CN104342695B - A kind of phosphatization slag content measurement device - Google Patents
A kind of phosphatization slag content measurement device Download PDFInfo
- Publication number
- CN104342695B CN104342695B CN201310747606.7A CN201310747606A CN104342695B CN 104342695 B CN104342695 B CN 104342695B CN 201310747606 A CN201310747606 A CN 201310747606A CN 104342695 B CN104342695 B CN 104342695B
- Authority
- CN
- China
- Prior art keywords
- ring support
- phosphatization slag
- measurement device
- reading
- sediment
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C22/00—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
- C23C22/73—Chemical surface treatment of metallic material by reaction of the surface with a reactive liquid, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals characterised by the process
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D11/00—Electrolytic coating by surface reaction, i.e. forming conversion layers
- C25D11/36—Phosphatising
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D13/00—Electrophoretic coating characterised by the process
- C25D13/22—Servicing or operating apparatus or multistep processes
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Electrochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Mechanical Engineering (AREA)
- Investigating Strength Of Materials By Application Of Mechanical Stress (AREA)
Abstract
The present invention relates to a kind of phosphatization slag content measurement device, the problem of solving easy erroneous judgement not accurate enough currently with artificial range estimation micro-judgment phosphating solution dregginess.The present apparatus includes bearing, there is ring support on bearing, ring support restocking is provided with up big and down small conical graduate, conical graduate upper portion side wall has the scale for reading phosphating solution pouring volume, conical graduate bottom sidewall has the scale for reading sediment height, and the conical graduate bottom vertex of a cone is additionally provided with dismountable screw of blocking up.The present invention realizes the quantization measurement of phosphatization slag, makes the phosphatization slag control of phosphating solution more accurate；Measurement apparatus can guarantee that sediment upper surface is concordant with scale, be easy to reading using the support of self-regulation；Measurement apparatus carries micromachine and provides frequency low-amplitude vibration, eliminates the pit of sediment upper surface, makes reading more accurate.
Description
Technical field
The present invention relates to a kind of survey tool, more particularly to a kind of phosphatization slag content measurement device.
Background technology
Automobile body-in-white is needing to carry out application after the welding fabrication that is welded, to possess its beautiful appearance and higher
Surcharge.In coating process, the phosphatization process before electrophoresis is particularly significant, preferable phosphating coat can be conducive to electrophoresis into
Film.During phosphorization filming, phosphating dregs are inevitably produced, further, since phosphating solution burden control is improper, meeting
Cause to produce excessive sediment.Phosphating dregs too high levels in tank liquor, will be attached on workpiece, influence film performance.If
Bring electrophoresis tank into, phosphating dregs will destroy electrophoresis groove liquid stabilization, influence the service life of ultrafiltration apparatus, therefore control phosphatization slag
Content it is very necessary.
Control for phosphatization slag at present is not allowed to the device quantified, is generally all method observation phosphatization visually
The state and observation phosphatization tank liquor of film carry out the judgement dregginess of empirical formula.There is very big risk in such a mode, on the one hand,
It is not energetic to phosphatization slag content, it is difficult to control；On the other hand, experience varies with each individual, and the people of different experiences frequently can lead to mistake
Understanding, therefore, causes phosphatization slag content many by mistake many times, phosphatization tank liquor " quick-fried slag ", and phosphatization circulation line is blocked, and causes whole groove
Phosphating solution is wasted.
The content of the invention
It is an object of the invention to for not accurate enough easily currently with artificial range estimation micro-judgment phosphating solution dregginess
The problem of erroneous judgement, there is provided a kind of phosphatization slag content measurement device.
The technical solution adopted for the present invention to solve the technical problems is：A kind of phosphatization slag content measurement device, including branch
There is ring support, ring support restocking is provided with up big and down small conical graduate, and conical graduate upper portion side wall has on seat, bearing
The scale of phosphating solution pouring volume is read, conical graduate bottom sidewall has the scale for reading sediment height, conical graduate bottom
The vertex of a cone is additionally provided with dismountable screw of blocking up.Take quantitative phosphating solution to import in conical graduate, stand 30~40 minutes, make phosphating solution
Natural sedimentation, by reading the height of phosphatization liquid precipitate, is contrasted with standard, judges whether phosphatization slag content allows actual
Within the scope of, and judge it is enough to need to carry out phosphating solution further control slagging-off, conical graduate bottom external diameter according to result
It is small, it can more accurately carry out reading.After the completion of one-time detection, screw of blocking up is screwed out, bottom of the phosphating solution from conical graduate can be said
Portion is discharged, and conical graduate is cleaned, in case experiment next time.
Preferably, the ring support includes interior ring support and outer ring support, outer shroud holder pivots are arranged on bearing,
Inner ring holder pivots are arranged on outer ring support, and the rotary shaft of interior ring support and outer ring support is mutually perpendicular to.Ensure accurately
Reading, it is necessary to assure the upper surface of sediment is vertical with the axis of conical graduate, using natural sedimentation, it is necessary to ensure taper amount
Cup axis, which can guarantee that, to be stood vertically, and conical graduate is erected on interior ring support, and interior ring support and outer ring support have mutually
Vertical rotational freedom, ensures that conical graduate is in axis vertical using the self gravitation of conical graduate and internal phosphating solution
State.
Preferably, the bearing includes base, base is provided with cantilever, annular branch provided with a vertical rod, vertical rod side
Frame is arranged on cantilever end.As other preferred, the bearing includes base, two vertical rods is oppositely arranged on base, two are stood
Described ring support is fixed between bar by cantilever erection.
Preferably, being provided with micromachine, motor on the ring support or with the bearing of ring support junction
The fixed eccentric block for being provided with eccentric vibrating in rotating shaft.Conical graduate is due to up big and down small.Some in precipitation process is precipitated
Thing slides along side wall, causes inactive state lower bottom part sediment top surface to have pyramidal pits, therefore sets micromachine, in precipitation
Start afterwards to a certain extent, driving eccentric block to rotate makes support have high-frequency vibration by a small margin, drive conical graduate vibration, make
Bottom sediment surfacing, makes reading more accurate.
Preferably, being connected with timer on the micromachine start-up circuit.It can be set in on-test, when heavy
Carry out vibrating for 1-2 minutes when shallow lake process is carried out 30~40 minutes.
Preferably, being provided with torsion spring at the interior ring support and outer shroud rack shaft.Torsion spring can prevent interior ring support and
Outer ring support inordinate rotation, causes phosphating solution to be poured out, and torsion spring energy ancillary vibration, is formed and is imitated with good dither by a small margin
Really.Motor can also be not provided with, precipitation one end time after, artificial vibration conical graduate, now torsion spring can keep once-through operation
The vibration of later long period.
The present invention detects the phosphatization slag of phosphating solution using conical graduate, realizes the quantization measurement of phosphatization slag, makes phosphating solution
Phosphatization slag control it is more accurate；Measurement apparatus can guarantee that sediment upper surface is concordant with scale, just using the support of self-regulation
In reading；Measurement apparatus carries micromachine and provides frequency low-amplitude vibration, eliminates the pit of sediment upper surface, makes reading more accurate
Really.
Brief description of the drawings
Fig. 1 is a kind of structural representation of the present invention.
Fig. 2 is the ring support structural representation of the present invention.
In figure：1. base, 2. vertical rods, 3. cantilevers, 4. micromachines, 5. conical graduates, 6. block up screw, 7. annular branch
Frame, 8. eccentric blocks, 9. torsion springs, 10 outer ring supports, ring support in 11..
Embodiment
Below by specific embodiment and the present invention is further described with reference to accompanying drawing.
Embodiment：A kind of phosphatization slag content measurement device, as shown in Figure 1.The present apparatus includes bearing, and bearing includes being placed on
The base 1 of table top, the upper surface of base 1 is provided with vertical rod 2, and vertical rod is adjustably provided with cantilever 3 about 2, cantilever end is connected with annular
Support 7.Ring support restocking is provided with up big and down small conical graduate 5, and the upper portion side wall of conical graduate 5 is carved with reading phosphatization liquid measure
Scale, bottom sidewall be carved with read precipitation object amount scale.The bottom vertex of a cone of conical graduate 5 passes through screw of removably blocking up
6 block, and can say that screw of blocking up is turned on during cleaning.
As shown in Figure 1, 2, cantilever 3 is fixed with micromachine 4, the rotating shaft of micromachine 4 close to the bottom of ring support 7
Be fixed with eccentric block 8, the start-up circuit of micromachine 4 is also associated with timer, for control micromachine the startup time and
Continuous working period.The structure of ring support 7 is as shown in Fig. 2 ring support includes outer ring support 10 and interior ring support 11, outer shroud branch
Frame 10 may be rotatably mounted at the end of cantilever 3, and interior ring support 11 may be rotatably mounted on the inside of outer ring support, outer ring support 10 and interior
The rotating shaft of ring support 11 is mutually perpendicular to.In the rotation for rotating junction, outer ring support and cantilever of outer ring support and interior ring support
Junction sets torsion spring respectively.Conical graduate is erected on interior ring support.
During experiment, conical graduate is set up onto interior ring support, and takes 1000ml phosphating solutions to import in conical graduate, taper
Under measuring cup Action of Gravity Field, rotation makes conical graduate center line vertical automatically for interior ring support and outer ring support, it is ensured that sediment upper surface
It is concordant with scale.By timer timing, when precipitating 25 minutes, start minitype motor driving eccentric block and rotate, make annular branch
Frame drives conical graduate to carry out frequency low-amplitude vibration, and micromachine continuous firing 2 minutes eliminates sediment upper surface due to taper
The pit that measuring cup sloped sidewall is brought.Precipitation reads the height of sediment after 30 minutes, and highly judges phosphatization according to sediment
Whether the phosphatization slag content of liquid is up to standard.
Claims (6)
1. a kind of phosphatization slag content measurement device, it is characterised in that：Including bearing, there is ring support, ring support on bearing
Restocking is provided with up big and down small conical graduate, and conical graduate upper portion side wall has the scale for reading phosphating solution pouring volume, taper amount
Cup bottom sidewall has the scale for reading sediment height, and the conical graduate bottom vertex of a cone is additionally provided with dismountable block up screw, institute
State on ring support or be provided with fixation on micromachine, machine shaft with the bearing of ring support junction and be provided with bias
Some sediment slides along side wall in the eccentric block of vibration, precipitation process, causes inactive state lower bottom part sediment top
There are pyramidal pits in face, and micromachine starts afterwards to a certain extent in precipitation, and driving eccentric block to rotate makes support have high frequency by a small margin
The vibration of rate, drives conical graduate vibration, makes bottom sediment surfacing, make reading more accurate.
2. a kind of phosphatization slag content measurement device according to claim 1, it is characterised in that：The ring support includes interior
Ring support and outer ring support, outer shroud holder pivots are arranged on bearing, and inner ring holder pivots are arranged on outer ring support, inner ring branch
The rotary shaft of frame and outer ring support is mutually perpendicular to.
3. a kind of phosphatization slag content measurement device according to claim 1 or 2, it is characterised in that：The bearing includes bottom
Seat, base are provided with cantilever provided with a vertical rod, vertical rod side, and ring support is arranged on cantilever end.
4. a kind of phosphatization slag content measurement device according to claim 1 or 2, it is characterised in that：The bearing includes bottom
It is oppositely arranged on seat, base between two vertical rods, two vertical rods and described ring support is fixed by cantilever erection.
5. a kind of phosphatization slag content measurement device according to claim 1, it is characterised in that：The micromachine starts electricity
Timer is connected with road.
6. a kind of phosphatization slag content measurement device according to claim 2, it is characterised in that：The interior ring support and outer shroud
Torsion spring is provided with rack shaft.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310747606.7A CN104342695B (en) | 2013-12-31 | 2013-12-31 | A kind of phosphatization slag content measurement device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310747606.7A CN104342695B (en) | 2013-12-31 | 2013-12-31 | A kind of phosphatization slag content measurement device |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104342695A CN104342695A (en) | 2015-02-11 |
| CN104342695B true CN104342695B (en) | 2017-10-31 |
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ID=52499131
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310747606.7A Expired - Fee Related CN104342695B (en) | 2013-12-31 | 2013-12-31 | A kind of phosphatization slag content measurement device |
Country Status (1)
| Country | Link |
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| CN (1) | CN104342695B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105483689A (en) * | 2015-12-23 | 2016-04-13 | 郑州日产汽车有限公司 | On-line monitoring method for automobile coating phosphated residues |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101301652A (en) * | 2008-01-17 | 2008-11-12 | 上海交通大学 | Device for separating mud and water depending on high-frequency small-amplitude mechanical vibration |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101482385B (en) * | 2009-02-20 | 2010-07-21 | 中建七局第三建筑有限公司 | Sediment detector for filling pile |
| US20110017230A1 (en) * | 2009-07-27 | 2011-01-27 | Memc Electronic Materials, Inc. | Method and System for Processing Abrasive Slurry |
| CN201818794U (en) * | 2010-10-13 | 2011-05-04 | 上海三彩机电设备有限公司 | Sealing structure for rotating main shaft penetrating through wall of cavity body |
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2013
- 2013-12-31 CN CN201310747606.7A patent/CN104342695B/en not_active Expired - Fee Related
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101301652A (en) * | 2008-01-17 | 2008-11-12 | 上海交通大学 | Device for separating mud and water depending on high-frequency small-amplitude mechanical vibration |
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| Publication number | Publication date |
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| CN104342695A (en) | 2015-02-11 |
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