CN104605443B - Quininic acid extract in a kind of Cranberry - Google Patents
Quininic acid extract in a kind of Cranberry Download PDFInfo
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- CN104605443B CN104605443B CN201510080156.XA CN201510080156A CN104605443B CN 104605443 B CN104605443 B CN 104605443B CN 201510080156 A CN201510080156 A CN 201510080156A CN 104605443 B CN104605443 B CN 104605443B
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- cranberry
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- 235000002118 Vaccinium oxycoccus Nutrition 0.000 title claims abstract description 51
- 244000291414 Vaccinium oxycoccus Species 0.000 title claims abstract description 51
- 235000012545 Vaccinium macrocarpon Nutrition 0.000 title claims abstract description 49
- 235000004634 cranberry Nutrition 0.000 title claims abstract description 49
- XXLFLUJXWKXUGS-UHFFFAOYSA-N 6-methoxyquinoline-4-carboxylic acid Chemical compound N1=CC=C(C(O)=O)C2=CC(OC)=CC=C21 XXLFLUJXWKXUGS-UHFFFAOYSA-N 0.000 title claims abstract description 48
- 238000000108 ultra-filtration Methods 0.000 claims abstract description 63
- 239000000706 filtrate Substances 0.000 claims abstract description 43
- 238000000926 separation method Methods 0.000 claims abstract description 26
- 235000012489 doughnuts Nutrition 0.000 claims abstract description 24
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims abstract description 19
- 235000015203 fruit juice Nutrition 0.000 claims abstract description 9
- 235000021022 fresh fruits Nutrition 0.000 claims abstract description 8
- 238000005507 spraying Methods 0.000 claims abstract description 6
- 239000012528 membrane Substances 0.000 claims description 32
- 230000004907 flux Effects 0.000 claims description 20
- 239000002253 acid Substances 0.000 claims description 3
- 230000007613 environmental effect Effects 0.000 abstract description 2
- 239000003960 organic solvent Substances 0.000 abstract description 2
- 238000000034 method Methods 0.000 description 4
- 235000013399 edible fruits Nutrition 0.000 description 3
- 238000000605 extraction Methods 0.000 description 3
- 238000004128 high performance liquid chromatography Methods 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- 241000609610 Gaylussacia Species 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 1
- 244000169938 Empetrum nigrum Species 0.000 description 1
- 235000012778 Empetrum nigrum Nutrition 0.000 description 1
- 235000012511 Vaccinium Nutrition 0.000 description 1
- 241000736767 Vaccinium Species 0.000 description 1
- 235000021028 berry Nutrition 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000003415 peat Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 241000894007 species Species 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/02—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
- A23L2/04—Extraction of juices
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/02—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
- A23L2/08—Concentrating or drying of juices
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/70—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
- A23L2/72—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter by filtration
- A23L2/74—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter by filtration using membranes, e.g. osmosis, ultrafiltration
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Water Supply & Treatment (AREA)
- Preparation Of Fruits And Vegetables (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses quininic acid extract in a kind of Cranberry, adopt following steps to prepare: (1), get Cranberry fresh fruit and squeeze, obtains fruit juice; And the concentrated Cranberry inspissated juice that obtains; (2), to use molecular cut off be 160000Da, and doughnut formula milipore filter carries out one-level ultra-filtration and separation to Cranberry inspissated juice, obtains filtrate I; (3), to use molecular cut off be 100000Da, and doughnut formula milipore filter carries out two-stage ultrafiltering separation to described filtrate I, obtains filtrate I I; (4), to use molecular cut off be 5000Da, and doughnut formula milipore filter carries out three grades of ultra-filtration and separation to described filtrate I I, obtains filtrate I II; (5), to use molecular cut off be 1000Da, and doughnut formula milipore filter carries out level Four ultra-filtration and separation to described filtrate I II, obtains filtrate I V; (6), by concentrated described filtrate I V, after spraying is dry, prepare Cranberry quininic acid extract. The present invention does not need extra organic solvent, more environmental protection.
Description
Technical field
The present invention relates to effective ingredients in plant extractive technique, particularly in a kind of Cranberry, quininic acid is carriedGet thing.
Background technology
Cranberry, claims again mossberry, cranberry, european cranberry, English name (Cranberry), its nameClaim to derive from former title " the crane certain kind of berries ", the head and the mouth that resemble very much crane because of the flower of Cranberry are gained the name. It is azaleaBeing commonly called as of section's Vaccinium crowberry subgenus (formal name used at school: Oxycoccos has another name called littlefruit craneberry subgenus), thisThe species of subgenus are evergreen shrubs, are mainly grown in the nice and cool area acid peat soil earth in the Northern HemisphereIn. Flower rediance, raceme.
Though Cranberry originates in North America, to cultivate successfully in China at present, its industrialization is planted in a few daysCan treat; Also there are the natural resources of other huckleberry plants in China in addition, therefore from huckleberry plant, outstandingIt is in Cranberry, to extract quininic acid to have wide market prospects.
Summary of the invention
Technical problem to be solved of the present invention is to provide quininic acid extract in a kind of Cranberry, thisInvention adopts membrane separation process to extract and purifying Cranberry inspissated juice, prepares Cranberry KuiPeaceful acid extractants thing; In the extract that the present invention prepares, quininic acid purity is higher, and purity reaches20.0％-22.0％。
The present invention solves the problems of the technologies described above adopted technical scheme:
Quininic acid extract in a kind of Cranberry, adopts following steps to prepare:
Step (1), get Cranberry fresh fruit and squeeze, obtain fruit juice; And by described concentration of juices extremely10 ° of Brix-15 ° of Brix, prepare Cranberry inspissated juice;
Step (2), one-level ultrafiltration: use the doughnut formula that molecular cut off is 160000Da superThe Cranberry inspissated juice that filter membrane prepares described step (1) carries out one-level ultra-filtration and separation,To filtrate I, ultrafiltration condition: pressure 0.2MPa, 40～50 DEG C of temperature; Membrane flux be 450 liters/littleTime;
Step (3), two-stage ultrafiltering: use the doughnut formula that molecular cut off is 100000Da superThe filtrate I that filter membrane prepares described step (2) is carried out two-stage ultrafiltering separation, obtains filter liquorII, ultrafiltration condition: pressure 0.4MPa, 40～50 DEG C of temperature; Membrane flux is 400 ls/h;
Step (4), three grades of ultrafiltration: use the doughnut formula ultrafiltration that molecular cut off is 5000DaThe filtrate I I that film obtains described step (3) carries out three grades of ultra-filtration and separation, obtains filtrate I II,Ultrafiltration condition: pressure 0.8MPa, 40～50 DEG C of temperature; Membrane flux is 350 ls/h;
Step (5), level Four ultrafiltration: use the doughnut formula ultrafiltration that molecular cut off is 1000DaThe filtrate I II that film obtains described step (3) carries out level Four ultra-filtration and separation, obtains filtrate I V,Ultrafiltration condition: pressure 1.0Mpa, 40～50 DEG C of temperature; Membrane flux is 200 ls/h;
Step (6), described filtrate I V is concentrated, after spraying is dry, prepares the present inventionDescribed Cranberry quininic acid extract.
In described step (1), get Cranberry fresh fruit and squeeze, obtain fruit juice; And by described fruitJuice is concentrated into 15 ° of Brix, prepares Cranberry inspissated juice.
In described step (6), described spray-dired design parameter is: 180 DEG C-210 of EATsDEG C, 80 DEG C-110 DEG C of leaving air temps.
" squeezing " of the present invention refers to and adopts squeezer of the prior art or juice extractor to carry out machinerySqueezing.
Compared with prior art, tool has the following advantages in the present invention:
(1) the present invention adopts membrane separation process to extract and purifying Cranberry inspissated juice, preparationObtain Cranberry quininic acid extract; Have compared with art methods raw material processing be more prone to,The features such as extraction efficiency is high, cost is low, are suitable for suitability for industrialized production.
(2) in the extract that the inventive method prepares, quininic acid purity is higher, and purity reaches20.0％-22.0％。
(3) the inventive method has improved extraction efficiency, has shortened extraction time.
(4) the present invention does not need extra organic solvent, more environmental protection.
Detailed description of the invention
Below, by specific embodiment, the present invention is described in further detail.
Embodiment 1:
Step (1), get 10kg Cranberry fresh fruit and squeeze, obtain fruit juice; And by described fruit juiceBe concentrated into 15 ° of Brix, prepare Cranberry inspissated juice;
Step (2), one-level ultrafiltration: use the doughnut formula that molecular cut off is 160000Da superThe Cranberry inspissated juice that filter membrane prepares described step (1) carries out one-level ultra-filtration and separation,To filtrate I, ultrafiltration condition: pressure 0.2MPa, temperature 45 C; Membrane flux is 450 ls/h;
Step (3), two-stage ultrafiltering: use the doughnut formula that molecular cut off is 100000Da superThe filtrate I that filter membrane prepares described step (2) is carried out two-stage ultrafiltering separation, obtains filter liquorII, ultrafiltration condition: pressure 0.4MPa, temperature 45 C; Membrane flux is 400 ls/h;
Step (4), three grades of ultrafiltration: use the doughnut formula ultrafiltration that molecular cut off is 5000DaThe filtrate I I that film obtains described step (3) carries out three grades of ultra-filtration and separation, obtains filtrate I II,Ultrafiltration condition: pressure 0.8MPa, temperature 45 C; Membrane flux is 350 ls/h;
Step (5), level Four ultrafiltration: use the doughnut formula ultrafiltration that molecular cut off is 1000DaThe filtrate I II that film obtains described step (3) carries out level Four ultra-filtration and separation, obtains filtrate I V,Ultrafiltration condition: pressure 1.0MPa, temperature 45 C; Membrane flux is 200 ls/h;
Step (6), described filtrate I V is concentrated into proportion 10 (B measurement), spraying is dryAfter, prepare 0.8kg Cranberry quininic acid extract. Described spray-dired design parameter is:180 DEG C of EATs, 80 DEG C of leaving air temps.
Measure through HPLC, in final Cranberry quininic acid extract, the purity of quininic acid is 20.2%.
Embodiment 2:
Step (1), get 10kg Cranberry fresh fruit and squeeze, obtain fruit juice; And by described fruit juiceBe concentrated into 13 ° of Brix, prepare Cranberry inspissated juice;
Step (2), one-level ultrafiltration: use the doughnut formula that molecular cut off is 160000Da superThe Cranberry inspissated juice that filter membrane prepares described step (1) carries out one-level ultra-filtration and separation,To filtrate I, ultrafiltration condition: pressure 0.2MPa, temperature 45 C; Membrane flux is 450 ls/h;
Step (3), two-stage ultrafiltering: use the doughnut formula that molecular cut off is 100000Da superThe filtrate I that filter membrane prepares described step (2) is carried out two-stage ultrafiltering separation, obtains filter liquorII, ultrafiltration condition: pressure 0.4MPa, temperature 45 C; Membrane flux is 400 ls/h;
Step (4), three grades of ultrafiltration: use the doughnut formula ultrafiltration that molecular cut off is 5000DaThe filtrate I I that film obtains described step (3) carries out three grades of ultra-filtration and separation, obtains filtrate I II,Ultrafiltration condition: pressure 0.8MPa, temperature 45 C; Membrane flux is 350 ls/h;
Step (5), level Four ultrafiltration: use the doughnut formula ultrafiltration that molecular cut off is 1000DaThe filtrate I II that film obtains described step (3) carries out level Four ultra-filtration and separation, obtains filtrate I V,Ultrafiltration condition: pressure 1.0MPa, temperature 45 C; Membrane flux is 200 ls/h;
Step (6), described filtrate I V is concentrated into proportion 11 (B measurement), spraying is dryAfter, prepare 0.7kg Cranberry quininic acid extract. Described spray-dired design parameter is:200 DEG C of EATs, 100 DEG C of leaving air temps.
Measure through HPLC, in final Cranberry quininic acid extract, the purity of quininic acid is 22.2%.
Embodiment 3:
Step (1), get 10kg Cranberry fresh fruit and squeeze, obtain fruit juice; And by described fruit juiceBe concentrated into 10 ° of Brix, prepare Cranberry inspissated juice;
Step (2), one-level ultrafiltration: use the doughnut formula that molecular cut off is 160000Da superThe Cranberry inspissated juice that filter membrane prepares described step (1) carries out one-level ultra-filtration and separation,To filtrate I, ultrafiltration condition: pressure 0.2MPa, temperature 45 C; Membrane flux is 450 ls/h;
Step (3), two-stage ultrafiltering: use the doughnut formula that molecular cut off is 100000Da superThe filtrate I that filter membrane prepares described step (2) is carried out two-stage ultrafiltering separation, obtains filter liquorII, ultrafiltration condition: pressure 0.4MPa, temperature 45 C; Membrane flux is 400 ls/h;
Step (4), three grades of ultrafiltration: use the doughnut formula ultrafiltration that molecular cut off is 5000DaThe filtrate I I that film obtains described step (3) carries out three grades of ultra-filtration and separation, obtains filtrate I II,Ultrafiltration condition: pressure 0.8MPa, temperature 45 C; Membrane flux is 350 ls/h;
Step (5), level Four ultrafiltration: use the doughnut formula ultrafiltration that molecular cut off is 1000DaThe filtrate I II that film obtains described step (3) carries out level Four ultra-filtration and separation, obtains filtrate I V,Ultrafiltration condition: pressure 1.0MPa, temperature 45 C; Membrane flux is 200 ls/h;
Step (6), described filtrate I V is concentrated into proportion 12 (B measurement), spraying is dryAfter, prepare 0.75kg Cranberry quininic acid extract. Described spray-dired design parameter is:210 DEG C of EATs, 100 DEG C of leaving air temps.
Measure through HPLC, in final Cranberry quininic acid extract, the purity of quininic acid is 21.5%.
As mentioned above, just can realize preferably the present invention.
Claims (3)
1. a quininic acid extract in Cranberry, is characterized in that, adopts following steps to be prepared intoArrive:
Step (1), get Cranberry fresh fruit and squeeze, obtain fruit juice; And by described concentration of juices extremely10 ° of Brix-15 ° of Brix, prepare Cranberry inspissated juice;
Step (2), one-level ultrafiltration: use the doughnut formula that molecular cut off is 160000Da superThe Cranberry inspissated juice that filter membrane prepares described step (1) carries out one-level ultra-filtration and separation,To filtrate I, ultrafiltration condition: pressure 0.2MPa, 40～50 DEG C of temperature; Membrane flux be 450 liters/littleTime;
Step (3), two-stage ultrafiltering: use the doughnut formula that molecular cut off is 100000Da superThe filtrate I that filter membrane prepares described step (2) is carried out two-stage ultrafiltering separation, obtains filter liquorII, ultrafiltration condition: pressure 0.4MPa, 40～50 DEG C of temperature; Membrane flux is 400 ls/h;
Step (4), three grades of ultrafiltration: use the doughnut formula ultrafiltration that molecular cut off is 5000DaThe filtrate I I that film obtains described step (3) carries out three grades of ultra-filtration and separation, obtains filtrate I II,Ultrafiltration condition: pressure 0.8MPa, 40～50 DEG C of temperature; Membrane flux is 350 ls/h;
Step (5), level Four ultrafiltration: use the doughnut formula ultrafiltration that molecular cut off is 1000DaThe filtrate I II that film obtains described step (3) carries out level Four ultra-filtration and separation, obtains filtrate I V,Ultrafiltration condition: pressure 1.0MPa, 40～50 DEG C of temperature; Membrane flux is 200 ls/h;
Step (6), described filtrate I V is concentrated, after spraying is dry, prepares CranberryQuininic acid extract.
2. quininic acid extract in a kind of Cranberry as claimed in claim 1, is characterized in that instituteState in step (1), get Cranberry fresh fruit and squeeze, obtain fruit juice; And by described concentration of juicesTo 15 ° of Brix, prepare Cranberry inspissated juice.
3. quininic acid extract in a kind of Cranberry as claimed in claim 1, is characterized in that instituteState in step (6), described spray-dired design parameter is: 180 DEG C-210 DEG C of EATs, go out80 DEG C-110 DEG C of air temperatures.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510080156.XA CN104605443B (en) | 2015-02-13 | 2015-02-13 | Quininic acid extract in a kind of Cranberry |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510080156.XA CN104605443B (en) | 2015-02-13 | 2015-02-13 | Quininic acid extract in a kind of Cranberry |
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| CN104605443A CN104605443A (en) | 2015-05-13 |
| CN104605443B true CN104605443B (en) | 2016-05-11 |
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Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104592011B (en) * | 2015-02-13 | 2016-05-11 | 宁波杰顺生物科技有限公司 | The preparation method of quininic acid extract in a kind of Cranberry |
| CN111357899A (en) * | 2020-04-26 | 2020-07-03 | 上海楷达生物科技有限公司 | Extraction process of concentrated juice powder |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101343225A (en) * | 2008-08-26 | 2009-01-14 | 施树云 | Preparation method for high-purity di-coffee mesitoyl quinine acid compounds |
| WO2012001347A1 (en) * | 2010-06-29 | 2012-01-05 | Ucl Business Plc | Products with oral health benefits |
| CN103570545A (en) * | 2013-09-17 | 2014-02-12 | 南京师范大学 | Method for preparing caffeoylquinic acid from Artemisia umbrosa |
| CN103570534A (en) * | 2012-08-01 | 2014-02-12 | 泰州市新威化工有限公司 | Method for preparing caffeoylquinic acid |
| CN104546989A (en) * | 2014-12-15 | 2015-04-29 | 宁波杰顺生物科技有限公司 | Method for preparing cranberry extract and capsules thereof |
-
2015
- 2015-02-13 CN CN201510080156.XA patent/CN104605443B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101343225A (en) * | 2008-08-26 | 2009-01-14 | 施树云 | Preparation method for high-purity di-coffee mesitoyl quinine acid compounds |
| WO2012001347A1 (en) * | 2010-06-29 | 2012-01-05 | Ucl Business Plc | Products with oral health benefits |
| CN103570534A (en) * | 2012-08-01 | 2014-02-12 | 泰州市新威化工有限公司 | Method for preparing caffeoylquinic acid |
| CN103570545A (en) * | 2013-09-17 | 2014-02-12 | 南京师范大学 | Method for preparing caffeoylquinic acid from Artemisia umbrosa |
| CN104546989A (en) * | 2014-12-15 | 2015-04-29 | 宁波杰顺生物科技有限公司 | Method for preparing cranberry extract and capsules thereof |
Non-Patent Citations (2)
| Title |
|---|
| 奎尼酸生物合成的代谢工程;何华庆等;《中国生物工程杂志》;20051125(第11期);第57－61页 * |
| 茶提取液中的奎尼酸含量及其提取特性;高木满等;《福建茶叶》;20020430(第01期);第26－28页 * |
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