CN104587917B - A kind of optical infrared imaging zinc sulphide reactor - Google Patents
A kind of optical infrared imaging zinc sulphide reactor Download PDFInfo
- Publication number
- CN104587917B CN104587917B CN201510050376.8A CN201510050376A CN104587917B CN 104587917 B CN104587917 B CN 104587917B CN 201510050376 A CN201510050376 A CN 201510050376A CN 104587917 B CN104587917 B CN 104587917B
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- shaft
- inner support
- hydrogen sulfide
- zinc sulphide
- reactor
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J10/00—Chemical processes in general for reacting liquid with gaseous media other than in the presence of solid particles, or apparatus specially adapted therefor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G9/00—Compounds of zinc
- C01G9/08—Sulfides
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Catalysts (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The invention discloses a kind of optical infrared imaging zinc sulphide reactor, including kettle, rotate the shaft being installed on kettle, drive the motor that shaft rotates, described kettle includes still top, still body and bottom, this still top is provided with zinc sulfate and adds mouth, the bottom of bottom is provided with zinc sulphide export mouth, the bottom of this still body is provided with hydrogen sulfide inlet port and sulfuric acid outlet, the inside of described still body is fixed with inner support, the lower end of this shaft is rotated by auxiliary support axle sleeve and is installed on inner support, hydrogen sulfide flow channel it is provided with on this inner support, the upper and lower surface of inner support is provided with multiple and hydrogen sulfide flow channel UNICOM solarization air cap, the upstream end of this hydrogen sulfide flow channel connects with hydrogen sulfide inlet port.This zinc sulphide reactor can meet zinc sulfate and hydrogen sulfide directly generates zinc sulphide, and zinc sulphide formation speed meets normal production, it is not necessary to adds any catalyst, thus can prepare the zinc sulphide that purity is high.
Description
Technical field
The present invention relates to a kind of reactor, particularly relate to a kind of optical infrared imaging zinc sulphide and react
Still.
Background technology
Zinc sulphide has good optical property, can apply on infrared imaging.So at present for
The preparation of zinc sulphide does not the most use zinc sulfate and hydrogen sulfide, and its reason is the heavy of such zinc sulphide
Form sediment few, and add other catalyst and be difficult to take out in follow-up operation, thus cannot obtain pure
Degree solid cure zinc, therefore, current zinc sulphide reactor cannot meet zinc sulfate and hydrogen sulfide
Normal reaction.
Summary of the invention
The technical problem to be solved is: provide a kind of optical infrared imaging zinc sulphide anti-
Answering still, this zinc sulphide reactor can meet zinc sulfate and hydrogen sulfide directly generates zinc sulphide, sulfuration
Zinc formation speed meets normal production, it is not necessary to add any catalyst, thus it is high to prepare purity
Zinc sulphide.
For solving above-mentioned technical problem, the technical scheme is that a kind of optical infrared imaging is used
Zinc sulphide reactor, including kettle, rotates the shaft being installed on kettle, drives shaft rotation
The motor turned, described kettle includes still top, still body and bottom, and this still top is provided with zinc sulfate and adds
Mouthful, the bottom of bottom is provided with zinc sulphide export mouth, and the bottom of this still body is provided with hydrogen sulfide and enters
Mouth and sulfuric acid outlet, the inside of described still body is fixed with inner support, and the lower end of this shaft is passed through
Auxiliary support axle sleeve rotates and is installed on inner support, and this inner support is provided with hydrogen sulfide flow channel, interior
The upper and lower surface of support is provided with multiple and hydrogen sulfide flow channel UNICOM solarization air cap, should
The upstream end of hydrogen sulfide flow channel connects with hydrogen sulfide inlet port.
As the preferred scheme of one, described inner support includes being positioned at the supporting part at middle part and discrete sets
It is placed in the outside at least two pieces of scallop being connected with supporting part of supporting part, the side of being provided with on this supporting part
Just shaft rotates the centre bore installed, and each scallop is provided with some curved channels and extremely
A few radial passage, this radial passage, by equal for each curved channel UNICOM, described supporting part is arranged
Having an annular communicating passage, the radial passage of each scallop is all connected by this annular communicating passage
Logical, described solarization air cap all connects with each curved channel.
As the preferred scheme of one, the quantity of described scallop is two pieces, and described supporting part is circle
Shape supporting part.
As the preferred scheme of one, the center of described inner support is run through in the lower end of described shaft
Hole, the lower end of this shaft is fixed with stirring vane, and this stirring vane is positioned at the lower section of inner support.
As the preferred scheme of one, described reactor inwall, shaft outer surface and inner support
Outer surface is provided with polytetrafluorethylecoatings coatings.
As the preferred scheme of one, the top of described reactor is run through in the upper end of described shaft,
The top on described still top is installed with pedestal, and shaft is rotated by upper bearing (metal) and lower bearing and installs
On pedestal, this support being fixed with decelerator, this decelerator is installed between motor and shaft.
After have employed technique scheme, the effect of the present invention is: owing to this still top is provided with sulfuric acid
Zinc adds mouth, and the bottom of bottom is provided with zinc sulphide export mouth, and the bottom of this still body is provided with sulfuration
Hydrogen inlet port and sulfuric acid outlet, the inside of described still body is fixed with inner support, under this shaft
Hold to be rotated by auxiliary support axle sleeve and be installed on inner support, this inner support is provided with hydrogen sulfide flowing logical
Road, the upper and lower surface of inner support is provided with multiple and hydrogen sulfide flow channel UNICOM aeration
Hole, the upstream end of this hydrogen sulfide flow channel connects with hydrogen sulfide inlet port.So, zinc sulfate from
Top adds, and hydrogen sulfide gas then enters in inner support from hydrogen sulfide inlet port, and passes through sulphur
Changing and flow out from solarization air cap after hydrogen flow channel, such hydrogen sulfide breaks up that to be dispersed in zinc sulfate molten the most completely
In liquid, then the High Rotation Speed with shaft, so that solution of zinc sulfate is abundant with hydrogen sulfide gas
Contact, thus the precipitation of accelerated cure zinc, after having reacted, zinc sulphide is put from zinc sulphide export mouth
Going out to enter in washing kettle and wash, the accessory substance dilute sulfuric acid generated then enters recycling can and reclaims.Should
Zinc sulphide reactor can meet the reaction of zinc sulfate and hydrogen sulfide, improves the degree speed of zinc sulphide,
Without extra other catalyst that add, thus the purity obtaining zinc sulphide is high, and subsequent technique difficulty drops
Low.
Again owing to described inner support includes being positioned at the supporting part at middle part and discrete is arranged at outside supporting part
At least two pieces of scallop that portion is connected with supporting part, this supporting part are provided with and facilitate shaft to rotate
The centre bore installed, each scallop is provided with some curved channels and at least one and radially leads to
Road, this radial passage, by equal for each curved channel UNICOM, described supporting part is provided with an annular even
Circulation passage, the radial passage of each scallop is all connected by this annular communicating passage, described solarization air cap
All connecting with each curved channel, this inner support is rational in infrastructure, and shaft not only can play guiding
Support effect, but also use as aeration board, thus facilitate hydrogen sulfide aeration fully to connect with zinc sulfate
Touch reaction.
The centre bore of described inner support is run through again, under this shaft due to the lower end of described shaft
End is fixed with stirring vane, and this stirring vane is positioned at the lower section of inner support, and this stirring vane can be right
Solution of zinc sulfate below solarization air cap quickly stirs, and makes the zinc sulfate below inner support and sulfuration
Zinc is also fully contacted, and accelerates reaction.
The top of described reactor, the top on described still top is run through again due to the upper end of described shaft
Being installed with pedestal, shaft is rotated by upper bearing (metal) and lower bearing and is installed on pedestal, this machine
Being fixed with decelerator on Zuo, this decelerator is installed between motor and shaft, in shaft utilization
Bearing, lower bearing and inner support with gentle support, can meet the support of the High Rotation Speed of shaft
Requirement.
Accompanying drawing explanation
The present invention is further described with embodiment below in conjunction with the accompanying drawings.
Fig. 1 is the structural representation of the embodiment of the present invention；
Fig. 2 is the sectional view of inner support；
Fig. 3 is the front view of inner support；
In accompanying drawing: 1. still body 1；2. still top 2；3. shaft 3；4. stirring vane 4；5. inner support
5；51. radial passages 51；52. curved channels 52；53. solarization air caps 53；54. scallop 54；55.
Supporting part；56. annular communicating passage 56；57. centre bores 57；6. hydrogen sulfide inlet port 6；7. sulfuric acid
Outlet；8. zinc sulphide export mouth 8；9. zinc sulfate adds mouth 9；10. pressure relief opening 10；11. upper shaft
Hold；12. lower bearings；13. motors；14. decelerators；15. pedestals.
Detailed description of the invention
Below by specific embodiment, the present invention is described in further detail.
As shown in Figure 1, 2, 3, a kind of optical infrared imaging zinc sulphide reactor, including kettle,
Rotate the shaft 3 being installed on kettle, drive the motor 13 that shaft 3 rotates, described kettle
Including still top 2, still body 1 and bottom, the top on described still top 2 is installed with pedestal 15, institute
The top of described reactor is run through in the upper end stating shaft 3, and shaft 3 is by upper bearing (metal) 11 He
Lower bearing 12 rotates and is installed on pedestal 15, this support is fixed with decelerator 14, this decelerator
14 are installed between motor 13 and shaft 3, and the output shaft of motor 13 is defeated with decelerator 14
Entering axle to connect, the output shaft of decelerator 14 is connected by shaft coupling with shaft 3 upper end, thus
Realize the transmission of power.The centre bore 57 of described inner support 5 is run through in the lower end of described shaft 3,
The lower end of this shaft 3 is fixed with stirring vane 4, and this stirring vane 4 is positioned at inner support 5 times
Side.Described reactor inwall, shaft 3 outer surface and inner support 5 outer surface are provided with poly-
Tetrafluoroethene coating.The platy structure that preferably inner support 5 is all made up of polytetrafluoroethylene (PTFE).For
In avoiding the hydrogen sulfide being passed in kettle not react and causing kettle, pressure is excessive, on still top
It is provided with pressure relief opening 10, at this pressure relief opening 10, relief valve can be connected.
This still top 2 is provided with zinc sulfate and adds mouth 9, and the bottom of bottom is provided with zinc sulphide export mouth
8, the bottom of this still body 1 is provided with hydrogen sulfide inlet port 6 and sulfuric acid outlet 7, described still body 1
Inside be fixed with inner support 5, the lower end of this shaft 3 by auxiliary support axle sleeve rotate be installed in
On support 5, this inner support 5 is provided with hydrogen sulfide flow channel, the upper surface of inner support 5 and
Lower surface is provided with multiple and hydrogen sulfide flow channel UNICOM solarization air cap 53, and the flowing of this hydrogen sulfide is logical
The upstream end in road connects with hydrogen sulfide inlet port 6.
Wherein, as shown in Figure 2,3, described inner support 5 includes supporting part 55 He being positioned at middle part
The discrete outside at least two pieces of scallop 54 being connected with supporting part 55 of supporting part 55 that are arranged at, described
The quantity of scallop 54 is two pieces and is arranged symmetrically with, and described supporting part 55 is circular support portion 55,
It is provided with on this supporting part 55 and facilitates shaft 3 to rotate the centre bore 57 installed, each fan
Being provided with some curved channels 52 and at least one radial passage 51 in shape portion 54, this is the most logical
Road 51, by each equal UNICOM of curved channel 52, described supporting part 55 is provided with an annular connection
Passage 56, the radial passage 51 of each scallop 54 is all connected by this annular communicating passage 56,
Described solarization air cap 53 all connects with each curved channel 52, so, and the entrance of hydrogen sulfide flow channel
As long as end arranges an equal UNICOM of passage that can make within whole inner support 5, thus simplifies gas
Road.
Embodiment described above is only the description to the preferred embodiment of the present invention, not as to this
The restriction of invention scope, on the basis of designing spirit without departing from the present invention, to the technology of the present invention side
Various deformation that case is made and transformation, all should fall into the protection model that claims of the present invention determines
In enclosing.
Claims (5)
- null1. an optical infrared imaging zinc sulphide reactor，Including kettle、Rotate the shaft being installed on kettle，Drive the motor that shaft rotates，It is characterized in that: described kettle includes still top、Still body and bottom，This still top is provided with zinc sulfate and adds mouth，The bottom of bottom is provided with zinc sulphide export mouth，The bottom of this still body is provided with hydrogen sulfide inlet port and sulfuric acid outlet，The inside of described still body is fixed with inner support，The lower end of this shaft is rotated by auxiliary support axle sleeve and is installed on inner support，Hydrogen sulfide flow channel it is provided with on this inner support，The upper and lower surface of inner support is provided with multiple and hydrogen sulfide flow channel UNICOM solarization air cap，The upstream end of this hydrogen sulfide flow channel connects with hydrogen sulfide inlet port，Described inner support includes being positioned at the supporting part at middle part and discrete is arranged at the outside at least two pieces of scallop being connected with supporting part of supporting part，It is provided with on this supporting part and facilitates shaft to rotate the centre bore installed，Some curved channels and at least one radial passage it is provided with in each scallop，This radial passage is by equal for each curved channel UNICOM，An annular communicating passage it is provided with on described supporting part，The radial passage of each scallop is all connected by this annular communicating passage，Described solarization air cap all connects with each curved channel.
- 2. a kind of optical infrared imaging zinc sulphide reactor as described in claim 1, it is characterised in that: the quantity of described scallop is two pieces, and described supporting part is circular support portion.
- 3. a kind of optical infrared imaging zinc sulphide reactor as described in claim 2, it is characterised in that: the centre bore of described inner support is run through in the lower end of described shaft, and the lower end of this shaft is fixed with stirring vane, and this stirring vane is positioned at the lower section of inner support.
- 4. a kind of optical infrared imaging zinc sulphide reactor as described in claim 3, it is characterised in that: described reactor inwall, shaft outer surface and inner support outer surface are provided with polytetrafluorethylecoatings coatings.
- 5. a kind of optical infrared imaging zinc sulphide reactor as described in claim 4, it is characterized in that: the top of described reactor is run through in the upper end of described shaft, the top on described still top is installed with pedestal, shaft is rotated by upper bearing (metal) and lower bearing and is installed on pedestal, being fixed with decelerator on this pedestal, this decelerator is installed between motor and shaft.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510050376.8A CN104587917B (en) | 2015-01-30 | 2015-01-30 | A kind of optical infrared imaging zinc sulphide reactor |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510050376.8A CN104587917B (en) | 2015-01-30 | 2015-01-30 | A kind of optical infrared imaging zinc sulphide reactor |
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| Publication Number | Publication Date |
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| CN104587917A CN104587917A (en) | 2015-05-06 |
| CN104587917B true CN104587917B (en) | 2016-08-17 |
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| CN201510050376.8A Active CN104587917B (en) | 2015-01-30 | 2015-01-30 | A kind of optical infrared imaging zinc sulphide reactor |
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Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107857292A (en) * | 2017-12-18 | 2018-03-30 | 张家港汇普光学材料有限公司 | A kind of zinc sulphide prepares production line |
| CN110550651A (en) * | 2019-07-09 | 2019-12-10 | 中化弘润石油化工有限公司 | Method for producing zinc sulfide by using acidic waste gas |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1443598A (en) * | 2002-03-11 | 2003-09-24 | 中国科学院过程工程研究所 | Surface aeration multiphase contact stirring equipment |
| CN201832643U (en) * | 2010-09-26 | 2011-05-18 | 铜陵市仕佰化工有限责任公司 | Ventilation reactor with mixing shaft with balancing air holes |
| CN201969557U (en) * | 2011-03-10 | 2011-09-14 | 张祯 | Hollow type ventilating agitator |
| CN102179227A (en) * | 2011-04-12 | 2011-09-14 | 浙江大学 | Airfoil type axial-flow stirrer |
| CN103302089A (en) * | 2013-07-01 | 2013-09-18 | 上海格林曼环境技术有限公司 | Integrated type multifunctional movable soil underground water repairing equipment and application thereof |
| CN104174350A (en) * | 2014-08-28 | 2014-12-03 | 张家港汇普光学材料有限公司 | High-speed stirring device of reaction kettle |
| CN203990639U (en) * | 2014-08-28 | 2014-12-10 | 张家港汇普光学材料有限公司 | A kind of reactor high-speed stirring apparatus |
| CN204447970U (en) * | 2015-01-30 | 2015-07-08 | 张家港汇普光学材料有限公司 | A kind of optical infrared imaging zinc sulphide reactor |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20070033863A1 (en) * | 2005-07-06 | 2007-02-15 | Butler Charles D | Method of producing biofuels, and related apparatus |
-
2015
- 2015-01-30 CN CN201510050376.8A patent/CN104587917B/en active Active
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1443598A (en) * | 2002-03-11 | 2003-09-24 | 中国科学院过程工程研究所 | Surface aeration multiphase contact stirring equipment |
| CN201832643U (en) * | 2010-09-26 | 2011-05-18 | 铜陵市仕佰化工有限责任公司 | Ventilation reactor with mixing shaft with balancing air holes |
| CN201969557U (en) * | 2011-03-10 | 2011-09-14 | 张祯 | Hollow type ventilating agitator |
| CN102179227A (en) * | 2011-04-12 | 2011-09-14 | 浙江大学 | Airfoil type axial-flow stirrer |
| CN103302089A (en) * | 2013-07-01 | 2013-09-18 | 上海格林曼环境技术有限公司 | Integrated type multifunctional movable soil underground water repairing equipment and application thereof |
| CN104174350A (en) * | 2014-08-28 | 2014-12-03 | 张家港汇普光学材料有限公司 | High-speed stirring device of reaction kettle |
| CN203990639U (en) * | 2014-08-28 | 2014-12-10 | 张家港汇普光学材料有限公司 | A kind of reactor high-speed stirring apparatus |
| CN204447970U (en) * | 2015-01-30 | 2015-07-08 | 张家港汇普光学材料有限公司 | A kind of optical infrared imaging zinc sulphide reactor |
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| CN104587917A (en) | 2015-05-06 |
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