CN104628398B - A kind of cement kiln burner prefabricated component and preparation method - Google Patents

A kind of cement kiln burner prefabricated component and preparation method Download PDF

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CN104628398B
CN104628398B CN201510071466.5A CN201510071466A CN104628398B CN 104628398 B CN104628398 B CN 104628398B CN 201510071466 A CN201510071466 A CN 201510071466A CN 104628398 B CN104628398 B CN 104628398B
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powder
parts
additive
prefabricated component
liquor alumini
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CN104628398A (en
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梁尤平
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Chengde Jidong Cement Co., Ltd.
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CHONGQING XIONGCHUANG CONSTRUCTION ENGINEERING TECHNOLOGY Co Ltd
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Priority to CN201610732096.XA priority Critical patent/CN106336230A/en
Priority to CN201510071466.5A priority patent/CN104628398B/en
Priority to CN201610732097.4A priority patent/CN106348767A/en
Priority to CN201610731618.4A priority patent/CN106396692A/en
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    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/66Monolithic refractories or refractory mortars, including those whether or not containing clay
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3205Alkaline earth oxides or oxide forming salts thereof, e.g. beryllium oxide
    • C04B2235/3206Magnesium oxides or oxide-forming salts thereof
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3205Alkaline earth oxides or oxide forming salts thereof, e.g. beryllium oxide
    • C04B2235/3213Strontium oxides or oxide-forming salts thereof
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3217Aluminum oxide or oxide forming salts thereof, e.g. bauxite, alpha-alumina
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3217Aluminum oxide or oxide forming salts thereof, e.g. bauxite, alpha-alumina
    • C04B2235/3222Aluminates other than alumino-silicates, e.g. spinel (MgAl2O4)
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3231Refractory metal oxides, their mixed metal oxides, or oxide-forming salts thereof
    • C04B2235/3244Zirconium oxides, zirconates, hafnium oxides, hafnates, or oxide-forming salts thereof
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
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    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/38Non-oxide ceramic constituents or additives
    • C04B2235/3804Borides
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    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/38Non-oxide ceramic constituents or additives
    • C04B2235/3817Carbides
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/38Non-oxide ceramic constituents or additives
    • C04B2235/3817Carbides
    • C04B2235/3839Refractory metal carbides
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/38Non-oxide ceramic constituents or additives
    • C04B2235/3852Nitrides, e.g. oxynitrides, carbonitrides, oxycarbonitrides, lithium nitride, magnesium nitride
    • C04B2235/3865Aluminium nitrides
    • C04B2235/3869Aluminium oxynitrides, e.g. AlON, sialon

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Furnace Housings, Linings, Walls, And Ceilings (AREA)
  • Ceramic Products (AREA)
  • Curing Cements, Concrete, And Artificial Stone (AREA)

Abstract

The invention discloses a kind of cement kiln burner prefabricated component and preparation method, and this cement kiln is with burner prefabricated component by magnesium aluminate spinel, Si2Al4O4N4、Al3BC3, zirconium spinel, strontium carbonate powder, be carbonized vanadium powder, alumina powder, pure calcium aluminate cement, composite powder, additive and liquor alumini chloridi composition.Using gravity flow pouring method shape, through conserving, dry after, be heat-treated at high temperature.Compared with traditional castable, there is this product gravity flow to construct, self-defoaming, anti-strip, and wearability is high, the features such as long lifespan, can be more widely used at the burner position of the rotary kiln used in various cement industries.

Description

A kind of cement kiln burner prefabricated component and preparation method
Technical field
The present invention relates to a kind of cement kiln burner prefabricated component and preparation method, more particularly to burnt ore industry, water Mud industry, lime industry, cement kiln combustion device prefabricated component and preparation method used in metallurgy industry.
Background technology
Generally all it is that vibrating casting shaping is being carried out using scene using balk cargo in traditional burner, so as to extend Stop the cycle of kiln, long construction period, field labor intensity are big, construction when add that water is more, length curing cycle, final products short life, It thus have impact on the normal production of cement kiln.Existing castable product also is difficult to meet anti-during burner use simultaneously Peel off, short life, construction quality is segregated the problems such as unstable.Prefabricated component refers to change supply of material pattern:Burner is in fire resisting factory Cast, maintenance and heat treatment are completed, the product is then moved to producer and directly used, the exploitation of this kind of product thoroughly solves biography The site operation weakness of system Unshaped Casting Refractories.
The content of the invention
It is exactly that thermal shock resistance is poor, and short life and construction quality are poor in order to solve product not anti-strip in the purpose of the present invention The defects of, there is provided a kind of cement kiln burner prefabricated component and preparation method, manufactured preform product disclosure satisfy that cement kiln The anti-strip of burner requirement, the long-life, thermal shock resistance is high, easy for construction, the problems such as steady quality.
In order to solve the above technical problems, the present invention adopts the following technical scheme that:Prefabricated component by magnesium aluminate spinel, Si2Al4O4N4、Al3BC3, zirconium spinel, strontium carbonate powder, be carbonized vanadium powder, alumina powder, pure calcium aluminate cement, composite powder, outside Agent and liquor alumini chloridi is added to form.
Magnesium aluminate spinel, Si in raw material2Al4O4N4、Al3BC3, zirconium spinel, strontium carbonate powder, be carbonized vanadium powder, and aluminum oxide is micro- Powder, pure calcium aluminate cement, the parts by weight of composite powder are:Magnesium aluminate spinel 15-20 parts, Si2Al4O4N420-25 parts, Al3BC37-12 parts, zirconium spinel 20-28 parts, strontium carbonate powder 1-3 parts, be carbonized vanadium powder 2-4 parts, alumina powder 8-12 parts, fine aluminium Sour calcium cement 3-7 parts, composite powder 0-1 parts.Liquor alumini chloridi, the addition of additive account for the percentage of above-mentioned gross weight respectively For:Liquor alumini chloridi 9%, additive 0.2-0.3%;Composite powder is made up of leucite powder and kaliophilite powder, and its weight is than 1:1.
Described additive is sulfonated melamine compound resin, and isooctanol, 5- Sulfonic Salicylic Acids, three's weight ratio is 2: 1:1.Described liquor alumini chloridi density is 1.25 grams/cc, pH3.5, viscosity 0.006KPas.
Above-mentioned each raw material is subjected to dispensing in above ratio, after being well mixed, shaped using the method for gravity flow pouring, through supporting Shield, after drying, it is heat-treated at high temperature, obtains this burner prefabricated component.
The present invention preparation method be:
Step 1: batch mixing and stirring, prepare raw material by proportioning, add additive, stirred in mixer, stir Liquor alumini chloridi is added after uniformly, 200 mm are controlled from flow valuve;Step 2: shaping, maintenance and dry, shaping:By mould Tool installs, add be stirred be stirred material, the deadweight and surface tension by compound are shakeout;The material of excess surface is smeared Go;Maintenance:The good sample of gravity flow pouring and mould are put into 25 DEG C of thermostatic chambers, are stripped after hardening on inspection, it is natural again after the demoulding Maintenance 48 hours;Dry:The sample conserved carries out 110 DEG C of 24h drying and processings in electrical kiln, closes power supply and treats that it is cooled to room Temperature;Step 3: heat treatment, dried sample are put into heating furnace, 300 DEG C are begun to warm to according to 5 DEG C/min, then with 10 DEG C/min speed is raised to 1000 DEG C, and is incubated 3 hours;After end, room temperature is naturally cooled to, this cement kiln is obtained after coming out of the stove Use prefabricated component.
The bulk density of gained prefabricated component is in 2.7g/cm3, strength at normal temperature 25MPa, wear-resisting to be less than 4, service life exists More than 18 months.
The present invention has obtained a kind of anti-strip, long-life, gravity flow construction, the cement kiln burner prefabricated component of self-defoaming. The prefabricated component high temperature resistant, anti-strip, the long-life, improve the running rate of cement kiln industry, gravity flow pouring during construction, stomata can be with Voluntarily eliminate, avoid caused by vibrating casting material quality and be segregated, the shortcomings that changing original bulk products, this kind of product is opened Hair thoroughly solves the site operation weakness of traditional Unshaped Casting Refractories.
Embodiment
Embodiment 1,16 parts of magnesium aluminate spinel, Si2Al4O4N425 parts, Al3BC312 parts, 20 parts of zirconium spinel, strontium carbonate powder 3 Part, be carbonized 4 parts of vanadium powder, 12 parts of alumina powder, 7 parts of pure calcium aluminate cement, 1 part of composite powder.Additive is added, is sufficiently mixed After even, liquor alumini chloridi is then added.Liquor alumini chloridi, the addition of additive account for the percentage of above-mentioned gross weight respectively For:Liquor alumini chloridi 9%, additive 0.3%.
Embodiment 2,17 parts of magnesium aluminate spinel, Si2Al4O4N424 parts, Al3BC312 parts, 20 parts of zirconium spinel, strontium carbonate powder 3 Part, be carbonized 4 parts of vanadium powder, 12 parts of alumina powder, 7 parts of pure calcium aluminate cement, 1 part of composite powder.Additive is added, is sufficiently mixed After even, liquor alumini chloridi is then added.Liquor alumini chloridi, the addition of additive account for the percentage of above-mentioned gross weight respectively For:Liquor alumini chloridi 9%, additive 0.2%.
Embodiment 3,18 parts of magnesium aluminate spinel, Si2Al4O4N423 parts, Al3BC312 parts, 21 parts of zirconium spinel, strontium carbonate powder 3 Part, be carbonized 4 parts of vanadium powder, 12 parts of alumina powder, 7 parts of pure calcium aluminate cement, 0 part of composite powder.Additive is added, is sufficiently mixed After even, liquor alumini chloridi is then added.Liquor alumini chloridi, the addition of additive account for the percentage of above-mentioned gross weight respectively For:Liquor alumini chloridi 9%, additive 0.3%.
The follow-up preparation technology of embodiment 1,2,3 is:Mould installion is good, add be stirred be stirred material, by mixed The deadweight and surface tension for closing material are shakeout;The material of excess surface is erased;Maintenance:The good sample of gravity flow pouring and mould are put into 25 DEG C thermostatic chamber, it is stripped after hardening on inspection, natural curing 48 hours again after the demoulding;Dry:The sample conserved enters in electrical kiln 110 DEG C of 24h drying and processings of row, close power supply and treat that it is cooled to room temperature;Step 3: heat treatment, dried sample are put into heating In stove, 300 DEG C are begun to warm to according to 5 DEG C/min, then 1000 DEG C are raised to 10 DEG C/min speed, and is incubated 3 hours;Terminate Afterwards, room temperature is naturally cooled to, this cement kiln burner prefabricated component is obtained after coming out of the stove.

Claims (3)

  1. A kind of 1. cement kiln burner prefabricated component, it is characterised in that:By magnesium aluminate spinel, Si2Al4O4N4、Al3BC3, zirconium point it is brilliant Stone, strontium carbonate powder, be carbonized vanadium powder, alumina powder, pure calcium aluminate cement, composite powder, additive and liquor alumini chloridi composition;Its In, 16 parts of magnesium aluminate spinel, Si2Al4O4N425 parts, Al3BC312 parts, 20 parts of zirconium spinel, 3 parts of strontium carbonate powder, be carbonized vanadium powder 4 Part, 12 parts of alumina powder, 7 parts of pure calcium aluminate cement, 1 part of composite powder;Additive is added, after being sufficiently mixed uniformly, Ran Houzai Add liquor alumini chloridi;The percentage that liquor alumini chloridi, the addition of additive account for above-mentioned gross weight respectively is:Liquor alumini chloridi 9%, additive 0.3%;Composite powder is made up of leucite powder and kaliophilite powder, and its weight is than 1:1;Additive is sulfonation melamine Amine-formaldehyde resins, isooctanol, 5- Sulfonic Salicylic Acids, three's weight ratio are 2:1:1.
  2. A kind of 2. cement kiln burner prefabricated component according to claim 1, it is characterised in that:Described liquor alumini chloridi Density is 1.25 grams/cc, pH3.5, viscosity 0.006KPas.
  3. A kind of 3. preparation method of cement kiln burner prefabricated component according to claim 1, it is characterised in that:Step First, batch mixing and stirring, raw material is prepared by proportioning, additive is added, stirs in mixer, added after stirring Liquor alumini chloridi, 200 mm are controlled from flow valuve;Step 2: shaping, maintenance and dry, shaping:Mould installion is good, add What is be stirred is stirred material, and the deadweight and surface tension by compound are shakeout;The material of excess surface is erased;Maintenance:Will gravity flow Pour the sample being poured in and mould is put into 25 DEG C of thermostatic chambers, be stripped after hardening on inspection, natural curing 48 hours again after the demoulding;It is dry It is dry:The sample conserved carries out 110 DEG C of 24h drying and processings in electrical kiln, closes power supply and treats that it is cooled to room temperature;It is Step 3: hot Processing, dried sample are put into heating furnace, and 300 DEG C, then the speed liter with 10 DEG C/min are begun to warm to according to 5 DEG C/min To 1000 DEG C, and it is incubated 3 hours;After end, room temperature is naturally cooled to, it is prefabricated that this cement kiln burner is obtained after coming out of the stove Part.
CN201510071466.5A 2015-02-11 2015-02-11 A kind of cement kiln burner prefabricated component and preparation method Active CN104628398B (en)

Priority Applications (4)

Application Number Priority Date Filing Date Title
CN201610732096.XA CN106336230A (en) 2015-02-11 2015-02-11 Burner prefab for cement kiln and preparation method thereof
CN201510071466.5A CN104628398B (en) 2015-02-11 2015-02-11 A kind of cement kiln burner prefabricated component and preparation method
CN201610732097.4A CN106348767A (en) 2015-02-11 2015-02-11 Combustor prefabricated part for cement kilns and preparation method thereof
CN201610731618.4A CN106396692A (en) 2015-02-11 2015-02-11 Combustor prefabricated part used for cement kilns, and preparation method thereof

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CN201510071466.5A CN104628398B (en) 2015-02-11 2015-02-11 A kind of cement kiln burner prefabricated component and preparation method

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CN201610732097.4A Division CN106348767A (en) 2015-02-11 2015-02-11 Combustor prefabricated part for cement kilns and preparation method thereof
CN201610731618.4A Division CN106396692A (en) 2015-02-11 2015-02-11 Combustor prefabricated part used for cement kilns, and preparation method thereof

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CN201610732097.4A Pending CN106348767A (en) 2015-02-11 2015-02-11 Combustor prefabricated part for cement kilns and preparation method thereof
CN201610732096.XA Pending CN106336230A (en) 2015-02-11 2015-02-11 Burner prefab for cement kiln and preparation method thereof
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CN201610731618.4A Pending CN106396692A (en) 2015-02-11 2015-02-11 Combustor prefabricated part used for cement kilns, and preparation method thereof

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CN104628398B (en) * 2015-02-11 2017-11-10 重庆雄创建筑工程技术有限公司 A kind of cement kiln burner prefabricated component and preparation method
CN107512918A (en) * 2017-08-25 2017-12-26 长兴兴鹰新型耐火建材有限公司 A kind of preformed bricks of resource reusing
CN107540397A (en) * 2017-08-25 2018-01-05 长兴兴鹰新型耐火建材有限公司 The preformed bricks that a kind of high strength and low thermal is led
CN107540356A (en) * 2017-09-04 2018-01-05 河南鑫诚耐火材料股份有限公司 A kind of carbon baking furnace flame path wall novel energy-conserving prefabricated component and preparation method thereof

Citations (2)

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Publication number Priority date Publication date Assignee Title
US5212123A (en) * 1990-10-24 1993-05-18 Savoie Refractaires Refractory materials formed from refractory grains bonded by a sialon matrix containing dispersed graphite and/or boron nitride particles and a process for the preparation of these materials
CN104058771A (en) * 2014-07-18 2014-09-24 徐梅子 Fire-resistant castable for pre-heater

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102503487B (en) * 2011-11-08 2013-05-01 山国强 Prefabricated member for combustor and preparation method for prefabricated member
CN104628398B (en) * 2015-02-11 2017-11-10 重庆雄创建筑工程技术有限公司 A kind of cement kiln burner prefabricated component and preparation method

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5212123A (en) * 1990-10-24 1993-05-18 Savoie Refractaires Refractory materials formed from refractory grains bonded by a sialon matrix containing dispersed graphite and/or boron nitride particles and a process for the preparation of these materials
CN104058771A (en) * 2014-07-18 2014-09-24 徐梅子 Fire-resistant castable for pre-heater

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CN104628398A (en) 2015-05-20

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