CN104403503A - High-adhesion corrosion-resistant dirt-removing coating - Google Patents
High-adhesion corrosion-resistant dirt-removing coating Download PDFInfo
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- CN104403503A CN104403503A CN201410713027.5A CN201410713027A CN104403503A CN 104403503 A CN104403503 A CN 104403503A CN 201410713027 A CN201410713027 A CN 201410713027A CN 104403503 A CN104403503 A CN 104403503A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D163/00—Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
- C09D7/62—Additives non-macromolecular inorganic modified by treatment with other compounds
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses a high-adhesion corrosion-resistant dirt-removing coating which comprises the following raw materials in parts by weight: 43-46 parts of epoxy resin, 30-33 parts of dual-component polyurethane, 22-25 parts of aldehyde ketone resin KR-80F, 24-27 parts of a Cu-TiO2 loaded mica material, 8-11 parts of diatomite, 4-7 parts of aluminum silicate, 0.5-0.8 part of an aluminum-zirconium coupling agent, 0.5-0.8 part of an antioxidant, 1.8-2.1 parts of a defoamer, 1.2-1.5 parts of a dispersant, 1.4-1.7 parts of a leveling agent, 1.2-1.4 parts of a curing agent and 55-58 parts of a solvent. The high-adhesion corrosion-resistant dirt-removing coating is high in adhesion power, good in corrosion resistance and excellent in dirt-removing effect.
Description
Technical field
The present invention relates to decontamination technical field of coatings, particularly relate to the corrosion-resistant decontamination coating of high adhesive force.
Background technology
Decontamination paint is after metal base surface, in the process contacted with organic pollutant, its catalyzer comprised can by katalysis decomposing organic pollutant, titanium dioxide is exactly a kind of novel photocatalyst, its catalytic efficiency is high, effectively organic pollutant can be resolved into the small molecules of toxicological harmless, thus reach cleaning action, but high easily generation of the surface energy of titanium dioxide is reunited thus loses katalysis, and the use cost of titanium dioxide is higher, the decontamination paint adhesion made with it is not high, erosion resistance is bad, therefore, develop a kind of high adhesive force, corrosion-resistant and the decontamination coating of catalytic effect excellence is the demand in market.
Summary of the invention
Based on the technical problem that background technology exists, the present invention proposes the corrosion-resistant decontamination coating of a kind of high adhesive force, sticking power is high, corrosion resistance and good and clean effect is excellent.
The present invention proposes the corrosion-resistant decontamination coating of a kind of high adhesive force, and its raw material comprises by weight: epoxy resin 43-46 part, two component polyurethane 30-33 part, and aldehyde ketone resin KR-80F 22-25 part, load has Cu-TiO
2mica material 24-27 part, diatomite 8-11 part, pure aluminium silicate 4-7 part, aluminum-zirconium coupling agent TL-2 0.5-0.8 part, anti-aging agent 0.5-0.8 part, defoamer 1.8-2.1 part, dispersion agent 1.2-1.5 part, flow agent 1.4-1.7 part, solidifying agent 1.2-1.4 part, solvent 55-58 part.
Preferably, two component polyurethane by two components in mass ratio 1.2-1.6:2-3 be mixed.
Preferably, the weight ratio of epoxy resin, two component polyurethane, aldehyde ketone resin KR-80F is 44-45:31-32:23-24.
Preferably, its raw material comprises by weight: epoxy resin 44-45 part, two component polyurethane 31-32 part, and aldehyde ketone resin KR-80F 23-24 part, load has Cu-TiO
2mica material 25-26 part, diatomite 9-10 part, pure aluminium silicate 5-6 part, aluminum-zirconium coupling agent TL-2 0.6-0.7 part, anti-aging agent 0.6-0.7 part, defoamer 1.9-2 part, dispersion agent 1.3-1.4 part, flow agent 1.5-1.6 part, solidifying agent 1.2-1.3 part, solvent 56-57 part.
Preferably, load has Cu-TiO
2in the preparation process of mica material, added by tetrabutyl titanate in the reaction vessel containing dehydrated alcohol, then add copper nitrate solution, after stirring, ageing, suction filtration, oven dry obtain material A; After material A, mica powder, deionized water being mixed, add salpeter solution, heat up, after insulation, ageing, washing, drying obtains load Cu-TiO
2mica material.
Preferably, load has Cu-TiO
2in the preparation process of mica material, by weight 8-10 part tetrabutyl titanate is added in the reaction vessel containing 12-14 part dehydrated alcohol by the speed of 1-1.5 part/min, adding 12-15 part massfraction is again the copper nitrate solution of 25-28wt%, ageing 2-4h after stirring, suction filtration, oven dry obtain material A; Material A, 20-23 part mica powder and 120-150 part deionized water are mixed, then add the salpeter solution that massfraction is 63-66wt%, regulate pH value to 4-5, be warming up to 75-80 DEG C, after insulation 12-16h, ageing, washing, drying obtains load Cu-TiO
2mica material.
Preferably, load has Cu-TiO
2in the preparation process of mica material, by weight 8.5-9 part tetrabutyl titanate is added in the reaction vessel containing 12.5-13 part dehydrated alcohol by the speed of 1.2-1.4 part/min, adding 13-14 part massfraction is again the copper nitrate solution of 26-27wt%, ageing 2.5-3h after stirring, suction filtration, oven dry obtain material A; Material A, 21-22 part mica powder and 130-140 part deionized water are mixed, add the salpeter solution that massfraction is 64-65wt% again, regulate pH value to 4.5-4.8, be warming up to 76-78 DEG C, after insulation 13-15h, ageing, washing, drying obtains load Cu-TiO
2mica material.
The present invention adopt epoxy resin, two component polyurethane and, aldehyde ketone resin KR-80F is as filmogen, the present invention is made to possess excellent sticking power, corrosion resistance nature and curing speed faster, simultaneously, also make the present invention have good space net structure to hold photocatalyst, thus substantially increase soil removability of the present invention, the load added has Cu-TiO
2mica material, diatomite, pure aluminium silicate substantially increases sticking power of the present invention and corrosion resistance, in addition, load has the mica material of copper-titanium dioxide to be a kind of novel antifouling material be carried on by copper-titanium dioxide compound in mica, solve the simple titanium dioxide that uses as in the process of photocatalyst, because titanium dioxide specific surface area is large, reunite between the titania molecule that surface energy causes greatly, thus lose the problem of photocatalysis performance, and cupric ion is separately as the instability problem of stain remover, in preparation process, by cupric ion and titanium dioxide with Van der Waals force compound, drastically increase degradable organic pollutant of the present invention, the ability of microbial contamination, and cupric ion can initiatively absorb polluted matter, strengthen detersive efficiency of the present invention, simultaneously, cupric ion and titanium dioxide compound, the present invention is possessed stable, efficient catalysis, soil removability, and copper-titanium dioxide compound is carried in mica, drastically increase stability of the present invention, expand the contact area of the present invention and pollutent, improve catalytic efficiency, and mica good hydrophilic property, with low cost, can while fully holding copper-titanium dioxide compound, reduce cost of the present invention, the interpolation of Silane coupling reagent KH-570, what make above-mentioned interpolation on the one hand is loaded with Cu-TiO
2mica material, diatomite, pure aluminium silicate are evenly dispersed in the present invention, on the other hand, one end of aluminum-zirconium coupling agent TL-2 can with the hydroxyl reaction applying metal base surface of the present invention, the other end can react with the epoxy group(ing) in epoxy resin, thus form firmly covalent linkage between coating metal base surface of the present invention and the present invention, thus substantially increase sticking power of the present invention.
Embodiment
Below, by specific embodiment, technical scheme of the present invention is described in detail.
Embodiment 1
The present invention proposes the corrosion-resistant decontamination coating of a kind of high adhesive force, and its raw material comprises by weight: epoxy resin 46 parts, two component polyurethane 30 parts, and aldehyde ketone resin KR-80F 25 parts, load has Cu-TiO
2mica material 24 parts, 11 parts, diatomite, pure aluminium silicate 4 parts, aluminum-zirconium coupling agent TL-2 0.8 part, 0.5 part, anti-aging agent, defoamer 2.1 parts, dispersion agent 1.2 parts, flow agent 1.7 parts, 1.2 parts, solidifying agent, solvent 58 parts; Two component polyurethane by two components in mass ratio 1.2:3 be mixed;
Load has Cu-TiO
2in the preparation process of mica material, by weight 9 parts of tetrabutyl titanates are added in the reaction vessel containing 13 parts of dehydrated alcohols by the speed of 1.2 parts/min, adding 13 parts of massfractions is again the copper nitrate solution of 27wt%, ageing 2.5h after stirring, and suction filtration, oven dry obtain material A; Material A, 22 parts of mica powders and 130 parts of deionized waters are mixed, then add the salpeter solution that massfraction is 65wt%, regulate pH value to 4.5, be warming up to 78 DEG C, after insulation 13h, ageing, washing, drying obtains load Cu-TiO
2mica material.
Embodiment 2
The present invention proposes the corrosion-resistant decontamination coating of a kind of high adhesive force, and its raw material comprises by weight: epoxy resin 43 parts, two component polyurethane 33 parts, and aldehyde ketone resin KR-80F 22 parts, load has Cu-TiO
2mica material 27 parts, 8 parts, diatomite, pure aluminium silicate 7 parts, aluminum-zirconium coupling agent TL-2 0.5 part, 0.8 part, anti-aging agent, defoamer 1.8 parts, dispersion agent 1.5 parts, flow agent 1.4 parts, 1.4 parts, solidifying agent, solvent 55 parts; Two component polyurethane by two components in mass ratio 1.6:2 be mixed;
Load has Cu-TiO
2in the preparation process of mica material, by weight 8.5 parts of tetrabutyl titanates are added in the reaction vessel containing 12.5 parts of dehydrated alcohols by the speed of 1.4 parts/min, adding 14 parts of massfractions is again the copper nitrate solution of 26wt%, ageing 3h after stirring, and suction filtration, oven dry obtain material A; Material A, 21 parts of mica powders and 140 parts of deionized waters are mixed, then add the salpeter solution that massfraction is 64wt%, regulate pH value to 4.8, be warming up to 76 DEG C, after insulation 15h, ageing, washing, drying obtains load Cu-TiO
2mica material.
Embodiment 3
The present invention proposes the corrosion-resistant decontamination coating of a kind of high adhesive force, and its raw material comprises by weight: epoxy resin 45 parts, two component polyurethane 31 parts, and aldehyde ketone resin KR-80F 24 parts, load has Cu-TiO
2mica material 25 parts, 10 parts, diatomite, pure aluminium silicate 5 parts, aluminum-zirconium coupling agent TL-2 0.7 part, 0.6 part, anti-aging agent, defoamer 2 parts, dispersion agent 1.3 parts, flow agent 1.6 parts, 1.2 parts, solidifying agent, solvent 57 parts; Two component polyurethane by two components in mass ratio 1.3:2.5 be mixed;
Load has Cu-TiO
2in the preparation process of mica material, by weight 8 parts of tetrabutyl titanates are added in the reaction vessel containing 12 parts of dehydrated alcohols by the speed of 1.5 parts/min, adding 15 parts of massfractions is again the copper nitrate solution of 25wt%, ageing 4h after stirring, and suction filtration, oven dry obtain material A; Material A, 20 parts of mica powders and 150 parts of deionized waters are mixed, then add the salpeter solution that massfraction is 63wt%, regulate pH value to 5, be warming up to 75 DEG C, after insulation 16h, ageing, washing, drying obtains load Cu-TiO
2mica material.
Embodiment 4
The present invention proposes the corrosion-resistant decontamination coating of a kind of high adhesive force, and its raw material comprises by weight: epoxy resin 44 parts, two component polyurethane 32 parts, and aldehyde ketone resin KR-80F 23 parts, load has Cu-TiO
2mica material 26 parts, 9 parts, diatomite, pure aluminium silicate 6 parts, aluminum-zirconium coupling agent TL-2 0.6 part, 0.7 part, anti-aging agent, defoamer 1.9 parts, disperses 1.4 parts, flow agent 1.5 parts, 1.3 parts, solidifying agent, solvent 56 parts; Two component polyurethane by two components in mass ratio 1.5:2.2 be mixed;
Load has Cu-TiO
2in the preparation process of mica material, by weight 10 parts of tetrabutyl titanates are added in the reaction vessel containing 14 parts of dehydrated alcohols by the speed of 1 part/min, adding 12 parts of massfractions is again the copper nitrate solution of 28wt%, ageing 2h after stirring, and suction filtration, oven dry obtain material A; Material A, 23 parts of mica powders and 120 parts of deionized waters are mixed, then add the salpeter solution that massfraction is 66wt%, regulate pH value to 4, be warming up to 80 DEG C, after insulation 12h, ageing, washing, drying obtains load Cu-TiO
2mica material.
The above; be only the present invention's preferably embodiment; but protection scope of the present invention is not limited thereto; anyly be familiar with those skilled in the art in the technical scope that the present invention discloses; be equal to according to technical scheme of the present invention and inventive concept thereof and replace or change, all should be encompassed within protection scope of the present invention.
Claims (7)
1. the corrosion-resistant decontamination coating of high adhesive force, it is characterized in that, its raw material comprises by weight: epoxy resin 43-46 part, two component polyurethane 30-33 part, and aldehyde ketone resin KR-80F 22-25 part, load has Cu-TiO
2mica material 24-27 part, diatomite 8-11 part, pure aluminium silicate 4-7 part, aluminum-zirconium coupling agent TL-20.5-0.8 part, anti-aging agent 0.5-0.8 part, defoamer 1.8-2.1 part, dispersion agent 1.2-1.5 part, flow agent 1.4-1.7 part, solidifying agent 1.2-1.4 part, solvent 55-58 part.
2. the corrosion-resistant decontamination coating of high adhesive force according to claim 1, is characterized in that, two component polyurethane by two components in mass ratio 1.2-1.6:2-3 be mixed.
3. the corrosion-resistant decontamination coating of high adhesive force according to claim 1 or 2, is characterized in that, the weight ratio of epoxy resin, two component polyurethane, aldehyde ketone resin KR-80F is 44-45:31-32:23-24.
4. the corrosion-resistant decontamination coating of high adhesive force according to any one of claim 1-3, it is characterized in that, its raw material comprises by weight: epoxy resin 44-45 part, two component polyurethane 31-32 part, and aldehyde ketone resin KR-80F 23-24 part, load has Cu-TiO
2mica material 25-26 part, diatomite 9-10 part, pure aluminium silicate 5-6 part, aluminum-zirconium coupling agent TL-20.6-0.7 part, anti-aging agent 0.6-0.7 part, defoamer 1.9-2 part, dispersion agent 1.3-1.4 part, flow agent 1.5-1.6 part, solidifying agent 1.2-1.3 part, solvent 56-57 part.
5. the corrosion-resistant decontamination coating of high adhesive force according to any one of claim 1-4, it is characterized in that, load has Cu-TiO
2in the preparation process of mica material, added by tetrabutyl titanate in the reaction vessel containing dehydrated alcohol, then add copper nitrate solution, after stirring, ageing, suction filtration, oven dry obtain material A; After material A, mica powder, deionized water being mixed, add salpeter solution, heat up, after insulation, ageing, washing, drying obtains load Cu-TiO
2mica material.
6. the corrosion-resistant decontamination coating of high adhesive force according to any one of claim 1-5, it is characterized in that, load has Cu-TiO
2in the preparation process of mica material, by weight 8-10 part tetrabutyl titanate is added in the reaction vessel containing 12-14 part dehydrated alcohol by the speed of 1-1.5 part/min, adding 12-15 part massfraction is again the copper nitrate solution of 25-28wt%, ageing 2-4h after stirring, suction filtration, oven dry obtain material A; Material A, 20-23 part mica powder and 120-150 part deionized water are mixed, then add the salpeter solution that massfraction is 63-66wt%, regulate pH value to 4-5, be warming up to 75-80 DEG C, after insulation 12-16h, ageing, washing, drying obtains load Cu-TiO
2mica material.
7. the corrosion-resistant decontamination coating of high adhesive force according to any one of claim 1-6, it is characterized in that, load has Cu-TiO
2in the preparation process of mica material, by weight 8.5-9 part tetrabutyl titanate is added in the reaction vessel containing 12.5-13 part dehydrated alcohol by the speed of 1.2-1.4 part/min, adding 13-14 part massfraction is again the copper nitrate solution of 26-27wt%, ageing 2.5-3h after stirring, suction filtration, oven dry obtain material A; Material A, 21-22 part mica powder and 130-140 part deionized water are mixed, add the salpeter solution that massfraction is 64-65wt% again, regulate pH value to 4.5-4.8, be warming up to 76-78 DEG C, after insulation 13-15h, ageing, washing, drying obtains load Cu-TiO
2mica material.
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Cited By (6)
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CN104861800A (en) * | 2015-04-28 | 2015-08-26 | 桐城市新丰彩印包装有限公司 | High adhesion and corrosion resistant decontamination coating |
CN104861820A (en) * | 2015-04-28 | 2015-08-26 | 桐城市新丰彩印包装有限公司 | Macroporous adsorption resin modified decontamination coating |
CN105602426A (en) * | 2015-12-28 | 2016-05-25 | 安徽安大华泰新材料有限公司 | Waterproof aqueous polyurethane coating |
CN105838189A (en) * | 2016-04-29 | 2016-08-10 | 南京晨光艺术工程有限公司 | High-adhesive-force coating formula |
CN105860750A (en) * | 2016-04-29 | 2016-08-17 | 南京晨光艺术工程有限公司 | High-adhesive-force paint |
CN107917351A (en) * | 2017-10-27 | 2018-04-17 | 中山市汉庭照明科技有限公司 | A kind of LED light bulbs and preparation method having except effect of formaldehyde |
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Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104861800A (en) * | 2015-04-28 | 2015-08-26 | 桐城市新丰彩印包装有限公司 | High adhesion and corrosion resistant decontamination coating |
CN104861820A (en) * | 2015-04-28 | 2015-08-26 | 桐城市新丰彩印包装有限公司 | Macroporous adsorption resin modified decontamination coating |
CN105602426A (en) * | 2015-12-28 | 2016-05-25 | 安徽安大华泰新材料有限公司 | Waterproof aqueous polyurethane coating |
CN105838189A (en) * | 2016-04-29 | 2016-08-10 | 南京晨光艺术工程有限公司 | High-adhesive-force coating formula |
CN105860750A (en) * | 2016-04-29 | 2016-08-17 | 南京晨光艺术工程有限公司 | High-adhesive-force paint |
CN107917351A (en) * | 2017-10-27 | 2018-04-17 | 中山市汉庭照明科技有限公司 | A kind of LED light bulbs and preparation method having except effect of formaldehyde |
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Application publication date: 20150311 |