CN104477939B - 一种低压水解工艺 - Google Patents
一种低压水解工艺 Download PDFInfo
- Publication number
- CN104477939B CN104477939B CN201410593772.0A CN201410593772A CN104477939B CN 104477939 B CN104477939 B CN 104477939B CN 201410593772 A CN201410593772 A CN 201410593772A CN 104477939 B CN104477939 B CN 104477939B
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- Prior art keywords
- pressure
- ammonium
- stripper
- hydrolyzer
- gas
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 230000007062 hydrolysis Effects 0.000 title claims abstract description 26
- 238000006460 hydrolysis reaction Methods 0.000 title claims abstract description 26
- 238000005516 engineering process Methods 0.000 title abstract description 11
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims abstract description 35
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims abstract description 33
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims abstract description 32
- 239000007789 gas Substances 0.000 claims abstract description 25
- 239000000463 material Substances 0.000 claims abstract description 22
- 239000004202 carbamide Substances 0.000 claims abstract description 17
- 229910021529 ammonia Inorganic materials 0.000 claims abstract description 16
- 229910002092 carbon dioxide Inorganic materials 0.000 claims abstract description 16
- 239000001569 carbon dioxide Substances 0.000 claims abstract description 15
- 239000007788 liquid Substances 0.000 claims abstract description 14
- 239000002699 waste material Substances 0.000 claims abstract description 6
- 238000011084 recovery Methods 0.000 claims abstract description 5
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 46
- 239000012530 fluid Substances 0.000 claims description 35
- 235000013877 carbamide Nutrition 0.000 claims description 15
- 238000000034 method Methods 0.000 claims description 11
- 230000008569 process Effects 0.000 claims description 9
- 239000012071 phase Substances 0.000 claims description 8
- 210000002700 urine Anatomy 0.000 claims description 7
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 6
- 238000005260 corrosion Methods 0.000 claims description 6
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 5
- 229910052799 carbon Inorganic materials 0.000 claims description 5
- 239000007791 liquid phase Substances 0.000 claims description 5
- 238000003860 storage Methods 0.000 claims description 4
- JJEJDZONIFQNHG-UHFFFAOYSA-N [C+4].N Chemical compound [C+4].N JJEJDZONIFQNHG-UHFFFAOYSA-N 0.000 claims description 3
- 230000008676 import Effects 0.000 claims description 3
- 229910052756 noble gas Inorganic materials 0.000 claims description 3
- 150000002835 noble gases Chemical class 0.000 claims description 3
- 239000004408 titanium dioxide Substances 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 2
- 238000005265 energy consumption Methods 0.000 abstract description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 4
- 229910001868 water Inorganic materials 0.000 abstract description 4
- 238000010438 heat treatment Methods 0.000 abstract description 3
- 238000001816 cooling Methods 0.000 abstract description 2
- ATRRKUHOCOJYRX-UHFFFAOYSA-N Ammonium bicarbonate Chemical compound [NH4+].OC([O-])=O ATRRKUHOCOJYRX-UHFFFAOYSA-N 0.000 abstract 8
- 239000001099 ammonium carbonate Substances 0.000 abstract 8
- 235000012501 ammonium carbonate Nutrition 0.000 abstract 8
- BVCZEBOGSOYJJT-UHFFFAOYSA-N ammonium carbamate Chemical compound [NH4+].NC([O-])=O BVCZEBOGSOYJJT-UHFFFAOYSA-N 0.000 abstract 2
- KXDHJXZQYSOELW-UHFFFAOYSA-N carbonic acid monoamide Natural products NC(O)=O KXDHJXZQYSOELW-UHFFFAOYSA-N 0.000 abstract 2
- 238000007599 discharging Methods 0.000 abstract 1
- 239000011261 inert gas Substances 0.000 abstract 1
- 229910000069 nitrogen hydride Inorganic materials 0.000 abstract 1
- 229960004424 carbon dioxide Drugs 0.000 description 10
- 230000008859 change Effects 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 238000010521 absorption reaction Methods 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 230000003301 hydrolyzing effect Effects 0.000 description 2
- 241000790917 Dioxys <bee> Species 0.000 description 1
- 235000011114 ammonium hydroxide Nutrition 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910002090 carbon oxide Inorganic materials 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000011344 liquid material Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 238000006396 nitration reaction Methods 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 238000010025 steaming Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
Abstract
Description
Claims (3)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201410593772.0A CN104477939B (zh) | 2014-10-28 | 2014-10-28 | 一种低压水解工艺 |
Applications Claiming Priority (1)
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CN201410593772.0A CN104477939B (zh) | 2014-10-28 | 2014-10-28 | 一种低压水解工艺 |
Publications (2)
Publication Number | Publication Date |
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CN104477939A CN104477939A (zh) | 2015-04-01 |
CN104477939B true CN104477939B (zh) | 2017-01-18 |
Family
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN201410593772.0A Active CN104477939B (zh) | 2014-10-28 | 2014-10-28 | 一种低压水解工艺 |
Country Status (1)
Country | Link |
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CN (1) | CN104477939B (zh) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106365165A (zh) * | 2016-08-26 | 2017-02-01 | 安徽昊源化工集团有限公司 | 一种新型尿素水解工艺 |
CN110746324A (zh) * | 2019-09-24 | 2020-02-04 | 四川金象赛瑞化工股份有限公司 | 一种尿素生产低温、高效、节能低压分解工艺 |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0542792B1 (en) * | 1990-08-01 | 1995-11-08 | NALCO FUEL TECH GmbH | Process for the in-line hydrolysis of urea |
CN1858005A (zh) * | 2006-05-18 | 2006-11-08 | 刘国胜 | 尿素工艺冷凝液节能净化回收工艺 |
CN202576000U (zh) * | 2012-05-18 | 2012-12-05 | 河南骏化发展股份有限公司 | 一种尿素工艺冷凝液水解系统 |
CN103570588A (zh) * | 2013-08-30 | 2014-02-12 | 北京丰汉工程技术有限公司 | 一种尿素合成装置及合成方法 |
-
2014
- 2014-10-28 CN CN201410593772.0A patent/CN104477939B/zh active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0542792B1 (en) * | 1990-08-01 | 1995-11-08 | NALCO FUEL TECH GmbH | Process for the in-line hydrolysis of urea |
CN1858005A (zh) * | 2006-05-18 | 2006-11-08 | 刘国胜 | 尿素工艺冷凝液节能净化回收工艺 |
CN202576000U (zh) * | 2012-05-18 | 2012-12-05 | 河南骏化发展股份有限公司 | 一种尿素工艺冷凝液水解系统 |
CN103570588A (zh) * | 2013-08-30 | 2014-02-12 | 北京丰汉工程技术有限公司 | 一种尿素合成装置及合成方法 |
Non-Patent Citations (1)
Title |
---|
水解汽提技术在氨氮废水处理中的应用;田玉青;《中氮肥》;20050731(第4期);第24-25页 * |
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CN104477939A (zh) | 2015-04-01 |
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Denomination of invention: Low-pressure hydrolysis technology Effective date of registration: 20191012 Granted publication date: 20170118 Pledgee: Zhumadian Rural Commercial Bank Co.,Ltd. Pledgor: HENAN JUNHUA DEVELOPMENT Co.,Ltd. Registration number: Y2019980000247 |
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Date of cancellation: 20200522 Granted publication date: 20170118 Pledgee: Zhumadian Rural Commercial Bank Co.,Ltd. Pledgor: HENAN JUNHUA DEVELOPMENT Co.,Ltd. Registration number: Y2019980000247 |
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