mixed and into sticky matters, are then cooled off, are granulated and screen, granular mixed Close auxiliary agent and prepare completion.The advantages of granular mixed aid, has:1. environmental protection, use and transport, cargo handling process does not produce powder Dirt;It 2. because not producing dust, will not cause to waste in use, while can ensure that materials are accurate, ensure addition The quality of the plastic, rubber product of above-mentioned auxiliary agent;3. the correlation of different purposes can be helped according to needed for different plastic rubber products Agent powder is mixed in advance, and it is accurate using convenience, materials to make first, while is saved cost, saved parking space;It is 4. because mixed Conjunction auxiliary agent is in granular form to be added to mix with aniseed in banbury and is kneaded, so just having at first very well Dispersiveness, be easily well mixed with aniseed, so as to be easily guaranteed that the stable physical property of the plastic rubber product of production, quality It is good.In summary, using the mixed aid prepared by the present invention, its innovate be related different auxiliary agents be pre-mixed and in Granular, its maximum feature is environmental protection, be provided simultaneously with using it is convenient, reduce waste, save cost, to save space, materials accurate etc. Plurality of advantages, and can make that the physical property of the plastic rubber product of production is more stable, better quality.
According to the preparation method of above-mentioned mixed aid, the preparation of rubber mix auxiliary agent can be carried out, is mixed preparing rubber When closing auxiliary agent, the selection species and weight proportion of auxiliary agent powder and stearic acid powder are:2500 grams of H foaming agents, 2500 grams of urea Fat, 900 grams of zinc oxide and 900 grams of stearic acid.
The preparation of plastic foamed mixed aid can also be carried out, when preparing plastic foamed mixed aid, auxiliary agent powder and The selection species and weight proportion of stearic acid powder be:2500 grams of AC foaming agents, 1000 grams of zinc oxide, 500 grams of zinc carbonates and 500 Gram stearic acid.
The preparation of PVC foam mixed aid can also be carried out, when preparing PVC foam mixed aid, auxiliary agent powder and hard The selection species and weight proportion of resin acid powder be:5000 grams of AC foaming agents, 3000 grams of zinc, barium, one kind in lead heat stabilizer, 500 grams of stearic acid.
The preparation of black masterbatch mixed aid can also be carried out, when preparing black masterbatch mixed aid, auxiliary agent powder and tristearin The selection species and weight proportion of sour powder be:3000 grams of not leaded carbon blacks and 100 grams of stearic acid.
Embodiment
Embodiment:The preparation method of the environmental protective type chemical mixed aid of the present invention, comprises the following steps:1. all kinds are helped Agent powder carries out fine crushing respectively, and the powder particle size after fine crushing is controlled in 2000-5000 mesh;2. by above-mentioned fine crushing All kinds of auxiliary agent powders and appropriate stearic acid powder be added to homogenizer together, control the rotating speed of mixer in 1000r/ More than min, until all powders are sufficiently mixed and into sticky matter;3. sticky matter cooled and solidified is into solid;4. by above-mentioned solid-state Thing is put into comminutor and is granulated, and mixed aid particle is formed after granulation;Carried out 5. mixed aid particle is put on screen cloth Sub-sieve, particle diameter 2-6mm are qualified finished product, and prepared by mixed aid completes.
When preparing rubber mix auxiliary agent, the selection species and weight proportion of auxiliary agent powder and stearic acid powder are:2500 Gram H foaming agents, 2500 grams of urea fat, 900 grams of zinc oxide and 900 grams of stearic acid.The weight error of auxiliary agent powder is controlled in percentage Ten within.
When preparing plastic foamed mixed aid, the selection species and weight proportion of auxiliary agent powder and stearic acid powder are: 2500 grams of AC foaming agents, 1000 grams of zinc oxide, 500 grams of zinc carbonates and 500 grams of stearic acid.The weight error control of auxiliary agent powder exists Within 10.
When preparing PVC foam mixed aid, the selection species and weight proportion of auxiliary agent powder and stearic acid powder are: 5000 grams of AC foaming agents, 3000 grams of zinc, barium, one kind in lead heat stabilizer, 500 grams of stearic acid.The weight error of auxiliary agent powder Control is within 10.
When preparing black masterbatch mixed aid, the selection species and weight proportion of auxiliary agent powder and stearic acid powder are: 3000 grams of not leaded carbon blacks and 100 grams of stearic acid.The weight error of auxiliary agent powder is controlled within 10.

Claims (5)

1. the preparation method of environmental protective type chemical mixed aid, it is characterised in that comprise the following steps:1. by all kinds of auxiliary agent powders Carry out fine crushing respectively, the powder particle size after fine crushing is controlled in 2000-5000 mesh;2. by all of above-mentioned fine crushing Kind of auxiliary agent powder and appropriate stearic acid powder are added to homogenizer together, control the rotating speed of mixer 1000r/min with On, until all powders are sufficiently mixed and into sticky matters;3. sticky matter cooled and solidified is into solid;4. above-mentioned solid is put into It is granulated in comminutor, mixed aid particle is formed after granulation;5. mixed aid particle is put on screen cloth and carries out sub-sieve, grain Footpath 2-6mm is qualified finished product, and prepared by mixed aid completes.
2. the preparation method of environmental protective type chemical mixed aid as claimed in claim 1, it is characterised in that preparing rubber mix During auxiliary agent, the selection species and weight proportion of auxiliary agent powder and stearic acid powder are:2500 grams of H foaming agents, 2500 grams of urea fat, 900 grams of zinc oxide and 900 grams of stearic acid.
3. the preparation method of environmental protective type chemical mixed aid as claimed in claim 1, it is characterised in that plastic foamed preparing During mixed aid, the selection species and weight proportion of auxiliary agent powder and stearic acid powder are:2500 grams of AC foaming agents, 1000 grams of oxygen Change zinc, 500 grams of zinc carbonates and 500 grams of stearic acid.
4. the preparation method of environmental protective type chemical mixed aid as claimed in claim 1, it is characterised in that mixed preparing PVC foam When closing auxiliary agent, the selection species and weight proportion of auxiliary agent powder and stearic acid powder are:5000 grams of AC foaming agents, 3000 grams of zinc, Barium, one kind in lead heat stabilizer, 500 grams of stearic acid.
5. the preparation method of environmental protective type chemical mixed aid as claimed in claim 1, it is characterised in that mixed preparing black masterbatch When closing auxiliary agent, the selection species and weight proportion of auxiliary agent powder and stearic acid powder are:3000 grams of not leaded carbon blacks and 100 grams are hard Resin acid.
CN201510108769.XA 2015-03-13 2015-03-13 The preparation method of environmental protective type chemical mixed aid Active CN104710650B (en)

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Publication number Priority date Publication date Assignee Title
CN109666245A (en) * 2018-12-14 2019-04-23 百尔罗赫塑料添加剂(江苏)有限公司 It is exclusively used in a pocket type environmental protection auxiliary agent and preparation method thereof for PVC stone plastic floor substrate production
CN110372975A (en) * 2019-09-02 2019-10-25 百尔罗赫塑料添加剂(江苏)有限公司 It is a kind of for improving the environmentally friendly auxiliary agent and preparation method thereof of PVC injection molding pipe part performance
CN113004574A (en) * 2021-02-26 2021-06-22 广东千千省化工有限公司 PVC material foaming color mixing auxiliary agent
CN114736451A (en) * 2022-04-02 2022-07-12 江阴市海江高分子材料有限公司 Preparation method of high-performance multifunctional cable shielding material

Citations (3)

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Publication number Priority date Publication date Assignee Title
CN101020770A (en) * 2007-03-15 2007-08-22 上海交通大学 Prepn process of foamed ethylene-octene copolymer material
CN103396675A (en) * 2013-07-19 2013-11-20 江西省大余章源竹木制品有限公司 Raw material treatment method for injection molding grade micro-foaming wood-plastic composite material
CN104277380A (en) * 2014-11-06 2015-01-14 安徽省三乐门窗幕墙工程有限公司 PVC wood plastic composite material with high cold resistance and preparation method of PVC wood plastic composite material

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102690457A (en) * 2011-03-25 2012-09-26 陈姜志 Flame-retardant environment-friendly material and manufacturing process thereof
CN102875880B (en) * 2012-10-22 2014-10-22 冼冰 Plastic foamed sheet with antistatic and flame-retardant functions and manufacturing technique thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101020770A (en) * 2007-03-15 2007-08-22 上海交通大学 Prepn process of foamed ethylene-octene copolymer material
CN103396675A (en) * 2013-07-19 2013-11-20 江西省大余章源竹木制品有限公司 Raw material treatment method for injection molding grade micro-foaming wood-plastic composite material
CN104277380A (en) * 2014-11-06 2015-01-14 安徽省三乐门窗幕墙工程有限公司 PVC wood plastic composite material with high cold resistance and preparation method of PVC wood plastic composite material

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Address after: 325000 Ge Yi village, Nanbin street, Ruian City, Wenzhou City, Zhejiang Province

Patentee after: Ruian Haobang New Material Technology Co.,Ltd.

Address before: 325000 Ge Yi village, Nanbin street, Ruian City, Wenzhou City, Zhejiang Province

Patentee before: RUI'AN HAOBANG RUBBER PLASTIC MATERIAL Co.,Ltd.

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Denomination of invention: Preparation method of environmental friendly chemical mixed additives

Effective date of registration: 20220411

Granted publication date: 20180202

Pledgee: Zhejiang Ruian Rural Commercial Bank Co.,Ltd. Plaza Science and Technology Branch

Pledgor: Ruian Haobang New Material Technology Co.,Ltd.

Registration number: Y2022980004123