CN104445547A - Flocculating agent and preparation method thereof - Google Patents
Flocculating agent and preparation method thereof Download PDFInfo
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- CN104445547A CN104445547A CN201410618719.1A CN201410618719A CN104445547A CN 104445547 A CN104445547 A CN 104445547A CN 201410618719 A CN201410618719 A CN 201410618719A CN 104445547 A CN104445547 A CN 104445547A
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- water
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- flocculation agent
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/5272—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using specific organic precipitants
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/5236—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using inorganic agents
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/5236—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using inorganic agents
- C02F1/5245—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using inorganic agents using basic salts, e.g. of aluminium and iron
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/5263—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using natural chemical compounds
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/54—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using organic material
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
- C02F1/54—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities using organic material
- C02F1/56—Macromolecular compounds
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/10—Inorganic compounds
- C02F2101/20—Heavy metals or heavy metal compounds
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2305/00—Use of specific compounds during water treatment
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Separation Of Suspended Particles By Flocculating Agents (AREA)
Abstract
The invention relates to a flocculating agent and a preparation method thereof. The flocculating agent consists of the following components in parts by weight: 13-20 parts of polyacrylamide, 3-8 parts of ferrate, 5-10 parts of polyphosphate chloride, 5-10 parts of natural organic acid and 3-8 parts of molecular resonance powder. The preparation method comprises the steps of preparing all components in parts by weight, mixing polyacrylamide, ferrate, polyphosphate chloride and the natural organic acid with water and stirring, then heating to 40 DEG C, adding the molecular resonance powder, and stirring for 10 minutes. The flocculating agent for treating sewage has the advantages of high flocculating sedimentation speed, good effect and low cost and can degrade harmful substances in water.
Description
Technical field
The present invention relates to a kind of flocculation agent and preparation method thereof, belong to the dirty water decontamination handles technical field.
Background technology
Sewage, be often referred to by certain that pollute, from life and the discharge water produced.According to the viewpoint of sewage source, sewage can be defined as from house, office, business or manufacturing district discharge and underground water.The liquid carrying refuse of the mixing such as surface water, snowstorm or water.Sewage is by many classifications, and correspondingly reducing sewage also has many technology and technique to the impact of environment.According to sewage source, sewage can be divided into this four class.The first kind: trade effluent, from the sewage manufacturing mining and industrial production activities, comprise from the runoff stored with industry or business, process Leachate site alive, and other is not the waste water of sanitary sewage.Equations of The Second Kind: sanitary sewage is from house, office building, office or similar sewage; Health sewage; Effluent sewerage, comprises the trade effluent mixed in sanitary sewage in sewerage.3rd class: business sewage exceedes nontoxic, the harmless sewage of sanitary sewage from commercial facility and some composition.As sewage from catering business.Using sewage of wash house, animal rearing sewage, the sewage etc. that hairdressing place produces.4th class: overland flow is from water under rainwater, snow-broth, motorway, and from the water etc. of city and industrial area, overland flow does not infilter soil, enters underground water along street and land.
In the water pollution that human production activity causes, the water pollution that industry causes is the most serious.As trade effluent, it is many containing pollutent, and complicated component, not only not easily purifies in water, and process is also more difficult.Industry waste water is the most important reason that industrial pollution causes water pollution.It accounts for the major part of the pollutent that industry is discharged.Pollutent contained by trade effluent varies because factory's kind is different, even same class factory, production process is different, and the quality and quantity of pollutent contained by it is also different.Industry is except the waste water of discharging directly injects water body and causes pollution, and solid waste and waste gas also can polluted-waters.First agricultural pollution is because farming or the reclamation of wasteland make soil surface porosity, the rainfall when soil and landform are not also stablized, and a large amount of silt flows in water, increases the suspended substance in water.Also have major reason be agricultural chemicals, chemical fertilizer usage quantity increasing, and the agricultural chemicals used and chemical fertilizer only have a small amount of attachment or are absorbed, all the other overwhelming majority remain in soil and in an atmosphere floating, by rainfall, enter surface water through washing away of rainwash and infiltrate surface water formation pollution.Urban pollution resource is because urban population is concentrated, and city domestic sewage, rubbish and waste gas cause water pollution to cause.Urban pollution resource is to the pollution of water body mainly sanitary sewage, and it is the mixed solution of the various sewage produced in people's daily life, comprising the sewage that kitchen, washing room, bathroom and lavatory are discharged.
Water resources is the most critical resource of human being's production life, but nowadays, ecotope is seriously damaged, and water pollution is serious, and the protection of water resources and the improvement of water pollutions become the problem that modern society pays close attention to most.China is the serious country of a drought and water shortage.Freshwater resources total amount is 28000 billion cubic meters, account for 6% of global water resources, be only second to Brazil, Russia and Canadian, occupy the 4th, the world, but only have 2200 cubic metres per capita, be only 1/4 of world average level, 1/5 of the U.S., be one of 13 countries that water resources is the poorest per capita in the whole world.After deducting the flood river rising in Ningxia and flowing into central Shaanxi stream being difficult to utilize and the groundwater resource being dispersed in remote districts, China's available Freshwater resources amount of reality is then less, about being only 11000 billion cubic meters, available water resource is about 900 cubic metres per capita, and its distributed pole is unbalanced.To 20 end of the centurys, in more than 600 city, the whole nation, there is insufficient water problem in existing more than 400 city, wherein more serious lack of water city reaches 110, and National urban lack of water total amount is 60 billion cubic meters.China's shortage of water resources, water pollutions are serious, severe water and soil erosion, water price seriously on the low side, water resource waste is serious.And southern water is many, northern water is few.Western water is few, many along seawater.According to monitoring, current national most urban groundwater by point-like to a certain extent and facial contamination, and has the trend increased the weight of year by year.The water pollutions be on the rise not only reduces the using function of water body, exacerbate the contradiction of shortage of water resources further, the strategy of sustainable development implemented China brings and has a strong impact on, but also the safe drinking water of serious threat to city resident and the health of the people.Along with urbanization and socio-economic development, soil is taken in a large number, and non-agricultural irrigation water demand is sharply increasing, agricultural with industry, rural area and city, produce and live, produce and ecology etc. all multiplex water contradiction aggravate further.Although China takes the strictest cultivated land protection measure, a large amount of farmlands and agricultural irrigation water source are taken by city and industry, and the impetus that cultivated land resource reduces is difficult to reverse, and the pressure of shortage of water resources increases further.
For at this shortage of water resources, when water pollutions is serious again, we need to process contaminated water, can again be utilized after making these contaminated water treatments.The coagulating treatment of water is one of key link in wastewater treatment, can go turbid scrubbing, reduces the pollution load of sewage subsequent disposal.And flocculation agent is the key factor determining coagulating treatment effect, all there is important impact to the situation of follow-up process flow operation, final outflow water water quality and cost etc.Flocculation agent totally can be divided into inorganic flocculating agent and organic floculant two class according to its chemical composition.
Chinese invention patent specification sheets CN 102491464 A openly so a kind of flocculation agent and preparation method thereof.This flocculation agent, its composition contained and shared weight percentage as follows: Tai-Ace S 150 35%-45%; Ferric sulfate 3%-9%; Iron(ic) chloride 0.3-2%; Aluminum chloride 0.5-3%.The flocculation agent of this invention, the existing effect being better than single inorganic flocculating agent, also solves the environmental pollution that flyash and VCM nitration mixture cause.The raw material of this invention flocculation agent is all waste residue and liquid, and production technique is simple, easy and simple to handle, and production process produces without the three wastes, belongs to process for cleanly preparing.But this flocculation agent is not fine for the treatment effect of sewage.
Chinese invention patent specification sheets CN 102745787 A openly so a kind of quick flocculating agent and preparation method thereof.The chemical composition of this flocculation agent by weight percentage ratio than meter by: mixed heavy pond mud 75 ~ 85%, blast furnace ground-slag 5 ~ 15%, Tai-Ace S 150 ammonia 2 ~ 10%, bodied ferric sulfate 2 ~ 10% and 1 ~ 2% additive combination form.Tai-Ace S 150 ammonia, bodied ferric sulfate, mixed heavy pond mud, blast furnace ground-slag successively stir by this preparation method in proportion under 80 ~ 200r/min condition; Obtain quick flocculating agent.This flocculation agent is by mixing heavy pond mud and blast furnace ground-slag forms, and blast furnace ground-slag surface has larger activity, flocculation can be made to accelerate, thus reach the object of rapid flocculation, realize recycling and the high value added utilization of solid waste.But this flocculation agent is not fine for the treatment effect of sewage.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of flocculation agent and preparation method thereof, and this flocculation agent is disposed of sewage, and soon, effective, cost is low for not only flocculation sediment speed, and the objectionable impurities in energy degradation water.
In order to solve the problems of the technologies described above, a kind of flocculation agent of the present invention is made up of by following portions by weight following component, polyacrylamide 13-20 part, ferrate 3-8 part, poly-phosphorus muriate 5-10 part, natural organic acids 5-10 part, molecular resonance powder 3-8 part.
Described ferrate is Na2Fe04 or potassium ferrate.
Described poly-phosphorus muriate is poly-phosphorus aluminum chloride or poly-phosphorus iron(ic) chloride.
Described natural organic acids is the one being selected from citric acid, lactic acid, iron lactate.
Described molecular resonance powder is the calcium carbonate the rhombspar of the carbon of weight ratio 20%-60%, 5%-25% and 5%-25%, through vacuum stirring, the mixing raw material after stirring is made particulate state, is placed in anaerobic stove and burns, at the temperature condition of 1100 DEG C-1250 DEG C, fire 8-12 hour.
The preparation method of described flocculation agent, by polyacrylamide, ferrate, poly-phosphorus muriate, natural organic acids adds water stirring, is then heated to 40 DEG C, then adds molecular resonance powder, stir 10 minutes.
The making raw material sources of this flocculation agent are extensive, with low cost.The polyacrylamide selected is soluble in water, and coagulation effect is excellent, product stability is good, and flocculating and purifying is effective, has been the main component of throwing out; Ferrate and poly-phosphorus muriate, by forming the effects such as colloidal precipitation, play the effect of auxiliary flocculation, enhance the flocculating effect of flocculating agent composition; Natural organic acids can Adsorption of Heavy Metal Ions and suspended solid and microorganism; Molecular resonance powder can be carried out sequence to water molecules and be arranged, and water molecule group is refined into 5-6 small water molecule group, not only can degradation of polypropylene acid amides remaining in water, but also can degrade other objectionable impuritiess and heavy metal.
Embodiment
Described a kind of flocculation agent is made up of by following portions by weight following component, polyacrylamide 13-20 part, ferrate 3-8 part, poly-phosphorus muriate 5-10 part, natural organic acids 5-10 part, molecular resonance powder 3-8 part.
Described ferrate is Na2Fe04 or potassium ferrate.
Described poly-phosphorus muriate is poly-phosphorus aluminum chloride or poly-phosphorus iron(ic) chloride.
Described natural organic acids is the one being selected from citric acid, lactic acid, iron lactate.
Described molecular resonance powder is the calcium carbonate the rhombspar of the carbon of weight ratio 20%-60%, 5%-25% and 5%-25%, through vacuum stirring, the mixing raw material after stirring is made particulate state, is placed in anaerobic stove and burns, at the temperature condition of 1100 DEG C-1250 DEG C, fire 8-12 hour.
The preparation method of described flocculation agent, by polyacrylamide, ferrate, poly-phosphorus muriate, natural organic acids adds water stirring, is then heated to 40 DEG C, then adds molecular resonance powder, stir 10 minutes.
Embodiment 1:
According to each composition weight number, get respectively: polyacrylamide 13 parts, ferrate 3 parts, poly-phosphorus muriate 5 parts, natural organic acids 5 parts, molecular resonance powder 3 parts.
Configured by each composition according to parts by weight, by polyacrylamide, ferrate, poly-phosphorus muriate, natural organic acids adds water stirring, is then heated to 40 DEG C, then adds molecular resonance powder, stir 10 minutes.
Embodiment 2:
According to each composition weight number, get respectively: polyacrylamide 15 parts, ferrate 5 parts, poly-phosphorus muriate 7 parts, natural organic acids 7 parts, molecular resonance powder 5 parts.
Configured by each composition according to parts by weight, by polyacrylamide, ferrate, poly-phosphorus muriate, natural organic acids adds water stirring, is then heated to 40 DEG C, then adds molecular resonance powder, stir 10 minutes.
Embodiment 3:
According to each composition weight number, get respectively: polyacrylamide 16 parts, ferrate 6 parts, poly-phosphorus muriate 8 parts, natural organic acids 8 parts, molecular resonance powder 6 parts.
Configured by each composition according to parts by weight, by polyacrylamide, ferrate, poly-phosphorus muriate, natural organic acids adds water stirring, is then heated to 40 DEG C, then adds molecular resonance powder, stir 10 minutes.
Embodiment 4:
According to each composition weight number, get respectively: polyacrylamide 18 parts, ferrate 7 parts, poly-phosphorus muriate 9 parts, natural organic acids 9 parts, molecular resonance powder 7 parts.
Configured by each composition according to parts by weight, by polyacrylamide, ferrate, poly-phosphorus muriate, natural organic acids adds water stirring, is then heated to 40 DEG C, then adds molecular resonance powder, stir 10 minutes.
Embodiment 5:
According to each composition weight number, get respectively: polyacrylamide 20 parts, ferrate 8 parts, poly-phosphorus muriate 10 parts, natural organic acids 10 parts, molecular resonance powder 8 parts.
Configured by each composition according to parts by weight, by polyacrylamide, ferrate, poly-phosphorus muriate, natural organic acids adds water stirring, is then heated to 40 DEG C, then adds molecular resonance powder, stir 10 minutes.
The making raw material sources of this flocculation agent are extensive, with low cost.The polyacrylamide selected is soluble in water, and coagulation effect is excellent, product stability is good, and flocculating and purifying is effective, has been the main component of throwing out; Ferrate and poly-phosphorus muriate, by forming the effects such as colloidal precipitation, play the effect of auxiliary flocculation, enhance the flocculating effect of flocculating agent composition; Natural organic acids can Adsorption of Heavy Metal Ions and suspended solid and microorganism; Molecular resonance powder can be carried out sequence to water molecules and be arranged, and water molecule group is refined into 5-6 small water molecule group, not only can degradation of polypropylene acid amides remaining in water, but also can degrade other objectionable impuritiess and heavy metal.
The technical characteristic described in detail is not had to be prior art in the application.Above-described embodiment is the principle of illustrative the application and effect thereof only, but not for limiting the application.Any person skilled in the art scholar all under the spirit and category of the application, can modify above-described embodiment or changes.Therefore, have in art and usually know that the knowledgeable modifies or changes not departing from all equivalences completed under the spirit and technological thought that the application discloses, must be contained by the claim of the application.
Claims (6)
1. a flocculation agent, is characterized in that: be made up of by following portions by weight following component, polyacrylamide 13-20 part, ferrate 3-8 part, poly-phosphorus muriate 5-10 part, natural organic acids 5-10 part, molecular resonance powder 3-8 part.
2. according to flocculation agent according to claim 1, it is characterized in that: described ferrate is Na2Fe04 or potassium ferrate.
3. according to flocculation agent according to claim 1, it is characterized in that: described poly-phosphorus muriate is poly-phosphorus aluminum chloride or poly-phosphorus iron(ic) chloride.
4. according to flocculation agent according to claim 1, it is characterized in that: described natural organic acids is the one being selected from citric acid, lactic acid, iron lactate.
5. according to flocculation agent according to claim 1, it is characterized in that: described molecular resonance powder is the calcium carbonate the rhombspar of the carbon of weight ratio 20%-60%, 5%-25% and 5%-25%, through vacuum stirring, mixing raw material after stirring is made particulate state, be placed in anaerobic stove to burn, at the temperature condition of 1100 DEG C-1250 DEG C, fire 8-12 hour.
6. a preparation method for flocculation agent as claimed in claim 1, is characterized in that: by polyacrylamide, ferrate, poly-phosphorus muriate, and natural organic acids adds water stirring, is then heated to 40 DEG C, then adds molecular resonance powder, stir 10 minutes.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410618719.1A CN104445547A (en) | 2014-11-06 | 2014-11-06 | Flocculating agent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410618719.1A CN104445547A (en) | 2014-11-06 | 2014-11-06 | Flocculating agent and preparation method thereof |
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| Publication Number | Publication Date |
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| CN104445547A true CN104445547A (en) | 2015-03-25 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201410618719.1A Withdrawn CN104445547A (en) | 2014-11-06 | 2014-11-06 | Flocculating agent and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105692834A (en) * | 2016-03-16 | 2016-06-22 | 张伟彬 | Preparation method of compound water purifying agent |
| CN107935069A (en) * | 2017-12-01 | 2018-04-20 | 杭州凯博特环保科技开发有限公司 | Industrial waste water treatment agent |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003251104A (en) * | 2001-12-27 | 2003-09-09 | Touso Sangyo Kk | Inorganic flocculant for water treatment and usage therefor |
| CN103241817A (en) * | 2013-05-29 | 2013-08-14 | 滁州友林科技发展有限公司 | Combined flocculant |
| CN103253752A (en) * | 2013-05-29 | 2013-08-21 | 滁州友林科技发展有限公司 | High-efficiency flocculant |
| CN103739051A (en) * | 2014-01-29 | 2014-04-23 | 江声 | Rapid flocculant |
| CN103803692A (en) * | 2013-12-30 | 2014-05-21 | 青岛碧水蓝天生物技术有限公司 | Anion material powder for water purification |
-
2014
- 2014-11-06 CN CN201410618719.1A patent/CN104445547A/en not_active Withdrawn
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003251104A (en) * | 2001-12-27 | 2003-09-09 | Touso Sangyo Kk | Inorganic flocculant for water treatment and usage therefor |
| CN103241817A (en) * | 2013-05-29 | 2013-08-14 | 滁州友林科技发展有限公司 | Combined flocculant |
| CN103253752A (en) * | 2013-05-29 | 2013-08-21 | 滁州友林科技发展有限公司 | High-efficiency flocculant |
| CN103803692A (en) * | 2013-12-30 | 2014-05-21 | 青岛碧水蓝天生物技术有限公司 | Anion material powder for water purification |
| CN103739051A (en) * | 2014-01-29 | 2014-04-23 | 江声 | Rapid flocculant |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105692834A (en) * | 2016-03-16 | 2016-06-22 | 张伟彬 | Preparation method of compound water purifying agent |
| CN107935069A (en) * | 2017-12-01 | 2018-04-20 | 杭州凯博特环保科技开发有限公司 | Industrial waste water treatment agent |
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Application publication date: 20150325 |