CN104611473A - Producing method of pharmaceutic adjuvant cane sugar by carbonic acid method process - Google Patents
Producing method of pharmaceutic adjuvant cane sugar by carbonic acid method process Download PDFInfo
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- CN104611473A CN104611473A CN201410797420.7A CN201410797420A CN104611473A CN 104611473 A CN104611473 A CN 104611473A CN 201410797420 A CN201410797420 A CN 201410797420A CN 104611473 A CN104611473 A CN 104611473A
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- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B5/00—Reducing the size of material from which sugar is to be extracted
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- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B10/00—Production of sugar juices
- C13B10/02—Expressing juice from sugar cane or similar material, e.g. sorghum saccharatum
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- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B20/00—Purification of sugar juices
- C13B20/005—Purification of sugar juices using chemicals not provided for in groups C13B20/02 - C13B20/14
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- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B20/00—Purification of sugar juices
- C13B20/02—Purification of sugar juices using alkaline earth metal compounds
- C13B20/04—Purification of sugar juices using alkaline earth metal compounds followed by saturation
- C13B20/06—Purification of sugar juices using alkaline earth metal compounds followed by saturation with carbon dioxide or sulfur dioxide
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- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B25/00—Evaporators or boiling pans specially adapted for sugar juices; Evaporating or boiling sugar juices
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- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B30/00—Crystallisation; Crystallising apparatus; Separating crystals from mother liquors ; Evaporating or boiling sugar juice
- C13B30/04—Separating crystals from mother liquor
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- C—CHEMISTRY; METALLURGY
- C13—SUGAR INDUSTRY
- C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
- C13B40/00—Drying sugar
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Crystallography & Structural Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Medicines Containing Plant Substances (AREA)
- Medicinal Preparation (AREA)
Abstract
A producing method of a pharmaceutic adjuvant cane sugar by a carbonic acid method process is disclosed. The producing method directly adopts sugarcane as a raw material and obtains the pharmaceutic cane sugar by steps of smashing, squeezing, clearing, evaporating, sugar boiling, separating molasses and drying. A sulphur bleaching-floating combined step is added between the evaporating step and the sugar boiling step to further remove various impurities in the cane sugar and to improve the cleanliness level of the cane sugar, so that contents of sulfates, residues on ignition, calcium salts, heavy metals, and the like in the cane sugar meet the index requirements in the Chinese Pharmacopoeia of the 2010 edition. The carbonic acid method is low in equipment requirement and simple in process, and therefore the producing method is suitable for large-scale production of cane sugar, and overcomes the problem that cane sugar produced by traditional carbonic acid method processes cannot meet the standards of the pharmaceutic cane sugar and the problem that the pharmaceutic cane sugar is difficult in large-scale production.
Description
Technical field
The present invention relates to a kind of method for manufacturing sugar, particularly a kind of method utilizing carbonatation process explained hereafter pharmaceutical excipient sugar.
Background technology
Medical cane sugar is one of pharmaceutical excipient important in China's pharmaceutical industry, it is important correctives, be again important vehicle, be used in the oral preparations such as the granule of medicine, tablet, syrup, oral liquid, cream taste, pill widely, especially in Chinese patent medicine preparation.Pharmaceutical excipient sucrose is one of kind being embodied in " Chinese Pharmacopoeia " the earliest, but after 2005 " letter about printing and distributing the requirement of pharmaceutical excipient registration declaration material " is issued, the authentication code of Cai You only a few enterprise application medical cane sugar.The quality standard of medical cane sugar is more more strict than common sucrose, its price be several times to tens times of common sucrose not etc.
Find through retrieval, domestic patent database discloses the pertinent literature of some medical cane sugar production technologies, can find that edible sucrose is used for pharmaceutical production by most of drug manufacturing enterprise, generally comprise and select food sugar, preparing tank, absorption, filtration and recrystallization, centrifugal, dry, pulverizing, the step such as packaging, warehouse-in, such as:
The production technique of [title] medical cane sugar, [patent No.] CN200910042951.4, [publication date] 2009-08-19, the production technique of [summary] medical cane sugar, comprise step: (1) is by sucrose dissolved pre-treatment: be dissolved in by food grade sucrose in 1: 1 ~ 100 (w/v) purified water, heat up, the gac adding raw material sucrose weight 0.5 ~ 1.5% stirs, filter, filtrate is in storage tank; (2) electrodialysis process: pretreated sucrose solution carries out clarification process by electrodialysis appts, wherein liquid glucose flow control is at 1.0m
3/ h ~ 1.5m
3/ h, control voltage makes current density be 75mA/cm
3; Until the specific conductivity of sucrose solution is less than 20 μ s/cm, liquid glucose is inputted underpressure distillation in retort, controlling Vacuum Pressure is-0.085MPa, and temperature is 45 DEG C, and being concentrated into water content is 10% ~ 40%, and crystallization is centrifugal.The present invention be a kind of with short production cycle, pollute little, energy expenditure is little, effectively can remove the production technique of the medical cane sugar of the impurity such as heavy metal and vitriol thereof in sucrose material.
Utilize edible sucrose for pharmaceutical production, security be high, relative low price, but medical cane sugar yields poorly, be difficult to scale operation.
Minority drug manufacturing enterprise produces medicinal sugar by directly utilizing sugarcane or sugar beet feedstock, general employing high-quality sugarcane is raw material, use and exchange cleaning technique and cook the technology such as sugar, microwave drying soon quickly, generally comprise sugarcane broken extraction of the juice, neutralization, precipitation, evaporate, boil the steps such as sugar, purging, drying, comminution by gas stream, dress bag, such as:
[title] a kind of medical cane sugar and production method thereof; [application number] CN00110458.6; [publication date] 2001-12-12; [summary] the present invention discloses a kind of medical cane sugar and production method thereof; this sucrose with high-quality sugarcane or beet for raw material; adopt advanced ion-exchange cleaning technique and cook the technology such as sugar, microwave drying soon quickly, producing a kind of sucrose meeting the physical and chemical index of pharmacopoeial requirements; A kind of sucrose powder of high-purity superfine that it is obtained through collision type Full-automatic air-flow disintegrating apparatus or the syrup of normal concentration.This novel medicinal sucrose not only meets physical and chemical index requirement under States Pharmacopoeia specifications item, and the specialized character had, and can produce provide convenience, can directly be used as medicine for pharmaceutical preparation, reduces costs, ensures the quality of products.
This method directly utilizing sugarcane or sugar beet feedstock to produce medical cane sugar, can reduce intermediate links in circulation, reduction cost of drugs, but equipment, technique are all quite complicated, at the direct abrasive dust of production line, sugared moisture-sensitive caking after dress bag, microorganism easily exceeds standard, and the less stable of medicinal sugar.
Current carbonatation process is widely used and produces sucrose, adopts sugarcane or beet to be raw material, with milk of lime, CO
2as finings removing impurity, through operations such as twice full charge, filtration, heating, reach purification effect high, make the object of sugarcane juice energy fast processing, but gained sucrose does not reach the standard of medicinal sugar, such as:
The improving technique of [title] a kind of clarifying sugar juice by carbonation method, [patent No.] CN200910114022.X, [publication date] 2009-09-23, the improving technique of [summary] a kind of clarifying sugar juice by carbonation method, first adds milk of lime by syrup to be clarified or calcium hydroxide must add lye to pH 10.8-11.8; Carry out first time full charge to pH 9.7-11 with carbon dioxide afterwards, solid-liquid separation obtains a clear juice; Carry out second time full charge with carbon dioxide again and obtain two carbon juice to pH 7.8-8.4, refilter with post-heating during two carbon juice are first and obtain subsider juice.The one-level or top grade white sugar that meet GB can be produced.Process of the present invention one ton of sugarcane uses CaO weight only to need 0.3 ~ 0.5%, and purity of clear juice improves 1 ~ 1.5, and the sulphur content of white sugar significantly reduces or not sulfur-bearing.And reduce 60 ~ 75% because of strong basicity filter mud amount, the organic ratio in filter mud is large, with in molasses alcohol waste liquid and after can be made into efficient organic fertilizer, thoroughly solve filter mud pollution problem.
But utilize the white sugar obtained by above-mentioned technique, the content of vitriol, residue on ignition, calcium salt, heavy metal PPM does not all reach the standard of medicinal sugar (Chinese Pharmacopoeia 2010 editions).
In sum, carbonatation process production technique can not directly utilize sugarcane or beet to produce medicinal sugar up to standard, and non-carbonatation process production technique exists again the problems such as industrial scale is little, complex process.Therefore existing medicinal sugared production technique, requires further improvement.
Summary of the invention
The invention solves conventional carbon acid technological process and produce the problem that sucrose does not reach medicinal Standard for Sugars, provide the improving technique that a kind of carbonatation process produces medicinal sugar.
The method of carbonatation process explained hereafter pharmaceutical excipient sucrose of the present invention, direct is raw material with sugarcane, the operation of broken-squeezing-peace and quiet-evaporate-boil sugar-purging-drying is adopted to obtain medical cane sugar, between described evaporation and Boiling Process, increase sulphur drift floating clustered operation together, concrete operation step is as follows:
(1) fragmentation of sugarcane: the sugarcane of strip is broken into sheet or thread sugarcane material.
(2) squeezing of sugarcane: the sugarcane material squeezing machine of fragmentation is squeezed.
(3) sugarcane juice is peace and quiet: with milk of lime, CO
2as finings, the sugar cane juice of squeezing gained is filled through pre-ash, mixing juice heating, a carbon bag first, a carbon heating, carbon filtrations, two carbon full charges, two carbon juice heating, two carbon filter, the clear drift of juice sulphur, clearly juice heat, the clear juice concentration obtained after clarify process is 12-14 ° of Bx, and pH value is 6.7.
(4) evaporation of sugarcane juice: clear juice enters evaporation section, and syrup moisture is condensed into 55-65 ° of Bx.
(5) sulphur drift floating clustered operation: sugarcane juice carries out Syrup Flotation again after over cure drift, wherein floating-upward process adds phosphoric acid and flocculation agent sulphur drift floating clustered operation: sugarcane juice carries out Syrup Flotation again after over cure drift, wherein floating-upward process adds phosphoric acid and flocculation agent, the clear juice pH value that sulphur drift obtains after floating and processing is 6.6, vitriol %<0.04, residue on ignition %<0.09, calcium salt %<0.02, heavy metal PPM<4.
(6) boil sugar: boiled by syrup, boil off moisture wherein, stay containing sucrose at soluble solids, make sugared grain or Icing Sugar.
(7) purging: the Crystallization Separation of the molasses boiled in the massecuite of sugared gained and sugar is opened.
(8) drying of sugar: under lower than the boiling temperature of water by the micro-moisture contained in material except going to medical cane sugar.
Further illustrate as to of the present invention, the described sugarcane broken condition of step (1) is when the sugarcane stem field brix of sugarcane reaches 20% or Sucrose reaches more than 13%, can cut after receipts remove leaf, the tip, root and can carry out break process.
Further illustrate as to of the present invention, step (7) purging process adopts the full-automatic sugar centrifuge of stainless steel scraper.
Sulphur drift floating clustered operation, on the basis that conventional carbon acid system is produced, clear up every impurity in sucrose further, improve the lustration class of sucrose, make vitriol in sucrose, residue on ignition, calcium salt and heavy metal equal size reach the index request of Chinese Pharmacopoeia 2010 editions; And carbonatation process in-house facility require just not high, technique simple, be very applicable to scale operation sucrose, also solve the problem that medical cane sugar is difficult to large-scale production like this.
Accompanying drawing explanation
Fig. 1 is process flow sheet of the present invention.
Embodiment
Below in conjunction with accompanying drawing and preferred embodiment, the method for the carbonatation process explained hereafter pharmaceutical excipient sucrose of invention is described further.The method of carbonatation process explained hereafter pharmaceutical excipient sucrose of the present invention, between the evaporation and Boiling Process of conventional carbon acid system, mainly increase sulphur drift floating clustered operation together, step is as follows:
(1) sugarcane raw material source: can cut receipts, the impurity such as leaf of pruning, the tip and root when the sugarcane stem field brix of sugarcane reaches 20% or Sucrose reaches more than 13.00%, delivers to sugar refinery processing, as the raw material of sugaring.
(2) fragmentation of sugarcane: sugarcane must carry out break process before entering squeezing machine, was called pre-treatment.Pretreated object is that the sugarcane of strip is broken into sheet or thread sucrose, and the fibrous tissue of sugarcane is torn, and sugar cell fully breaks.
(3) squeezing of sugarcane: cane milling is exactly squeezed by pretreated sugarcane material squeezing machine, extrudes the process of sugarcane juice.
(4) sugarcane juice is peace and quiet: with milk of lime, CO
2as finings, the sugar cane juice of squeezing gained is filled through pre-ash, mixing juice heating, a carbon bag first, a carbon heating, carbon filtrations, two carbon full charges, two carbon juice heating, two carbon filter, the clear drift of juice sulphur, clearly juice heat, the clear juice concentration obtained after clarify process is 12-14 ° of Bx, and pH value is 6.7.
(5) evaporation of sugarcane juice: the clear juice concentration that sugarcane juice obtains after clarify process is 12-14 ° of Bx(and moisture 86%-88%).If the dilute juice containing large quantity of moisture is directly sent to crystallization, a large amount of steam will be consumed, so namely consume the energy, extend again the time of boiling sugar.Therefore, clear juice has to pass through evaporation section, removes a large amount of moisture, is condensed into the syrup (60 ° of Bx best results) of 55-65 ° of about Bx, just can carries out crystallization.
(6) sulphur drift floating clustered operation: sugarcane juice carries out Syrup Flotation again after over cure drift, wherein floating-upward process adds phosphoric acid and flocculation agent, the clear juice pH value that sulphur drift obtains after floating and processing is 6.6, vitriol %<0.04, residue on ignition %<0.09, calcium salt %<0.02, heavy metal PPM<4;
(7) boil sugar: boiled by syrup, boil off moisture wherein, stay containing sucrose at soluble solids, make sugared grain or Icing Sugar.
(8) purging: the Crystallization Separation of the molasses boiled in the massecuite of sugared gained and sugar is opened.
(9) drying of sugar: generally, the moisture of the sugar after purging also containing 0.5%-1.5%, has to pass through fully dry and cooling, could fill bag and storage.Its principle is exactly the micro-moisture removing that will contain in material under lower than the boiling temperature of water.The drying of granulated sugar, is be medium with air substantially, makes air flow through granulated sugar surface, thus is taken away by moisture contained in granulated sugar.
(10) dried granulated sugar is sieved, weighs, packs and puts in storage.
Embodiment
Utilize the method for carbonatation process explained hereafter pharmaceutical excipient sucrose of the present invention, the operation being adopted by sugarcane broken-squeezing-peace and quiet-evaporation-sulphur drift floating combine-to boil sugar-purging-drying obtains medical cane sugar.
Wherein sulphur drift floating clustered operation: sugarcane juice carries out Syrup Flotation again after over cure drift, and wherein floating-upward process adds phosphoric acid and flocculation agent, the clear juice obtained after the process of sulphur drift floating.Gained sucrose, residue on ignition %<0.09, calcium salt %<0.02, heavy metal PPM<4.
Utilize the Comparison of standards situation of carbonatation process explained hereafter pharmaceutical excipient sucrose of the present invention and Chinese Pharmacopoeia 2010 editions.
| Project | Product of the present invention | Medical cane sugar |
| Sucrose (%) >= | 99.7 | 99.6 (by specific optical rotation conversions) |
| Reducing sugar content (%)≤ | 0.08 | 0.10 |
| Vitriol % < | 0.04 | 0.05 |
| Residue on ignition % < | 0.09 | 0.1 |
| Calcium salt % < | 0.02 | 0.05 |
| Heavy metal PPM < | 4 | 5 |
Above test-results shows, of the present inventionly utilizes carbonatation process explained hereafter pharmaceutical excipient sucrose of the present invention to reach the index request of Chinese Pharmacopoeia 2010 editions completely.
Claims (3)
1. the method for a carbonatation process explained hereafter pharmaceutical excipient sucrose, direct is raw material with sugarcane, the operation of broken-squeezing-peace and quiet-evaporate-boil sugar-purging-drying is adopted to obtain medical cane sugar, it is characterized in that: between described evaporation and Boiling Process, increase sulphur drift floating clustered operation together, concrete operation step is as follows:
(1) fragmentation of sugarcane: the sugarcane of strip is broken into sheet or thread sugarcane material;
(2) squeezing of sugarcane: the sugarcane material squeezing machine of fragmentation is squeezed;
(3) sugarcane juice is peace and quiet: with milk of lime, CO
2as finings, the sugar cane juice of squeezing gained is filled through pre-ash, mixing juice heating, a carbon bag first, a carbon heating, carbon filtrations, two carbon full charges, two carbon juice heating, two carbon filter, the clear drift of juice sulphur, clearly juice heat, the clear juice concentration obtained after clarify process is 12-14 ° of Bx, and pH value is 6.7;
(4) evaporation of sugarcane juice: clear juice enters evaporation section, and syrup moisture is condensed into 55-65 ° of Bx;
(5) sulphur drift floating clustered operation: sugarcane juice carries out Syrup Flotation again after over cure drift, wherein floating-upward process adds phosphoric acid and flocculation agent, the clear juice pH value that sulphur drift obtains after floating and processing is 6.6, vitriol %<0.04, residue on ignition %<0.09, calcium salt %<0.02, heavy metal PPM<4;
(6) boil sugar: boiled by syrup, boil off moisture wherein, stay containing sucrose at soluble solids, make sugared grain or Icing Sugar;
(7) purging: the Crystallization Separation of the molasses boiled in the massecuite of sugared gained and sugar is opened;
(8) drying of sugar: under lower than the boiling temperature of water by the micro-moisture contained in material except going to medical cane sugar.
2. the method for carbonatation process explained hereafter pharmaceutical excipient sucrose according to claim 1, it is characterized in that: step (1) sugarcane broken condition be when the sugarcane stem field brix of sugarcane reach 20% or Sucrose reach more than 13%, can cut after receipts remove leaf, the tip, root and can carry out break process.
3. the method for carbonatation process explained hereafter pharmaceutical excipient sucrose according to claim 1 and 2, is characterized in that: step (7) purging process adopts the full-automatic sugar centrifuge of stainless steel scraper.
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107475465A (en) * | 2017-09-06 | 2017-12-15 | 云南九吉公农业发展有限公司 | A kind of brown sugar processing technology |
| CN107604103A (en) * | 2017-10-31 | 2018-01-19 | 南宁市桂润环境工程有限公司 | A kind of method for eliminating heavy metal in sugarcane |
| CN108330217A (en) * | 2017-12-26 | 2018-07-27 | 白教法 | Complete sugarcane band leaf band tip squeezing sugaring clarifies production technology without sulphur |
| CN109182612A (en) * | 2018-08-30 | 2019-01-11 | 安徽珠峰生物科技有限公司 | A kind of detection method for extracting fructose and fructose content from hawthorn |
| CN112029912A (en) * | 2020-09-17 | 2020-12-04 | 宜章县丰乐古方红糖有限公司 | Brown sugar making process combining ancient method with modern method |
| CN114292965A (en) * | 2021-12-29 | 2022-04-08 | 米易华森糖业有限责任公司 | Preparation method of ecological brown sugar |
-
2014
- 2014-12-22 CN CN201410797420.7A patent/CN104611473A/en active Pending
Non-Patent Citations (3)
| Title |
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| 广东化工学院制糖教研组: "《甘蔗制糖技术_下》", 31 December 1977 * |
| 许广球等: "赤砂糖回溶糖浆硫熏中和上浮脱色工艺研究", 《甘蔗糖业》 * |
| 黄广盛等: "《甘蔗制糖工艺学》", 31 October 1991, 中国轻工业出版社 * |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107475465A (en) * | 2017-09-06 | 2017-12-15 | 云南九吉公农业发展有限公司 | A kind of brown sugar processing technology |
| CN107604103A (en) * | 2017-10-31 | 2018-01-19 | 南宁市桂润环境工程有限公司 | A kind of method for eliminating heavy metal in sugarcane |
| CN108330217A (en) * | 2017-12-26 | 2018-07-27 | 白教法 | Complete sugarcane band leaf band tip squeezing sugaring clarifies production technology without sulphur |
| CN109182612A (en) * | 2018-08-30 | 2019-01-11 | 安徽珠峰生物科技有限公司 | A kind of detection method for extracting fructose and fructose content from hawthorn |
| CN112029912A (en) * | 2020-09-17 | 2020-12-04 | 宜章县丰乐古方红糖有限公司 | Brown sugar making process combining ancient method with modern method |
| CN114292965A (en) * | 2021-12-29 | 2022-04-08 | 米易华森糖业有限责任公司 | Preparation method of ecological brown sugar |
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