CN104549076B - 一种粉末气溶胶发生器 - Google Patents

一种粉末气溶胶发生器 Download PDF

Info

Publication number
CN104549076B
CN104549076B CN201410825939.1A CN201410825939A CN104549076B CN 104549076 B CN104549076 B CN 104549076B CN 201410825939 A CN201410825939 A CN 201410825939A CN 104549076 B CN104549076 B CN 104549076B
Authority
CN
China
Prior art keywords
negative pressure
air
injector
powder
pressure cavity
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201410825939.1A
Other languages
English (en)
Other versions
CN104549076A (zh
Inventor
钱军
刘林娜
赵思言
禹忠全
陈权威
夏志平
郭振东
周博
王承宇
李忠义
黄耕
李乾学
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Institute of Military Veterinary Academy of Military Medical Sciences PLA
Original Assignee
Institute of Military Veterinary Academy of Military Medical Sciences PLA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Institute of Military Veterinary Academy of Military Medical Sciences PLA filed Critical Institute of Military Veterinary Academy of Military Medical Sciences PLA
Priority to CN201410825939.1A priority Critical patent/CN104549076B/zh
Publication of CN104549076A publication Critical patent/CN104549076A/zh
Application granted granted Critical
Publication of CN104549076B publication Critical patent/CN104549076B/zh
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • B01J13/0095Preparation of aerosols
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/30Mixing gases with solids
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/30Mixing gases with solids
    • B01F23/34Mixing gases with solids by introducing gases in solid materials, e.g. in masses of powder or particles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/70Spray-mixers, e.g. for mixing intersecting sheets of material
    • B01F25/72Spray-mixers, e.g. for mixing intersecting sheets of material with nozzles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/71Feed mechanisms
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002Chemical plants
    • B01J2219/00004Scale aspects
    • B01J2219/00006Large-scale industrial plants
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00162Controlling or regulating processes controlling the pressure
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/19Details relating to the geometry of the reactor
    • B01J2219/192Details relating to the geometry of the reactor polygonal

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Nozzles (AREA)

Abstract

一种粉末气溶胶发生器,包括空气压缩机、空气过滤器、干法分散仪以及分散喷头。其通过超声波高频振荡使加料漏斗中的粉末样品均匀进入分散漏斗,再通过高速压缩气体产生负压带动粉末粒子运动,在分散漏斗中搅拌、剪切、碰撞等方式充分分散,最后进入分散喷头,形成均匀的粉末气溶胶。本发明通过调节超声波振动频率、振幅大小、压缩气体压力、喷头孔径等参数,可产生直径为0.1~100μm,质量浓度为0.01-7g/m3的粉末气溶胶。该气溶胶发生器具有准确可靠、发生速度快、重复性好、操作简便等突出特点。

Description

一种粉末气溶胶发生器
技术领域
本发明属于流体力学技术领域,具体涉及一种粉末气溶胶发生器。
背景技术
气溶胶是固态或液态微粒悬浮于气体介质中所形成的分散系统。发生稳定且符合一定粒径分布的气溶胶是一项重要的气溶胶技术,它主要用于进行气溶胶实验研究、标定测量仪器以及开发和测试空气净化与采样设备等应用领域。
随着人类的发展以及科学技术的进步,环境污染问题逐渐突出,尤其近年来,我国北方地区经常遭受雾霾袭击。霾是一种特殊的粉末气溶胶。为了研究雾霾的相关性质以及危害性,在实验室内进行相关模拟实验至关重要。为此,开发稳定可靠的粉末气溶胶发生器成为环境科学以及生命科学领域的重要内容之一。
发明内容
本发明提供粉末气溶胶发生器,能产生颗粒分散度较好、粒径分布和浓度可调节的粉末气溶胶;该装置结构简单,操作维护方便,投资及维护费用低廉。
本发明提供的一种粉末气溶胶发生装置,包括空气压缩机、三级空气过滤器、干法分散仪和分散喷头。其中,干法分散仪包括主机箱、加料漏斗、超声振动器、进样器、分散漏斗、负压腔、气压调节阀、分散喷头和带推拉门的保护罩。空气压缩机通过管路连接到三级空气过滤器,三级空气过滤器出来的气体管路进入负压腔;加料漏斗的外面设有带推拉门的保护罩,防止灰尘进入加料漏斗。加料漏斗在进样器上方,槽状的进样器与超声振动器连接,超声振动器产生超声波高频振荡带动进样器匀速运动。分散漏斗的开口在进样器的末端下方,下端的出口与负压腔相通,分散漏斗接收从槽状的进样器滑下的气溶胶粉末,将气溶胶粉末带入负压腔,与负压腔内的高速气流发生作用。分散喷头在负压腔的管道一端,负压腔与三级空气过滤器之间设有气压调节阀。
本发明与现有技术相比,具有以下优点及突出性效果:本发明通过调节振动器振动频率和振幅大小、压缩气体压力、分散喷头孔径等参数,可产生直径为0.1~100μm,质量浓度为0.01-7g/m3的粉末气溶胶,可以完全满足各种设备检测和实验研究的需要。另外,本发明的所有操作程序均由电脑统一控制,按预设程序自动完成。本发明结构简单,操作方便,维护简单,投资及维护费用低。
附图说明
图1是本发明的结构示意图。
图2是粉末气溶胶与高速气流发生的作用力示意图。
图中:1空气压缩机;2三级空气过滤器;3主机箱;4推拉门;5保护罩;6加料漏斗;7超声振动器;8进样器;9分散漏斗;10负压腔;11气压调节阀;12分散喷头;13气体管路。
具体实施方式
如图所示,一种粉末气溶胶发生装置,主要由空气压缩机1、三级空气过滤器2、主机箱3、推拉门4、加料漏斗6、超声振动器7、进样器8、分散漏斗9、负压腔10、气压调节阀11、分散喷头12组成,其中主机箱、加料漏斗、超声振动器、进样器、分散漏斗、负压腔、气压调节阀、分散喷头和带推拉门的保护罩共同构成干法分散仪。空气压缩机通过管路连接到三级空气过滤器,三级空气过滤器出来的气体管路进入负压腔;加料漏斗的外面有带推拉门的保护罩。加料漏斗在进样器上方,槽状的进样器与超声振动器连接,超声振动器产生超声波高频振荡带动进样器匀速运动。分散漏斗的开口在进样器的末端下方,下端的出口与负压腔相通,分散漏斗接收从槽状的进样器滑下的气溶胶粉末,将气溶胶粉末带入负压腔,和负压腔内的高速气流发生作用。分散喷头在负压腔管道的一端,负压腔与三级空气过滤器之间设有气压调节阀。
粉末样品通过加料漏斗加入,超声振动器产生超声波高频振荡带动进样器,使样品从加料漏斗中均匀进入进样器,并按照一定速度均匀通过,落入分散漏斗。通过空气压缩机和三级空气过滤器产生压力为0.1MPa~0.4MPa的洁净压缩空气,通过气体管路进入负压腔;高速气流产生负压带动分散漏斗中的粉末运动,在分散漏斗中搅拌、剪切、碰撞等方式充分分散,再由气流产生的负压带动进入分散喷头,形成均匀的粉末气溶胶。

Claims (2)

1.一种粉末气溶胶发生装置,包括空气压缩机、三级空气过滤器、干法分散仪和分散喷头;其特征在于,其中,干法分散仪包括主机箱、加料漏斗、超声振动器、进样器、分散漏斗、负压腔、气压调节阀、分散喷头和带推拉门的保护罩;空气压缩机通过管路连接到三级空气过滤器,三级空气过滤器出来的气体管路进入负压腔;加料漏斗的外面设有带推拉门的保护罩,防止灰尘进入加料漏斗;加料漏斗在进样器上方,槽状的进样器与超声振动器连接,超声振动器产生超声波高频振荡带动进样器匀速运动;分散漏斗的开口在进样器的末端下方,下端的出口与负压腔相通,分散漏斗接收从槽状的进样器滑下的气溶胶粉末,将气溶胶粉末带入负压腔,与负压腔内的高速气流发生作用;分散喷头在负压腔的管道一端,负压腔与三级空气过滤器之间设有气压调节阀。
2.根据权利要求1所述的一种粉末气溶胶发生装置,其特征在于,空气压缩机和三级空气过滤器产生压力为0.1MPa~0.4MPa的洁净压缩空气。
CN201410825939.1A 2014-12-26 2014-12-26 一种粉末气溶胶发生器 Active CN104549076B (zh)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201410825939.1A CN104549076B (zh) 2014-12-26 2014-12-26 一种粉末气溶胶发生器

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201410825939.1A CN104549076B (zh) 2014-12-26 2014-12-26 一种粉末气溶胶发生器

Publications (2)

Publication Number Publication Date
CN104549076A CN104549076A (zh) 2015-04-29
CN104549076B true CN104549076B (zh) 2016-06-15

Family

ID=53066788

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201410825939.1A Active CN104549076B (zh) 2014-12-26 2014-12-26 一种粉末气溶胶发生器

Country Status (1)

Country Link
CN (1) CN104549076B (zh)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105372164B (zh) * 2015-12-11 2018-02-27 天津开发区合普工贸有限公司 自稀释气溶胶筛分标定装置
CN105944632B (zh) * 2016-07-11 2017-09-26 中国环境科学研究院 一种防止低流动性药物结块的粉末气溶胶发生器
CN107469728B (zh) * 2017-08-04 2020-08-14 上海交通大学 一种可控微量颗粒物加料装置及其使用方法
EP3743224A4 (en) 2017-11-21 2021-06-30 New Mexico Tech University Research Park Corporation AEROSOL PROCESS FOR COATING
CN108187514B (zh) * 2018-01-30 2021-03-23 中国科学院过程工程研究所 一种粉尘发生系统及其处理方法
CN112807127A (zh) * 2021-02-03 2021-05-18 军事科学院军事医学研究院军事兽医研究所 一种可控粒径气溶胶发生暴露装置

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102658039A (zh) * 2012-04-20 2012-09-12 哈尔滨工程大学 一种双筒多级流化循环型气溶胶发生装置
CN202860509U (zh) * 2012-09-28 2013-04-10 青岛众瑞智能仪器有限公司 一种dop气溶胶发生器
CN203525677U (zh) * 2013-08-02 2014-04-09 广西桂测科技有限公司 气溶胶发生器
CN204395794U (zh) * 2014-12-26 2015-06-17 中国人民解放军军事医学科学院军事兽医研究所 一种粉末气溶胶发生器

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7802569B2 (en) * 2005-12-22 2010-09-28 Kaer Biotherapeutics Corporation Aerosol processing and inhalation method and system for high dose rate aerosol drug delivery

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102658039A (zh) * 2012-04-20 2012-09-12 哈尔滨工程大学 一种双筒多级流化循环型气溶胶发生装置
CN202860509U (zh) * 2012-09-28 2013-04-10 青岛众瑞智能仪器有限公司 一种dop气溶胶发生器
CN203525677U (zh) * 2013-08-02 2014-04-09 广西桂测科技有限公司 气溶胶发生器
CN204395794U (zh) * 2014-12-26 2015-06-17 中国人民解放军军事医学科学院军事兽医研究所 一种粉末气溶胶发生器

Also Published As

Publication number Publication date
CN104549076A (zh) 2015-04-29

Similar Documents

Publication Publication Date Title
CN104549076B (zh) 一种粉末气溶胶发生器
Liu et al. Frequency comparative study of coal-fired fly ash acoustic agglomeration
Zhou et al. Experimental study on improving the efficiency of dust removers by using acoustic agglomeration as pretreatment
Zu et al. Modeling and experimental study on acoustic agglomeration for dust particle removal
CN206740587U (zh) Pm2.5切割器切割特性检测装置
CN204395794U (zh) 一种粉末气溶胶发生器
Khmelev et al. Effciency increase of the dust-extraction plant by high-intensity ultrasonic action
Kilikevičienė et al. Experimental investigation of acoustic agglomeration of diesel engine exhaust particles using new created acoustic chamber
Zhou et al. Preliminary experimental study of acoustic agglomeration of coal-fired fine particles
Zhang et al. A new model for the acoustic wake effect in aerosol acoustic agglomeration processes
CN102607789A (zh) 气锤式振动台的加速度控制方法以及装置
Amiri et al. Experimental parametric study of frequency and sound pressure level on the acoustic coagulation and precipitation of PM2. 5 aerosols
CN205055672U (zh) 移动式布袋除尘器
CN204086080U (zh) 微小固体颗粒气溶胶高精度稳恒标定装置
Chakravarty et al. Towards a theoretical understanding of dustiness
CN203663497U (zh) 填料色谱柱制备装置
CN201828501U (zh) 除尘滤料性能测试实验台用发尘器
Noorpoor et al. Influence of acoustic waves on deposition and coagulation of fine particles
CN103754587A (zh) 高稳定性细颗粒粉尘给料装置
CN104340410B (zh) 一种固态气溶胶实验供粉装置及供粉方法
CN203577657U (zh) 一种定量控制微粒径粘滞性粉尘扩散装置
CN106076053A (zh) 基于共振腔的分离式声团聚悬浮细颗粒减排系统
CN203916828U (zh) 立式磨粉机
Li et al. Improved Pulsed-Jet Cleaning of Pleated Cone Filter Cartridges Using a Diffusion Nozzle
Shen et al. Experimental study of acoustic agglomeration and fragmentation on coal-fired ash

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant