CN104651740A - High-strength and -toughness 150 steel-grade drill pipe material and preparation method thereof - Google Patents

High-strength and -toughness 150 steel-grade drill pipe material and preparation method thereof Download PDF

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Publication number
CN104651740A
CN104651740A CN201310589071.5A CN201310589071A CN104651740A CN 104651740 A CN104651740 A CN 104651740A CN 201310589071 A CN201310589071 A CN 201310589071A CN 104651740 A CN104651740 A CN 104651740A
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inevitable impurity
drill pipe
preparation
material according
steel
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徐欣
王新虎
刘文红
宋生印
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China National Petroleum Corp
CNPC Tubular Goods Research Institute
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China National Petroleum Corp
CNPC Tubular Goods Research Institute
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Priority to CN201310589071.5A priority Critical patent/CN104651740A/en
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    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/005Ferrous alloys, e.g. steel alloys containing rare earths, i.e. Sc, Y, Lanthanides
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D8/00Modifying the physical properties by deformation combined with, or followed by, heat treatment
    • C21D8/10Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of tubular bodies
    • C21D8/105Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of tubular bodies of ferrous alloys
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/02Ferrous alloys, e.g. steel alloys containing silicon
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/04Ferrous alloys, e.g. steel alloys containing manganese
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/08Ferrous alloys, e.g. steel alloys containing nickel
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/12Ferrous alloys, e.g. steel alloys containing tungsten, tantalum, molybdenum, vanadium, or niobium
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/18Ferrous alloys, e.g. steel alloys containing chromium

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Earth Drilling (AREA)

Abstract

The invention discloses a high-strength and -toughness 150 steel-grade drill pipe material and belongs to the field of drill pipe materials. The high-strength and -toughness 150 steel-grade drill pipe material includes following chemical components, by mass: 0.23-0.30% of carbon, 0.5-1.5% of chromium, 0.6-1.0% of nickel, 0.9-1.5% of manganese, 0.8-1.4% of molybdenum, 0.1-0.5% of silicon, 0.6-1.0% of cerium, 0.01-0.08% of niobium, 0.01-0.08% of vanadium, and the balanced iron and unavoidable impurities, which include sulfur, phosphorus and aluminum, wherein the mass percentage ratio of the sulfur, phosphorus and aluminum are described as follows: S<=0.008%, P<=0.08% and Al<=0.07%. By means of addition of the rare earth element cerium with the contents of other components being controlled at the same time, the high-strength and -toughness 150 steel-grade drill pipe material, on the basis of satisfying mechanical performances of an API standard, is enhanced in fatigue resistance and is prolonged in fatigue life, so that the drill pipe material is more suitable for equipment service working conditions being more and more rigorous.

Description

A kind of high tough 150 steel grade drill pipe materials and preparation method thereof
Technical field
The present invention relates to drill rod materials field, particularly a kind of high tough 150 steel grade drill pipe materials and preparation method thereof.
Background technology
Drill string is the instrument of irreplaceable high-tech content in petroleum industry, is widely used in the underground deep layer operations such as oil production, geological prospecting and deep-well excavation.Drill string generally includes: drill bit, drill collar, drilling rod, stabilizer, special joint and square kelly.Wherein, drilling rod is the element of drill string, is mainly used in transmitting torque, conveying drilling fluid and in drilling process, is reached the object of constantly deepening well by the not connection breaking of drilling rod.Therefore, in oil development, require that drilling rod must can bear huge interior external pressure, distortion power and bending force etc.At present, in oil-gas exploration and development process, in order to improve the intensity of drill rod materials, 150 steel grade drill pipe materials of high strength are by progressively application.
Realizing in process of the present invention, contriver finds that prior art at least exists following problem:
Drilling rod in use, owing to being subject to the repeated action of various external force, can produce fatigue, thus brings the drilling rod even fatigure failure of drill string, i.e. drilling rod or drilling string failure.At present in day by day harsh oil development environment, the fatigue lifetime of oil drill rocker material is low, and drilling rod failure accidents incidence is high, has had a strong impact on the widespread use of material in oil drill rocker is produced.
Summary of the invention
In order to solve the problem that in prior art, 150 steel grade drill pipe material fatigue lifes are low, embodiments provide a kind of high tough 150 steel grade drill pipe materials and preparation method thereof.Described technical scheme is as follows:
On the one hand, the invention provides a kind of high tough 150 steel grade drill pipe materials, the chemical composition of described material and mass percentage content are: C(carbon): 0.23% ~ 0.30%, Cr(chromium): 0.5% ~ 1.5%, Ni(nickel): 0.6% ~ 1.0%, Mn(manganese): 0.9% ~ 1.5%, Mo(molybdenum): 0.8% ~ 1.4%, Si(silicon): 0.1% ~ 0.5%, Ce(cerium): 0.6% ~ 1.0%, Nb(niobium): 0.01 ~ 0.08%, V(vanadium): 0.01% ~ 0.08%, surplus is Fe(iron) and inevitable impurity, S(sulphur in described inevitable impurity), P(phosphorus), Al(aluminium) mass percent be: S :≤0.008%, P :≤0.08%, Al :≤0.07%.
A preferred technical scheme of the present invention is: the chemical composition of described material and mass percentage content are: C:0.26% ~ 0.29%, Cr:1.1% ~ 1.3%, Ni:0.7% ~ 0.9%, Mn:1.0% ~ 1.2%, Mo:1.0% ~ 1.2%, Si:0.2% ~ 0.3%, Ce:0.7% ~ 0.9%, Nb:0.03 ~ 0.06%, V:0.03% ~ 0.07%, surplus is Fe and inevitable impurity, in described evitable impurity, the mass percent of S, P, Al is: S :≤0.008%, P :≤0.08%, Al :≤0.07%.。
A preferred technical scheme is: the chemical composition of described material and mass percentage content are: C:0.29%, Cr:0.9%, Ni:0.75%, Mn:1.2%, Mo:0.9%, Si:0.30%, Ce:0.7%, Nb:0.06%, V:0.04%, surplus is Fe and inevitable impurity, in described inevitable impurity, the mass percent of S, P, Al is: S :≤0.005%, P :≤0.008%Al :≤0.03%.。
Another preferred technical scheme is: the chemical composition of described material and mass percentage content are: C:0.26%, Cr:0.8%, Ni:0.9%, Mn:1.0%, Mo:1.0%, Si:0.25%, Ce:0.9%, Nb:0.07%, V:0.06%, surplus is Fe and inevitable impurity, and in described inevitable impurity, the mass percent of S, P, Al is: S :≤0.003%, P :≤0.008%, Al :≤0.06%.
A preferred technical scheme is in addition: the chemical composition of described material and mass percentage content are: C:0.30%, Cr:0.75%, Ni:0.6%, Mn:1.35%, Mo:1.1%, Si:0.35%, Ce:0.71%, Nb:0.03%, V:0.01%, surplus is Fe and inevitable impurity, and in described inevitable impurity, the mass percent of S, P, Al is: S :≤0.003%, P :≤0.008%, Al :≤0.02%.
The chemical composition of material described in the present invention and the principle of design of mass percent as follows.
In deep-well construction process, the stress that drilling rod bears is very complicated, comprises tensile, compressive, bending, turns round, shears and compound and repeated load etc., easily causes the fatigure failure of drilling rod; Meanwhile, in deep-well construction, very high to the rotation speed requirements of drill string, and the too fast reversed of stress frequency that can increase of drilling speed, thus reduce the fatigue lifetime of drilling rod; In addition, according to mechanical vibration theory, when rotating speed overlaps with drill string natural frequency, drill string just resonates, and when occurring when resonating, drilling rod is new and old all can be very fast tired.Therefore, at present in deep-well construction process, the accident that drilling rod lost efficacy gets more and more.According to statistics, the accident of annual drilling string failure has 1000 example left and right, wherein causes the accident of drilling string failure to account for 50% ~ 60% of drilling string failure accident because drilling rod lost efficacy.
Existing theory, experiment and production practice all show, material Fatigue Failure Process under repeated load mainly contains two steps, and one is the germinating of fatigue cracking, and two is expansions of fatigue cracking.The time of fatigue crack initiation process account for 80% of whole Fatigue Failure Process total time.If the germinating time of fatigue cracking can be become sufficiently long, the ability that the antifatigue that just can improve material is to a great extent destroyed.According to the theory about material fatigue life up-to-date at present, think that the germinating process in fatigue cracking source of material is the process of damage accumulation.In the process, be first form FATIGUE SHORT CRACK GROWTH, short crack polymerization is final forms fatigue cracking source.According to up-to-date achievement in research, when certain energy input, the length of FATIGUE SHORT CRACK GROWTH concentrates near the grain-size of material, and the length of FATIGUE SHORT CRACK GROWTH, only when increasing input energy, just may continue to grow up to two grain sizes.Reason is in this process, and crystal boundary makes crack propagation be hindered.And continuing to increase and be polymerized, the crackle that final formation is large of these short cracks, become fatigue cracking source, accelerate expansion.So think that the anti-fatigue performance impact of grain-size on material is very large, grain-size is less, and anti-fatigue performance is better.In addition, topmost germinating place of fatigue cracking is the defect produced in second-phase in material and processing and manufacturing process, therefore, in the manufacture and heat treatment process of material, make the second phase particles in material little as far as possible, and glomeration, to reduce its surface energy, and avoid as much as possible producing surface imperfection.
In order to solve the problem, the embodiment of the present invention is passed through to add rare earth element ce and the content controlling other chemical compositions, namely the formula adjusting 150 steel grade drill pipe materials carrys out crystal grain thinning, make second phase particles glomeration, thus improve the obdurability coupling of described drill rod materials, improve the anti-fatigue performance of material, extend fatigue lifetime.
Specific explanations is as follows:
In the embodiment of the present invention, C is austenite former, the effect that minimizing is the consumption of the Ni of austenite former equally can be played containing C, but above-mentioned DeGrain when C content is too low, also the intensity of material is damaged, C is also carbide forming element, can improve the intensity of steel containing C, but high-content C is easily formed containing the thick M of Cr particle 23c 6type carbide, reduces anti-SSC performance and the impelling strength of steel.For taking into account strength and toughness, C addition of the present invention is 0.23 ~ 0.30%.
In the embodiment of the present invention, Mn cost is lower, has the effect improving hardening capacity and improved ferrite intensity by solution strengthening.But Mn content cross manganese alloy cementite can be caused at most too much be distributed in crystal boundary, reduce toughness of material.
Rare earth element ce is with the addition of in the embodiment of the present invention.Rare earth element ce can cleaning molten steel, reduces the segregation of P on crystal boundary, eliminates Fe 3p weakens the deleterious effect of crystal boundary, and strengthening grain boundary state, forms spherical oxysulfide simultaneously.This compound hardness, higher than MnS, can not be strip distribution along rolling direction when rolling, avoid stress concentration, improve intensity, toughness and fatigue strength.Rare earth element ce can promote that the microalloy element being solid-solution in austenitic area is separated out in ferrite area simultaneously, improves the utilization ratio of microalloy element.The microalloying mechanism of rare earth element ce has a certain impact to the mechanical property of drill rod materials, improves the purity of drilling rod steel, the harmful element content such as P, S, O, N are down to minimum.In addition, adding of rare earth element ce makes inclusion spherical in shape, the tiny branch of further disperse; Many alloy cpds disperse educt, effectively prevents germinating and the expansion of fatigue cracking.
In the embodiment of the present invention, Nb separates out tiny carbide in austenitic area, by Grain boundary pinning effect restrain grain growth, crystal grain thinning, recrystallization temperature and grain coarsening temperature can be improved at the Nb of recrystallization zone solid solution simultaneously, be conducive to making grain deformation then be recrystallised to tiny crystal grain by controlled rolling.The precipitation of tiny carbide simultaneously is also conducive to the intensity improving steel.The effect that Nb improves obdurability by microalloying is the strongest, effectively improves intensity 150Mpa simultaneously.Rare earth and Nb combine the amount of precipitation that doping can significantly improve Nb carbide simultaneously, reduce carbide size, are conducive to the effect improving grain refining and dispersion-strengthened.
On the other hand, the invention provides the preparation method of the tough 150 steel grade drill pipe materials of a kind of above-mentioned height, the preparation method of described material comprises:
The manufacturing processed of material and the heat treatment process of material, first carry out melting and continuous casting to described material, then through extrusion tube blank or pierced billet pipe, be rolled into body, finally carry out body thermal treatment.
Further, described body thermal treatment comprises Quench and temper.
Described quenching is specially water quenching.
Further, need after being rolled into body described in carry out sizing and aligning.
Described sizing specifically comprises the expanding and thermotension tube reducing of thermotension.
The beneficial effect that the technical scheme that the embodiment of the present invention provides is brought is: by adding rare earth element ce, having purified molten steel, having decreased the segregation of P on crystal boundary, eliminate Fe 3p weakens the deleterious effect of crystal boundary, strengthening grain boundary state; In addition, rare earth element ce and element nb combine the amount of precipitation that doping can significantly improve Nb carbide, reduce carbide size, improve the effect of grain refining and dispersion-strengthened.The formation of spherical oxysulfide simultaneously, makes material can not be strip distribution along rolling direction when rolling, avoids stress concentration.Gained 150 steel grade drill pipe material of the present invention is on the basis of mechanical property meeting all API standards, and be under the condition of yield strength 80% at fatigue stress peak value, tired cycle is 10 7, anti-fatigue performance is improved, and fatigue lifetime obtains prolongation; Apply the drilling rod that the tough 150 steel grade drill pipe materials of above-mentioned height manufacture, in the underground deep layer operations such as oil production, geological prospecting and deep-well excavation, be more applicable to day by day harsh equipment military service operating mode.
Accompanying drawing explanation
In order to be illustrated more clearly in the technical scheme in the embodiment of the present invention, below the accompanying drawing used required in describing embodiment is briefly described, apparently, accompanying drawing in the following describes is only some embodiments of the present invention, for those of ordinary skill in the art, under the prerequisite not paying creative work, other accompanying drawing can also be obtained according to these accompanying drawings.
Fig. 1 is the scanning electron microscope schematic diagram of the tough 150 steel grade drill pipe materials of height that the embodiment of the present invention 1 provides;
Fig. 2 is the scanning electron microscope schematic diagram of the tough 150 steel grade drill pipe materials of height that the embodiment of the present invention 5 provides;
Fig. 3 is the scanning electron microscope schematic diagram of the tough 150 steel grade drill pipe materials of height that the embodiment of the present invention 10 provides.
Embodiment
For making the object, technical solutions and advantages of the present invention clearly, below embodiment of the present invention is described further in detail.
The preparation method of a kind of 150 steel grade drill pipe materials that the embodiment of the present invention provides, comprise the manufacture of material and the heat treatment process of material, specifically operate in accordance with the following steps: the quality that the formula calculation of the drill rod materials first provided according to the embodiment of the present invention is raw materials used, wherein raw materials used and model, specification, quality are selected according to the steelmaking process of this area routine and method; Then all raw materials are carried out melting at 1600-1700 DEG C; Then, under 1560-1600 DEG C of condition, carry out external refining, at vacuum tightness-0.08Pa, under temperature 1500 DEG C of conditions, carry out extrusion tube blank or pierced billet pipe under continuous casting, 1150-1180 DEG C condition; Then after 950-980 DEG C of body rolling, 750-850 DEG C is carried out the expanding and thermotension tube reducing of thermotension, reaches after specified dimension requires and carries out cooling and aligning; Then, carry out pier at 1100-1200 DEG C and slightly thicken, then after 950 DEG C of austenitizing 30min, carry out water quenching, finally in 600-650 DEG C of tempering 25-50min.The preparation method of described 150 steel grade drill pipe materials, technique is simple, easy to implement, with low cost.
In specific embodiment 1-10 the composition of 150 steel grade drill pipe materials and mass percent as shown in table 2, surplus is Fe and inevitable impurity, in described inevitable impurity, the mass percent of S, P, Al is: S :≤0.008%, P :≤0.08%, Al :≤0.07%, all the other inevitable foreign matter contents are very little, negligible.
The composition of table 2 embodiment 1-10150 steel grade drill pipe material and mass percent thereof
In specific embodiment 1-10, the preparation technology parameter of 150 steel grade drill pipe materials is as shown in table 3.
The preparation technology parameter of table 3 embodiment 1-10150 steel grade drill pipe material
The material mechanical performance that embodiment of the present invention 1-10 provides is tested according to the regulation of GB/T6394-2002, uses tensile testing machine or balance weight impact testing machine to test; The test of the safe range of stress value of described material uses draws-pulling fatigue experimental machine, and safe range of stress value test condition is: fatigue of materials cycle 10 7.The material mechanical performance that embodiment of the present invention 1-10 provides and tired extreme value are limit as shown in table 4.
Comparative example: with 150 commercially available steel grade drill pipe materials for contrast product, it is carried out to the test of the mechanical property identical with the embodiment of the present invention and safe range of stress value, the results are shown in Table 4.
The structure of 150 drill rod materials that the embodiment of the present invention provides for the electron-microscope scanning figure of embodiment 1,5,10 resulting materials, as Figure 1-3.
Table 4 embodiment 1-10150 steel grade drill pipe material mechanical performance and safe range of stress detected result
As can be seen from Table 4, when fatigue of materials cycle 10 7time, the drill rod materials safe range of stress value prepared by embodiment of the present invention 1-10 is 850-885Mpa, and 150 drill rod materials safe range of stress of comparative example are 710Mpa, are starkly lower than the safe range of stress value of the drill rod materials that embodiment of the present invention 1-10 provides.Under identical tired cycle condition, the safe range of stress value of drill rod materials is higher, and its fatigue lifetime is longer, more fatigure failure is less likely to occur.
The drilling rod of 150 steel grade drill pipe materials manufactures that the height that Application Example 1-10 provides is tough, in the underground deep layer operations such as oil production, geological prospecting and deep-well excavation, under fatigue stress peak value is the condition of yield strength 80%, tired cycle is 10 7, and the drilling rod that 150 drill rod materials of Comparison study example manufacture is in the underground deep layer operations such as oil production, geological prospecting and deep-well excavation, fatigue stress peak value is under the condition of yield strength 80%, and tired cycle is 10 5-10 6.Visible, the drilling rod that the 150 steel grade drill pipe materials that the application embodiment of the present invention provides manufacture is long for fatigue lifetime, is more applicable to day by day harsh equipment military service operating mode.
The invention described above embodiment sequence number, just to describing, does not represent the quality of embodiment.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, within the spirit and principles in the present invention all, any amendment done, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.

Claims (10)

1. one kind high tough 150 steel grade drill pipe materials, it is characterized in that, the chemical composition of described material and mass percentage content are: C:0.23% ~ 0.30%, Cr:0.5% ~ 1.5%, Ni:0.6% ~ 1.0%, Mn:0.9% ~ 1.5%, Mo:0.8% ~ 1.4%, Si:0.1% ~ 0.5%, Ce:0.6% ~ 1.0%, Nb:0.01 ~ 0.08%, V:0.01% ~ 0.08%, surplus is Fe and inevitable impurity, in described inevitable impurity, the mass percent of S, P, Al is: S :≤0.008%, P :≤0.08%, Al :≤0.07%.
2. material according to claim 1, it is characterized in that, the chemical composition of described material and mass percentage content are: C:0.26% ~ 0.29%, Cr:1.1% ~ 1.3%, Ni:0.7% ~ 0.9%, Mn:1.0% ~ 1.2%, Mo:1.0% ~ 1.2%, Si:0.2% ~ 0.3%, Ce:0.7% ~ 0.9%, Nb:0.03 ~ 0.06%, V:0.03% ~ 0.07%, surplus is Fe and inevitable impurity, in described inevitable impurity, the mass percent of S, P, Al is: S :≤0.008%, P :≤0.08%, Al :≤0.07%.
3. material according to claim 1, is characterized in that, the chemical composition of described material and mass percentage content are: C:0.29%, Cr:0.9%, Ni:0.75%, Mn:1.2%, Mo:0.9%, Si:0.30%, Ce:0.7%, Nb:0.06%, V:0.04%, surplus is Fe and inevitable impurity, in described inevitable impurity, the mass percent of S, P, Al is: S :≤0.005%, P :≤0.008%Al :≤0.03%.
4. material according to claim 1, is characterized in that, the chemical composition of described material and mass percentage content are: C:0.26%, Cr:0.8%, Ni:0.9%, Mn:1.0%, Mo:1.0%, Si:0.25%, Ce:0.9%, Nb:0.07%, V:0.06%, surplus is Fe and inevitable impurity, in described inevitable impurity, the mass percent of S, P, Al is: S :≤0.003%, P :≤0.008%, Al :≤0.06%.
5. material according to claim 1, is characterized in that, the chemical composition of described material and mass percentage content are: C:0.30%, Cr:0.75%, Ni:0.6%, Mn:1.35%, Mo:1.1%, Si:0.35%, Ce:0.71%, Nb:0.03%, V:0.01%, surplus is Fe and inevitable impurity, in described inevitable impurity, the mass percent of S, P, Al is: S :≤0.003%, P :≤0.008%, Al :≤0.02%.
6. prepare the method for the material described in any one of claim 1-5 for one kind, it is characterized in that, the preparation method of described material comprises the manufacturing processed of material and the heat treatment process of material, first melting and continuous casting are carried out to raw material, again through extrusion tube blank or pierced billet pipe, be rolled into body, finally carry out body thermal treatment.
7. the preparation method of material according to claim 6, is characterized in that, described body thermal treatment comprises Quench and temper.
8. the preparation method of material according to claim 7, is characterized in that, described quenching is water quenching.
9. the preparation method of material according to claim 6, is characterized in that, described in be rolled into body after need to carry out sizing and aligning.
10. the preparation method of material according to claim 9, is characterized in that, described sizing comprises the expanding and thermotension tube reducing of thermotension.
CN201310589071.5A 2013-11-20 2013-11-20 High-strength and -toughness 150 steel-grade drill pipe material and preparation method thereof Pending CN104651740A (en)

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CN106287053A (en) * 2016-08-11 2017-01-04 宁波市鄞州亚大汽车管件有限公司 One withholds casing joint
CN106282763A (en) * 2016-08-11 2017-01-04 宁波市鄞州亚大汽车管件有限公司 A kind of brake pipe joint
CN106282764A (en) * 2016-08-11 2017-01-04 宁波市鄞州亚大汽车管件有限公司 A kind of preparation method of brake pipe joint
CN109943764A (en) * 2019-04-24 2019-06-28 西王金属科技有限公司 A kind of railroad train connection high intensity 23Mn2CrNiMoVREA steel and preparation method thereof

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CN106287053A (en) * 2016-08-11 2017-01-04 宁波市鄞州亚大汽车管件有限公司 One withholds casing joint
CN106282763A (en) * 2016-08-11 2017-01-04 宁波市鄞州亚大汽车管件有限公司 A kind of brake pipe joint
CN106282764A (en) * 2016-08-11 2017-01-04 宁波市鄞州亚大汽车管件有限公司 A kind of preparation method of brake pipe joint
CN109943764A (en) * 2019-04-24 2019-06-28 西王金属科技有限公司 A kind of railroad train connection high intensity 23Mn2CrNiMoVREA steel and preparation method thereof

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Application publication date: 20150527