CN104351204B - 一种戊唑醇和大蒜素的微囊悬浮剂 - Google Patents
一种戊唑醇和大蒜素的微囊悬浮剂 Download PDFInfo
- Publication number
- CN104351204B CN104351204B CN201410630587.4A CN201410630587A CN104351204B CN 104351204 B CN104351204 B CN 104351204B CN 201410630587 A CN201410630587 A CN 201410630587A CN 104351204 B CN104351204 B CN 104351204B
- Authority
- CN
- China
- Prior art keywords
- tebuconazole
- garlicin
- suspending agent
- present
- microcapsule suspending
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- PXMNMQRDXWABCY-UHFFFAOYSA-N 1-(4-chlorophenyl)-4,4-dimethyl-3-(1H-1,2,4-triazol-1-ylmethyl)pentan-3-ol Chemical compound C1=NC=NN1CC(O)(C(C)(C)C)CCC1=CC=C(Cl)C=C1 PXMNMQRDXWABCY-UHFFFAOYSA-N 0.000 title claims abstract description 27
- 239000005839 Tebuconazole Substances 0.000 title claims abstract description 27
- 239000003094 microcapsule Substances 0.000 title claims abstract description 18
- 239000000375 suspending agent Substances 0.000 title claims abstract description 15
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims abstract description 27
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 27
- 239000002253 acid Substances 0.000 claims abstract description 11
- 150000007513 acids Chemical class 0.000 claims abstract description 9
- 150000001266 acyl halides Chemical class 0.000 claims abstract description 9
- 150000001298 alcohols Chemical class 0.000 claims abstract description 9
- BEFDCLMNVWHSGT-UHFFFAOYSA-N ethenylcyclopentane Chemical compound C=CC1CCCC1 BEFDCLMNVWHSGT-UHFFFAOYSA-N 0.000 claims abstract description 8
- 229940075582 sorbic acid Drugs 0.000 claims abstract description 8
- 235000010199 sorbic acid Nutrition 0.000 claims abstract description 8
- 239000004334 sorbic acid Substances 0.000 claims abstract description 8
- -1 polyoxyethylene Polymers 0.000 claims abstract description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- 239000002994 raw material Substances 0.000 claims description 7
- 150000001412 amines Chemical class 0.000 claims description 5
- 239000008367 deionised water Substances 0.000 claims description 5
- 229910021641 deionized water Inorganic materials 0.000 claims description 5
- 229940051841 polyoxyethylene ether Drugs 0.000 claims description 5
- 229920000056 polyoxyethylene ether Polymers 0.000 claims description 5
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims 1
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims 1
- 239000000600 sorbitol Substances 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 16
- 241000221785 Erysiphales Species 0.000 abstract description 10
- 240000008067 Cucumis sativus Species 0.000 abstract description 9
- 235000010799 Cucumis sativus var sativus Nutrition 0.000 abstract description 9
- 230000002265 prevention Effects 0.000 abstract description 9
- IJCWFDPJFXGQBN-RYNSOKOISA-N [(2R)-2-[(2R,3R,4S)-4-hydroxy-3-octadecanoyloxyoxolan-2-yl]-2-octadecanoyloxyethyl] octadecanoate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OC[C@@H](OC(=O)CCCCCCCCCCCCCCCCC)[C@H]1OC[C@H](O)[C@H]1OC(=O)CCCCCCCCCCCCCCCCC IJCWFDPJFXGQBN-RYNSOKOISA-N 0.000 abstract description 8
- 239000000203 mixture Substances 0.000 abstract description 8
- 229960004129 sorbitan tristearate Drugs 0.000 abstract description 8
- 235000011078 sorbitan tristearate Nutrition 0.000 abstract description 8
- 239000001589 sorbitan tristearate Substances 0.000 abstract description 8
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 abstract description 4
- 239000004615 ingredient Substances 0.000 abstract description 3
- 230000002045 lasting effect Effects 0.000 abstract description 3
- 230000000844 anti-bacterial effect Effects 0.000 abstract description 2
- 239000012752 auxiliary agent Substances 0.000 abstract description 2
- 229940083608 sodium hydroxide Drugs 0.000 abstract description 2
- 235000011121 sodium hydroxide Nutrition 0.000 abstract description 2
- 229920003171 Poly (ethylene oxide) Polymers 0.000 abstract 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 10
- 201000010099 disease Diseases 0.000 description 8
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 8
- 239000003814 drug Substances 0.000 description 7
- 238000000034 method Methods 0.000 description 6
- 230000003902 lesion Effects 0.000 description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- 239000000575 pesticide Substances 0.000 description 4
- 240000002234 Allium sativum Species 0.000 description 3
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 150000001336 alkenes Chemical class 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- 238000007667 floating Methods 0.000 description 3
- 235000004611 garlic Nutrition 0.000 description 3
- 241000234282 Allium Species 0.000 description 2
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- 239000003899 bactericide agent Substances 0.000 description 2
- 238000002242 deionisation method Methods 0.000 description 2
- 238000011835 investigation Methods 0.000 description 2
- 231100000572 poisoning Toxicity 0.000 description 2
- 230000000607 poisoning effect Effects 0.000 description 2
- 238000001228 spectrum Methods 0.000 description 2
- 238000005507 spraying Methods 0.000 description 2
- 150000003852 triazoles Chemical class 0.000 description 2
- JDLKFOPOAOFWQN-VIFPVBQESA-N Allicin Natural products C=CCS[S@](=O)CC=C JDLKFOPOAOFWQN-VIFPVBQESA-N 0.000 description 1
- 240000002791 Brassica napus Species 0.000 description 1
- 235000006008 Brassica napus var napus Nutrition 0.000 description 1
- 241000219112 Cucumis Species 0.000 description 1
- 235000015510 Cucumis melo subsp melo Nutrition 0.000 description 1
- 241000234280 Liliaceae Species 0.000 description 1
- 241000220324 Pyrus Species 0.000 description 1
- 241000221662 Sclerotinia Species 0.000 description 1
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 1
- 229930182558 Sterol Natural products 0.000 description 1
- FJJCIZWZNKZHII-UHFFFAOYSA-N [4,6-bis(cyanoamino)-1,3,5-triazin-2-yl]cyanamide Chemical compound N#CNC1=NC(NC#N)=NC(NC#N)=N1 FJJCIZWZNKZHII-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- JDLKFOPOAOFWQN-UHFFFAOYSA-N allicin Chemical compound C=CCSS(=O)CC=C JDLKFOPOAOFWQN-UHFFFAOYSA-N 0.000 description 1
- 235000010081 allicin Nutrition 0.000 description 1
- 235000001014 amino acid Nutrition 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 235000013339 cereals Nutrition 0.000 description 1
- 238000000205 computational method Methods 0.000 description 1
- 230000017858 demethylation Effects 0.000 description 1
- 238000010520 demethylation reaction Methods 0.000 description 1
- 230000006806 disease prevention Effects 0.000 description 1
- 230000000857 drug effect Effects 0.000 description 1
- 238000009313 farming Methods 0.000 description 1
- 235000012055 fruits and vegetables Nutrition 0.000 description 1
- 230000000855 fungicidal effect Effects 0.000 description 1
- 230000002070 germicidal effect Effects 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 150000002898 organic sulfur compounds Chemical class 0.000 description 1
- 244000052769 pathogen Species 0.000 description 1
- 230000001717 pathogenic effect Effects 0.000 description 1
- 235000021017 pears Nutrition 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 230000003449 preventive effect Effects 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 238000005070 sampling Methods 0.000 description 1
- 150000003432 sterols Chemical class 0.000 description 1
- 235000003702 sterols Nutrition 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
Description
Claims (1)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201410630587.4A CN104351204B (zh) | 2014-11-11 | 2014-11-11 | 一种戊唑醇和大蒜素的微囊悬浮剂 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201410630587.4A CN104351204B (zh) | 2014-11-11 | 2014-11-11 | 一种戊唑醇和大蒜素的微囊悬浮剂 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN104351204A CN104351204A (zh) | 2015-02-18 |
CN104351204B true CN104351204B (zh) | 2016-10-05 |
Family
ID=52518598
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201410630587.4A Active CN104351204B (zh) | 2014-11-11 | 2014-11-11 | 一种戊唑醇和大蒜素的微囊悬浮剂 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN104351204B (zh) |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103250707A (zh) * | 2012-02-15 | 2013-08-21 | 陕西美邦农药有限公司 | 一种含烯丙苯噻唑与三唑类的农药组合物 |
CN103355343A (zh) * | 2013-07-26 | 2013-10-23 | 海南正业中农高科股份有限公司 | 含有硫磺的农用组合物 |
CN103651337A (zh) * | 2012-09-24 | 2014-03-26 | 宜德雅(北京)科技有限公司 | 一种杀菌增效悬浮剂组合物 |
-
2014
- 2014-11-11 CN CN201410630587.4A patent/CN104351204B/zh active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103250707A (zh) * | 2012-02-15 | 2013-08-21 | 陕西美邦农药有限公司 | 一种含烯丙苯噻唑与三唑类的农药组合物 |
CN103651337A (zh) * | 2012-09-24 | 2014-03-26 | 宜德雅(北京)科技有限公司 | 一种杀菌增效悬浮剂组合物 |
CN103355343A (zh) * | 2013-07-26 | 2013-10-23 | 海南正业中农高科股份有限公司 | 含有硫磺的农用组合物 |
Non-Patent Citations (1)
Title |
---|
大蒜素对辣椒炭疽病和辣椒疫病病菌的室内活性测定及田间防效研究;周清,等;《草业学报》;20040620;第23卷(第3期);第263页第1段 * |
Also Published As
Publication number | Publication date |
---|---|
CN104351204A (zh) | 2015-02-18 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN103999865B (zh) | 一种含有环氟菌胺与烯酰吗啉或苯酰菌胺的杀菌组合物及应用 | |
CN103704215B (zh) | 一种含壳寡糖的杀菌组合物 | |
CN103798240A (zh) | 含有吡噻菌胺与甲氧基丙烯酸酯类杀菌成分的组合物 | |
CN103828812A (zh) | 含寡糖与嘧啶类杀菌成分的组合物 | |
CN102293205A (zh) | 蛇床子素与宁南霉素复配杀菌剂 | |
CN104396957B (zh) | 用于防治茶树茶尺蠖的微乳剂 | |
CN104351203B (zh) | 一种戊唑醇和大蒜素的微乳剂 | |
CN104351206B (zh) | 一种戊唑醇和大蒜素的可湿性粉剂 | |
CN104872204A (zh) | 一种防治蔬菜疫霉根腐病的植物性杀菌剂及制备方法 | |
CN104351204B (zh) | 一种戊唑醇和大蒜素的微囊悬浮剂 | |
CN103814902B (zh) | 一种含咯菌腈和苯醚甲环唑防治菊花病害的组合物 | |
CN104351199B (zh) | 一种戊唑醇和大蒜素的水分散粒剂 | |
CN104351197B (zh) | 一种戊唑醇和大蒜素的微囊悬浮-悬浮剂 | |
CN104351200B (zh) | 一种戊唑醇和大蒜素杀菌组合物 | |
CN104351196B (zh) | 一种用于菊花的微乳剂 | |
CN104351194B (zh) | 一种棉花杀虫剂 | |
CN104351198B (zh) | 一种用于菊花的微囊悬浮剂 | |
CN104322494B (zh) | 有效成分为大蒜素和井冈霉素a的水乳剂 | |
CN104351202B (zh) | 一种用于菊花的水乳剂 | |
CN104351205B (zh) | 一种用于菊花的水分散粒剂 | |
CN104351182B (zh) | 用于防治番茄病害的水乳剂 | |
Hofmann et al. | Optimisation of downy mildew (Plasmopara viticola) control in organic viticulture with low copper doses, new copper formulations and plant strengtheners, results of four years of on farm research | |
CN103651353A (zh) | 一种含苯酰菌胺和甲霜灵的杀菌组合物及应用 | |
CN102318664A (zh) | 一种杀菌组合物 | |
CN104351201A (zh) | 一种菊花杀菌剂 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C41 | Transfer of patent application or patent right or utility model | ||
CB03 | Change of inventor or designer information |
Inventor after: Wang Xu Inventor before: Sun Bo Inventor before: Sun Qian Inventor before: Mu Kexiao Inventor before: Hao Aihua Inventor before: Wang Mengmeng |
|
COR | Change of bibliographic data | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20160830 Address after: 266000 Shandong province Qingdao City, Shandong Road No. 109 Building No. 3 3102 Taiwan Jing Applicant after: QINGDAO JINZHI HI-TECH CO.,LTD. Address before: 250001 Shandong Province, Ji'nan City District Court building 2303 No. 288 Applicant before: JINAN XINQIDIAN MEDICAL TECHNOLOGY Co.,Ltd. |
|
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right | ||
TR01 | Transfer of patent right |
Effective date of registration: 20201130 Address after: The intersection of 274300 Shandong city in Heze Province Economic Development Zone of Shanxian County Plain Road and North Road Patentee after: SHANXIAN ZHONGYI HAIDING FORAGE Co.,Ltd. Address before: 266000 Shandong province Qingdao City, Shandong Road No. 109 Building No. 3 3102 Taiwan Jing Patentee before: QINGDAO JINZHI HI-TECH Co.,Ltd. |
|
TR01 | Transfer of patent right | ||
TR01 | Transfer of patent right |
Effective date of registration: 20210428 Address after: Room 78328, building 3, No. 1800, Panyuan Road, Changxing Town, Chongming District, Shanghai 202150 (Shanghai Taihe Economic Development Zone) Patentee after: Dushi (Shanghai) science and Technology Service Center Address before: The intersection of 274300 Shandong city in Heze Province Economic Development Zone of Shanxian County Plain Road and North Road Patentee before: SHANXIAN ZHONGYI HAIDING FORAGE Co.,Ltd. |
|
TR01 | Transfer of patent right | ||
TR01 | Transfer of patent right |
Effective date of registration: 20230412 Address after: 274600, 50 meters east of the intersection of Juanshi Road and North Ring Road, Juancheng County, Heze City, Shandong Province Patentee after: Shandong SHANGNONG Agricultural Technology Co.,Ltd. Address before: Room 78328, building 3, No. 1800, Panyuan Road, Changxing Town, Chongming District, Shanghai 202150 (Shanghai Taihe Economic Development Zone) Patentee before: Dushi (Shanghai) science and Technology Service Center |
|
PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Microcapsule suspension of tebuconazole and Allicin Effective date of registration: 20230612 Granted publication date: 20161005 Pledgee: Shandong juancheng Rural Commercial Bank Co.,Ltd. Pledgor: Shandong SHANGNONG Agricultural Technology Co.,Ltd. Registration number: Y2023980043752 |