CN104473808A - Sterilizing hand sanitizer and preparation method thereof - Google Patents
Sterilizing hand sanitizer and preparation method thereof Download PDFInfo
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- CN104473808A CN104473808A CN201410688633.6A CN201410688633A CN104473808A CN 104473808 A CN104473808 A CN 104473808A CN 201410688633 A CN201410688633 A CN 201410688633A CN 104473808 A CN104473808 A CN 104473808A
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Abstract
The invention discloses a sterilizing hand sanitizer, which comprises the following raw materials in parts by weight: 12 to 25 parts of alkyl phosphorus carboxylate, 7 to 10 parts of fat polyoxyethylene ether sodium vinyl ether sulfate, 5-10 parts of functional plant extract, 4 to 7 parts of glycerol, 1 to 4 parts of betaine, 0.5 to 3 parts of a pH adjusting agent and 50 to 70 parts of water. The invention also discloses a preparation method of the sterilizing hand sanitizer. The sterilizing hand sanitizer provided by the invention has the advantages of sterilizing and antibacterial effects and skin whitening effect.
Description
Technical field
The present invention relates to a kind of daily handwashing liquid, particularly relate to a kind of disinfection hand cleanser and preparation method thereof.
Background technology
Along with the raising day by day of people's living standard, people are no longer cleaning actions only to the demand of handwashing liquid, and also need handwashing liquid to have sterilization, effect of antibacterial and skin protection, many disinfection hand cleansers are there is on the market now, but its sterilization component safety is not high, after containing hypotoxic cleaning composition hands, by direct for hands contacting foodstuff, certain injury will be caused to people's health, therefore its safety is not high enough, although the safety of other handwashing liquid is high, but function is incomplete, preparation method is complicated, cost is high, general consumer can not accept.
It is CN103194338A that State Intellectual Property Office discloses a publication number on July 10th, 2013, the patent of invention that name is called " a kind of handwashing liquid and preparation method thereof ", and the percentage by weight of this patent component and each component is: soap base: 6-15%; Aliphatic acid polyethenoxy ether sodium sulfate: 6-10%; Dodecyldimethylammonium hydroxide inner salt: 2-5%; Cocoanut fatty acid diethanolamide: 2-5%; Essence: 0.01-0.5%; Pigment: 0.01-0.5% water: surplus; The preparation method of handwashing liquid is: a, the component of above-mentioned handwashing liquid be mixed in proportion; B, stirring be heated to 80-85 DEG C; Handwashing liquid finished product is obtained after c, cooling.Handwashing liquid provided by the invention and preparation method thereof, the handwashing liquid obtained cleans that dynamics is strong, performance is gentle.Although this patent has certain cleaning action, it sterilizes, fungistatic effect is good not, and not containing skin care ingredient, without moisturizing and skin Caring effect.
Summary of the invention
The present invention is intended to solve the sterilization of handwashing liquid in prior art, antipathogenic composition is few, and effect is bad, and does not have the problem of skin-protection and skin-makeup effect, proposes a kind of disinfection hand cleanser comprising functional plants extract.
In order to realize foregoing invention object, technical scheme of the present invention is as follows:
A kind of disinfection hand cleanser, is characterized in that: comprise following raw material by weight:
Alkyl phosphorus carboxylate 12 ~ 25 parts
7 ~ 10 parts, fatty polyoxyethylene esters sodium sulfate
Functional plants extract 5 ~ 10 parts
Glycerol 4 ~ 7 parts
Betanin 1 ~ 4 part
PH regulator 0.5 ~ 3 part
50 ~ 70 parts, water;
In above-mentioned formula, described functional plants extract is the mixture after being extracted by Fructus Forsythiae, Radix Glycyrrhizae, Radix Scutellariae, Radix Et Rhizoma Rhei, Flos Camelliae Japonicae fruit.
The preparation method of described functional plants extract, comprises the following steps:
A. decoct
The Fructus Forsythiae taken for 5:3:2:1:1 in mass ratio, Radix Glycyrrhizae, Radix Scutellariae, Radix Et Rhizoma Rhei, Flos Camelliae Japonicae fruit are added in container, then add the water of 40 ~ 50 DEG C, after soaking 1 ~ 1.5h, raised temperature decocts, under boiling state, after decocting 40 ~ 60min, filtering and collecting filter liquid, again plant residue is decocted, under boiling state, decoct 1 ~ 1.5h, again filter, and collect filtrate, finally the filtrate of twice is merged;
B. concentrate
Concentrate filtrate to the extractum that relative density is 1.3 ~ 1.38, after cooling, add the ethanol that concentration of volume percent is 70%, after static 12h, filter, after the leaching supernatant, reclaim ethanol, at 55 DEG C, be concentrated into relative density is after the extractum of 1.2 ~ 1.25, is drying to obtain functional plants extract.
Described water is deionized water.
The essence of 0.5 ~ 1 part and the pigment of 0.05 ~ 0.5 part can also be comprised in formula of the present invention.
The preparation method of the anti-bacterial hand lotion in the present invention is: in reaction vessel, add 2/3rds of the water taken by formula, after being warming up to 45 ~ 50 DEG C, add glycerol, after stirring, be cooled to 15 ~ 25 DEG C, add again by remaining 1/3rd water and the alkyl phosphorus carboxylate that takes by formula, fatty polyoxyethylene esters sodium sulfate, after betanin, continue to stir, mixing time is 15 ~ 20min, puddler rotating speed is 10 ~ 15r/min, finally add functional plants extract, after continuing stirring 5 ~ 8min, solution pH value is regulated to be after 7 ~ 8 with PH regulator, get product.
In said method, described adds glycerol, stirs, and the time of stirring is 5 ~ 10min, and the rotating speed of puddler is 20 r/min.
Described PH regulator is citric acid.
Beneficial effect of the present invention:
1, the present invention is compared with the conventional handwashing liquid of prior art; with the addition of surfactant; wetting agent, after emulsifying agent, also added plant extract; effect that each material in plant extract mixes together be make handwashing liquid have sterilization, antibacterial, on skin, form layer protecting film; from the invasion of the antibacterial in the external world, and the safety of plant extract and chemical bactericide is higher, and antibacterial can not develop immunity to drugs; bactericidal effect is more lastingly good, can life-time service.
The preparation method of the plant extract 2, in the present invention is gentle, carries out twice decoction, has extraction efficiency high, remain effective ingredient to greatest extent, thus makes sterilization, fungistatic effect the best of handwashing liquid.
Detailed description of the invention
Embodiment 1
A kind of disinfection hand cleanser, comprises following raw material by weight:
Alkyl phosphorus carboxylate 12 parts
7 parts, fatty polyoxyethylene esters sodium sulfate
Functional plants extract 5 parts
Glycerol 4 parts
Betanin 1 part
PH regulator 0.5 part
50 parts, water;
In above-mentioned formula, functional plants extract is the mixture after being extracted by Fructus Forsythiae, Radix Glycyrrhizae, Radix Scutellariae, Radix Et Rhizoma Rhei, Flos Camelliae Japonicae fruit.
Embodiment 2
A kind of disinfection hand cleanser, comprises following raw material by weight:
Alkyl phosphorus carboxylate 25 parts
10 parts, fatty polyoxyethylene esters sodium sulfate
Functional plants extract 10 parts
Glycerol 7 parts
Betanin 4 parts
PH regulator 3 parts
70 parts, water;
In this enforcement, functional plants extract is the mixture after being extracted by Fructus Forsythiae, Radix Glycyrrhizae, Radix Scutellariae, Radix Et Rhizoma Rhei, Flos Camelliae Japonicae fruit, and its preparation method, comprises the following steps:
A. decoct
The Fructus Forsythiae taken for 5:3:2:1:1 in mass ratio, Radix Glycyrrhizae, Radix Scutellariae, Radix Et Rhizoma Rhei, Flos Camelliae Japonicae fruit are added in container, then add the water of 40 DEG C, after soaking 1.5h, raised temperature decocts, under boiling state, after decocting 40min, filtering and collecting filter liquid, again plant residue is decocted, under boiling state, decoct 1h, again filter, and collect filtrate, finally the filtrate of twice is merged;
B. concentrate
Concentrate filtrate to the extractum that relative density is 1.3, after cooling, add the ethanol that concentration of volume percent is 70%, after static 12h, filter, after the leaching supernatant, reclaim ethanol, at 55 DEG C, be concentrated into relative density is after the extractum of 1.2, is drying to obtain functional plants extract.
Embodiment 3
A kind of disinfection hand cleanser, is characterized in that: comprise following raw material by weight:
Alkyl phosphorus carboxylate 20 parts
8 parts, fatty polyoxyethylene esters sodium sulfate
Functional plants extract 8 parts
Glycerol 5 parts
Betanin 3 parts
PH regulator 1 part
60 parts, water;
In the present embodiment, functional plants extract is the mixture after being extracted by Fructus Forsythiae, Radix Glycyrrhizae, Radix Scutellariae, Radix Et Rhizoma Rhei, Flos Camelliae Japonicae fruit, and its preparation method, comprises the following steps:
A. decoct
The Fructus Forsythiae taken for 5:3:2:1:1 in mass ratio, Radix Glycyrrhizae, Radix Scutellariae, Radix Et Rhizoma Rhei, Flos Camelliae Japonicae fruit are added in container, then add the water of 50 DEG C, after soaking 1h, raised temperature decocts, under boiling state, after decocting 60min, filtering and collecting filter liquid, again plant residue is decocted, under boiling state, decoct 1h, again filter, and collect filtrate, finally the filtrate of twice is merged;
B. concentrate
Concentrate filtrate to the extractum that relative density is 1.38, after cooling, add the ethanol that concentration of volume percent is 70%, after static 12h, filter, after the leaching supernatant, reclaim ethanol, at 55 DEG C, be concentrated into relative density is after the extractum of 1.25, is drying to obtain functional plants extract.
In above-mentioned formula, water is deionized water.
Embodiment 4
A kind of disinfection hand cleanser, is characterized in that: comprise following raw material by weight:
Alkyl phosphorus carboxylate 22 parts
9 parts, fatty polyoxyethylene esters sodium sulfate
Functional plants extract 9 parts
Glycerol 5 parts
Betanin 3 parts
PH regulator 0.8 part
65 parts, water;
In above-mentioned formula, functional plants extract is the mixture after being extracted by Fructus Forsythiae, Radix Glycyrrhizae, Radix Scutellariae, Radix Et Rhizoma Rhei, Flos Camelliae Japonicae fruit, and its preparation method is identical with embodiment 3.
The preparation method of described disinfection hand cleanser is as follows: in reaction vessel, add 2/3rds of the water taken by formula, after being warming up to 45 DEG C, add glycerol, after stirring, be cooled to 15 DEG C, add again by remaining 1/3rd water and the alkyl phosphorus carboxylate taken by formula, fatty polyoxyethylene esters sodium sulfate, after betanin, continue to stir, mixing time is 15min, puddler rotating speed is 10 ~ 15r/min, finally adds functional plants extract, after continuing to stir 5min, regulate solution pH value to be after 7 ~ 8 with PH regulator, get product.
Embodiment 5
A kind of disinfection hand cleanser comprises following raw material by weight:
Alkyl phosphorus carboxylate 15 parts
9 parts, fatty polyoxyethylene esters sodium sulfate
Functional plants extract 9 parts
Glycerol 6 parts
Betanin 2 parts
PH regulator 2 parts
55 parts, water
0.5 part, essence;
In above-mentioned formula, functional plants extract is the mixture after being extracted by Fructus Forsythiae, Radix Glycyrrhizae, Radix Scutellariae, Radix Et Rhizoma Rhei, Flos Camelliae Japonicae fruit, and its preparation method is identical with embodiment 3; Described water is deionized water.
The preparation method of the disinfection hand cleanser of the present embodiment is: in reaction vessel, add 2/3rds of the water taken by formula, after being warming up to 50 DEG C, add glycerol, after stirring, be cooled to 25 DEG C, add again by remaining 1/3rd water and the alkyl phosphorus carboxylate taken by formula, fatty polyoxyethylene esters sodium sulfate, after betanin, continue to stir, mixing time is 20min, puddler rotating speed is 15r/min, finally adds functional plants extract, after continuing to stir 8min, regulate solution pH value to be after 7 ~ 8 with PH regulator, get product.
In the method, add glycerol, stir, the time of stirring is 5min, and the rotating speed of puddler is 20 r/min.
Embodiment 6
A kind of disinfection hand cleanser comprises following raw material by weight:
Alkyl phosphorus carboxylate 15 parts
9 parts, fatty polyoxyethylene esters sodium sulfate
Functional plants extract 9 parts
Glycerol 6 parts
Betanin 2 parts
PH regulator 1.5 parts
65 parts, water
1 part, essence
Pigment 0.08 part;
In above-mentioned formula, functional plants extract is the mixture after being extracted by Fructus Forsythiae, Radix Glycyrrhizae, Radix Scutellariae, Radix Et Rhizoma Rhei, Flos Camelliae Japonicae fruit, and its preparation method is identical with embodiment 3; Water described in formula is deionized water.
The preparation method of the disinfection hand cleanser of the present embodiment is: in reaction vessel, add 2/3rds of the water taken by formula, after being warming up to 48 DEG C, add glycerol, after stirring, be cooled to 20 DEG C, add again by remaining 1/3rd water and the alkyl phosphorus carboxylate taken by formula, fatty polyoxyethylene esters sodium sulfate, after betanin, continue to stir, mixing time is 18min, puddler rotating speed is 12r/min, finally adds functional plants extract, after continuing to stir 6min, be after 7 ~ 8 with citric acid regulating solution pH value, get product.
In said method, add glycerol, stir, the time of stirring is 10min, and the rotating speed of puddler is 20 r/min.
Claims (7)
1. a disinfection hand cleanser, is characterized in that: comprise following raw material by weight:
Alkyl phosphorus carboxylate 12 ~ 25 parts
7 ~ 10 parts, fatty polyoxyethylene esters sodium sulfate
Functional plants extract 5 ~ 10 parts
Glycerol 4 ~ 7 parts
Betanin 1 ~ 4 part
PH regulator 0.5 ~ 3 part
50 ~ 70 parts, water;
Described functional plants extract is the mixture after being extracted by Fructus Forsythiae, Radix Glycyrrhizae, Radix Scutellariae, Radix Et Rhizoma Rhei, Flos Camelliae Japonicae fruit.
2. disinfection hand cleanser as claimed in claim 1, is characterized in that: the preparation method of described functional plants extract, comprises the following steps:
Decoct
The Fructus Forsythiae taken for 5:3:2:1:1 in mass ratio, Radix Glycyrrhizae, Radix Scutellariae, Radix Et Rhizoma Rhei, Flos Camelliae Japonicae fruit are added in container, then add the water of 40 ~ 50 DEG C, after soaking 1 ~ 1.5h, raised temperature decocts, under boiling state, after decocting 40 ~ 60min, filtering and collecting filter liquid, again plant residue is decocted, under boiling state, decoct 1 ~ 1.5h, again filter, and collect filtrate, finally the filtrate of twice is merged;
Concentrated
Concentrate filtrate to the extractum that relative density is 1.3 ~ 1.38, after cooling, add the ethanol that concentration of volume percent is 70%, after static 12h, filter, after the leaching supernatant, reclaim ethanol, at 55 DEG C, be concentrated into relative density is after the extractum of 1.2 ~ 1.25, is drying to obtain functional plants extract.
3. disinfection hand cleanser as claimed in claim 1 or 2, is characterized in that: described water is deionized water.
4. disinfection hand cleanser as claimed in claim 1, is characterized in that: also comprise the essence of 0.5 ~ 1 part and the pigment of 0.05 ~ 0.5 part in described raw material.
5. disinfection hand cleanser as claimed in claim 1, it is characterized in that: its preparation method comprises the following steps: in reaction vessel, add 2/3rds of the water taken by formula, after being warming up to 45 ~ 50 DEG C, add glycerol, after stirring, be cooled to 15 ~ 25 DEG C, add again by remaining 1/3rd water and the alkyl phosphorus carboxylate that takes by formula, fatty polyoxyethylene esters sodium sulfate, after betanin, continue to stir, mixing time is 15 ~ 20min, puddler rotating speed is 10 ~ 15r/min, finally add functional plants extract, after continuing stirring 5 ~ 8min, solution pH value is regulated to be after 7 ~ 8 with PH regulator, get product.
6. disinfection hand cleanser as claimed in claim 5, it is characterized in that: described adds glycerol, stirs, the time of stirring is 5 ~ 10min, and the rotating speed of puddler is 20 r/min.
7. disinfection hand cleanser as claimed in claim 5, is characterized in that: described PH regulator is citric acid.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410688633.6A CN104473808A (en) | 2014-11-26 | 2014-11-26 | Sterilizing hand sanitizer and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410688633.6A CN104473808A (en) | 2014-11-26 | 2014-11-26 | Sterilizing hand sanitizer and preparation method thereof |
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| CN104473808A true CN104473808A (en) | 2015-04-01 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201410688633.6A Pending CN104473808A (en) | 2014-11-26 | 2014-11-26 | Sterilizing hand sanitizer and preparation method thereof |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1451732A (en) * | 2002-04-12 | 2003-10-29 | 花王株式会社 | Cleaner composition |
| CN103695208A (en) * | 2013-11-19 | 2014-04-02 | 青岛汇而通商贸有限公司 | Antiseptic bactericidal condensed hand lotion |
-
2014
- 2014-11-26 CN CN201410688633.6A patent/CN104473808A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1451732A (en) * | 2002-04-12 | 2003-10-29 | 花王株式会社 | Cleaner composition |
| CN103695208A (en) * | 2013-11-19 | 2014-04-02 | 青岛汇而通商贸有限公司 | Antiseptic bactericidal condensed hand lotion |
Non-Patent Citations (2)
| Title |
|---|
| 傅文栋: "中草药及其有效成分体外抗菌抗病毒研究进展", 《中兽医医药杂志》 * |
| 符柳英: ""利用多酚氧化酶活性强的植物杀菌"", 《湖南林业科技》 * |
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