CN104338341B - A kind of injecting type hypergravity bed - Google Patents
A kind of injecting type hypergravity bed Download PDFInfo
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- CN104338341B CN104338341B CN201410526390.6A CN201410526390A CN104338341B CN 104338341 B CN104338341 B CN 104338341B CN 201410526390 A CN201410526390 A CN 201410526390A CN 104338341 B CN104338341 B CN 104338341B
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Abstract
The present invention relates to a kind of injecting type hypergravity bed, comprising: spray chassis, jet chamber's housing, jet chamber's base, heater, post bake circle, injection apparatus, outer hydrops circle, interior hydrops circle, a Ji Qiquan; Wherein, jet chamber's housing is arranged on described jet chamber base; In described jet chamber housing, the described injection chassis being provided with difficult volatilization phase recovery port is arranged on jet chamber's base, a described heater is then arranged on and sprays on chassis, around a heater, spray on chassis and also injection apparatus is installed, a described heater is provided with interior hydrops coil support, this interior hydrops coil support is provided with interior hydrops circle, the inwall of jet chamber's housing is provided with outer hydrops circle, be provided with at the top of jet chamber's housing and volatilely export mutually, close on the inwall at top, Ji Qiquan is installed at jet chamber's housing.
Description
Technical field
The present invention relates to rectifying, recovery, gas-liquid mass transfer technical field, particularly a kind of injecting type hypergravity bed.
Background technology
High-gravity technology is the new technique of the strengthening gas-liquid mass transfer grown up the eighties in last century, and its operation principle is that the hundreds of centrifugal force fields to thousand times of gravity (abbreviation super gravity field) utilizing High Rotation Speed to produce replace conventional gravitational field.Under super gravity field, what present during liquid dispersion flight is very tiny drop, brin state, therefore the specific area of vapour-liquid contact is very large, the mixing of its splendid microcosmic and the boundary regeneration characteristics be exceedingly fast, make it greatly can strengthen mass-transfer progress, height of transfer unit is reduced by 1 order of magnitude.Thus make huge tower become height less than the overweight machine of 2 meters, reach the object increasing efficiency, reduced volume and significantly can reduce energy consumption in some occasion.
Hypergravity bed is the equipment of the continuous rectification process be applied to by high-gravity technology in industrial production, can be widely used in the rectifying of following organic solvent, recovery: methyl alcohol, formaldehyde, toluene, ethanol, ethylene glycol, acetone, ethyl acetate, acetonitrile, oxolane, dimethyl sulfoxide (DMSO), dimethoxym ethane, n-butanol, carrene, silicon ether, cyclohexane, iso-butane, isopropyl alcohol, glacial acetic acid, aceticanhydride, DMF, DMSO, DMAA, DMDA etc.Compared with traditional rectifying column, have the following advantages:
1, device height is low, civil engineering cost is low, floor space is little
Due under Elevated Gravity, gas-liquid two-phase has very large contact area and collision probability, and microcosmic mixing and mass transport process are strengthened greatly, and mass-transfer efficiency can improve ten times, and huge tower is become highly less than the hypergravity bed of 2 meters.The hypergravity bed that 1.8 meters, fuselage is high is equivalent to the conventional rectifying column of 15 meters high.Due to the advantage on hypergravity bed height, compared with traditional rectifying column, in whole design, for the civil engineering cost realized required for rectifying object reduces greatly.The height of tradition required for rectifying column usually reaches more than 10 meters, and even higher, installation requirement is high, and need provide the workbench etc. of operating personnel, and for this reason, civil engineering cost is relatively large.And hypergravity sheet machine equipment height only has (containing base height) more than 2 meters, installation requirement is lower, so civil engineering requires relatively simple, civil engineering costs reduces greatly.Tradition rectifying column, generally needs pedestal and special support, and floor space is large, and hypergravity bed only needs the floor space of about 1 ~ 2 square.
In addition, because traditional rectifying column is higher, in windproof, shockproof, anti-lightning strike etc., there is very high requirement.Hypergravity bed, owing to being arranged on indoor, does not need to carry out special safeguard procedures in above-mentioned several respects.Simultaneously because tower is high, need through certain examination and approval procedures, and hypergravity bed is the same with other indoor equipmenies, just can installation and operation after entirety approves and initiate a project examination & approval, do not need special examination and approval procedures, thus save more front-end fee and use.
2, energy consumption is saved
Hypergravity bed due to volume little, area of dissipation is little, and according to expert appraisal, at identical conditions, hypergravity bed can be more energy-conservation than traditional rectifying column large about 20% ~ 40%.
3, more heat sensitive material is adapted to
Due to hypergravity bed apparatus High Rotation Speed and volume is less, the feed liquid of delay is few, and it is short to hold the liquid time, according to ruuning situation, only have an appointment 1-2 minute in a device by the holdup time for feed liquid, and heat sensitive material can not volatilize in equipment, sex change, thus produce very large economic benefit.At high temperature long-time just resolvent material is applicable to using hypergravity bed very much.
4, easy to operate
Hypergravity bed is compared with traditional rectifying column, and due to highly low, volume is little, operates relative tower convenient a lot.Tower runs needs operator often to go up tower top observation material situation, brings certain hidden danger to safety in production.Meanwhile, move to tower top design component required time longer in tower start, reaching the balance usual shortest time is not less than 30 minutes, operator at this moment between section must observe operation at the scene.And the operation of hypergravity bed is observed very convenient, simultaneously because the start of hypergravity bed is short to equilibration time, general only needs tens minutes, operator need not look at equipment for a long time and examines and can take into account the operation of other equipment, thus alleviate operator's labour intensity and save cost of labor, also ensure that the security of production simultaneously.
5, maintenance is convenient, maintenance cost is low
Generally, traditional rectifying column needs overhaul once every half a year, needs every year to clean filler, and each maintenance needs a couple of days consuming time; And hypergravity bed only needs every half a year by consumable accessorys such as national standard changing machine envelopes, each replacing only needs several hours, simple to operate, keeps in repair also very convenient.
6, discharging of waste liquid
At identical conditions, the discharging of waste liquid of general tower is about 3%, and hypergravity bed can meet client and environmental requirement, and discharge can be controlled in less than 0.5%, has good environment protecting, has good social benefit and Business Economic Benefit simultaneously.
Because hypergravity bed has above-mentioned many-sided advantage compared with rectifying column equipment, replace traditional rectifying column equipment with it, can steel resources be saved to the development of society, extend the service life of earth resource; For the development of enterprise, can save place and space resources, decreasing pollution discharges, and improves the quality of products, pattern of improving management and administration, and reduces productive labor intensity, increases the security of producing.Hypergravity bed has very wide application prospect in the industry such as environmental protection, medicine, chemical industry, is being increasing user-selected use.
Polytype hypergravity bed is there is in prior art, the continuous rectification process realized in single device in industrial production all failed so far by filled type wherein or disc-type hypergravity bed, though invented by Zhejiang Polytechnical University and be successfully applied to the continuous rectification process in industrial production with the deflector type hypergravity bed that Hangzhou Ke-Li Chemical Equipment Co., Ltd. develops jointly, but deflector type hypergravity bed accessory has following defect: (1) deflector type hypergravity bed is due to the existence of mechanical rotor, make the frequency that mechanical breakdown occurs higher, maintenance capacity is large; (2) rotating speed of mechanical rotor is subject to the restriction of material, machining accuracy, installation accuracy, and its hypergravity amplitude is less than the hypergravity amplitude of jet, and the operating efficiency of equipment and disposal ability are all decreased.
Summary of the invention
The object of the invention is to overcome the defect existing for deflector type hypergravity bed of the prior art, thus a kind of injecting type hypergravity bed is provided.
To achieve these goals, the invention provides a kind of injecting type hypergravity bed, comprising: spray chassis, jet chamber's housing, jet chamber's base, heater, post bake circle, injection apparatus, outer hydrops circle, interior hydrops circle, a Ji Qiquan; Wherein,
Described jet chamber housing is arranged on described jet chamber base; In described jet chamber housing, the described injection chassis being provided with difficult volatilization phase recovery port is arranged on jet chamber's base, a described heater is then arranged on and sprays on chassis, around a heater, spray on chassis and also injection apparatus is installed, a described heater is provided with interior hydrops coil support, this interior hydrops coil support is provided with interior hydrops circle, the inwall of jet chamber's housing is provided with outer hydrops circle, be provided with at the top of jet chamber's housing and volatilely export mutually, close on the inwall at top, Ji Qiquan is installed at jet chamber's housing.
In technique scheme, described injection apparatus circlewise, comprising: nozzle, nozzle carrier, nozzle install ring pipe, nozzle installs annular pipe support and jetting fluid import; Wherein,
Described nozzle installation ring pipe is installed annular pipe support by described nozzle and is fixed on injection chassis, its inner connection, jetting fluid import and nozzle are installed ring pipe and are communicated with, and nozzle is fixed on to spray on chassis and install ring pipe with described nozzle by nozzle carrier and is communicated with;
At nozzle, annular Bottomhole pressure is installed after the mixing jetting liquid with certain pressure enters injection apparatus by jetting fluid import, is finally sprayed by each nozzle, form liquid grain pearl.
In technique scheme, described nozzle is with rotating room.
In technique scheme, a described heater comprises: at the bottom of Heating medium, sidewall, cover of heater, heater and inner bag; Wherein,
Form the cavity of an inner hollow at the bottom of described sidewall, cover of heater, heater, the cavity of this inner hollow is called for short cavity, and described inner bag is positioned at this cavity; Heating medium is communicated with inner bag, and inner bag also has inner bag hole; High in the middle of described cover of heater, both sides are low, it has the tapering of 10-20 °, has slip liquid edge in the edge of cover of heater; Described sidewall has multiple hole, to export as the first heating agent; The bottom of cavity formed at the bottom of by described sidewall, cover of heater, heater, the periphery of Heating medium also have the second heating agent outlet, and described Heating medium and the outlet of the second heating agent all have Valve controlling; When heating agent sprays into, the valve opening of Heating medium, the valve closing of the second heating agent outlet, heating agent enters inner bag through Heating medium, then enter in described cavity by inner bag hole, sprayed in hypergravity bed by the first heating agent outlet on sidewall, finally flow back to heating source.
In technique scheme, described interior hydrops circle comprises hydrops circle in one deck, hydrops circle in two layers, hydrops circle in hydrops circle and four layers in three layers, hydrops circle funneling in these, the interval keeping certain is each other arranged on interior hydrops coil support according to order from top to bottom; In each, hydrops circle all adopts fish scale sieve plate to make, and down, each fish scale tripe is staggered the fish scale tripe of described fish scale sieve plate.
In technique scheme, gap is arranged at the bottom of described interior hydrops coil support, the non-edging of lower limb of described fish scale sieve plate.
In technique scheme, described outer hydrops circle comprises the outer hydrops circle of one deck, two layers of outer hydrops circle, three layers of outer hydrops circle, four layers of outer hydrops circle, five layers of outer hydrops circle; These outer hydrops circles all become annular, and adopt fish scale sieve plate to make, and down, each fish scale tripe is staggered the fish scale tripe of described fish scale sieve plate.
In technique scheme, described post bake circle comprises Heating medium, heating agent outlet, ring pipe, puff prot; Described Heating medium and heating agent outlet all have Valve controlling.
In technique scheme, described Ji Qiquan comprises outer Ji Qiquan and interior Ji Qiquan, and described interior Ji Qiquan is fixed on the inwall of jet chamber's case top by interior collection vapour coil, and outer Ji Qiquan is then direct to be connected with the inwall of jet chamber's case top.
The invention has the advantages that:
1, injecting type hypergravity bed of the present invention eliminates centrifugal rotor, saves a large amount of power consumption, steel consumption and flight-line maintenance amount.Impressed pressure source (usually using membrane pump) makes mixing material define High Rotation Speed jet at each nozzle place, firing rate 5-50 rice per second, and the speed thrown away than centrifugal force is high tens times, and in hypergravity bed, forms numerous liquid grain pearl rapidly.Between these pearl and steam, mutual mass transfer turns heat, the height of efficiency, is not far that centrifugal force can ratio.The rotating speed of centrifugal rotor and diameter, be all subject to material and machining accuracy, installation accuracy restrict.And the mechanical movement of various pump (membrane pump or centrifugal pump or plunger displacement pump), the mechanical movement of relative centrifugal rotor, amount of exercise is little, and pressure and jet velocity increasing degree are very large on the contrary;
2, injecting type hypergravity bed of the present invention eliminates the firing equipments such as heating kettle, and heating agent directly enters hypergravity bed, and carry out mass-and heat-transfer with numerous granular liquid pearl, heat transfer efficiency is than the raising more than 50% of deflector type, and thermal loss also reduces more than 50%.
3, the manufacturing cost of injecting type hypergravity bed of the present invention is than few more than a times of deflector type; The hypergravity bed of deflector type has mechanical rotor and high power motor transmission thereof, and power is comparatively large, needs steel more; Only its manufacturing cost of feed liquid heating kettle has inherently exceeded the manufacturing cost of hypergravity bed.
Accompanying drawing explanation
Fig. 1 is the structural representation of injecting type hypergravity bed of the present invention;
Fig. 2 is the sectional view of the injection apparatus in injecting type hypergravity bed of the present invention;
Fig. 3 is the installation diagram of the injection apparatus in injecting type hypergravity bed of the present invention;
Fig. 4 is the schematic diagram on the injection chassis in injecting type hypergravity bed of the present invention;
Fig. 5 is the schematic perspective view of the injection apparatus in injecting type hypergravity bed of the present invention;
Fig. 6 is the schematic diagram of the Ji Qiquan in injecting type hypergravity bed of the present invention;
Fig. 7 (a) is the schematic perspective view of a heater in injecting type hypergravity bed of the present invention;
The sectional view of a heater in Fig. 7 (b) injecting type hypergravity of the present invention bed;
Fig. 8 is the schematic diagram of the interior knot liquid circle in injecting type hypergravity bed of the present invention;
Fig. 9 is the schematic diagram of the outer knot liquid circle in injecting type hypergravity bed of the present invention;
Figure 10 is the partial schematic diagram of the outer knot liquid circle in injecting type hypergravity bed of the present invention;
Figure 11 is the upward view of the interior knot liquid circle in injecting type hypergravity bed of the present invention;
Figure 12 is the upward view of the interior knot liquid circle in injecting type hypergravity bed of the present invention;
Figure 13 is the schematic diagram of outer knot liquid circle in injecting type hypergravity bed of the present invention and housing junction, jet chamber;
Figure 14 is the structural representation of the post bake circle in injecting type hypergravity bed of the present invention.
Drawing explanation
1 sprays chassis 2 jet chamber housing
3 jet chamber's base No. 4 one times heaters
4-1 Heating medium 4-2 slips liquid edge
4-3 first heating agent outlet 4-4 sidewall
4-6 cover of heater at the bottom of 4-5 heater
4-7 second heating agent outlet 4-8 inner bag
4-9 inner bag hole 5 post bake circle
5-1 Heating medium 5-2 ring pipe
5-3 steam jet 5-4 heating agent exports
6 flow rate of heat medium controller 7 pressure sensor devices
8 multi-point temp sensing devices 9 are volatile to be exported mutually
10 Heating medium 11 jetting fluid imports
12 difficult volatilization phase recovery port 13 nozzles install ring pipe
14 nozzle 15 nozzle carriers
16 nozzles install annular pipe support 17 bolt
18 shell flange 19 end bearing flanges
The outer Ji Qiquan of 20 nut 21
Hydrops coil support in collection vapour circle 23 in 22
23-1 column 23-2 retainer ring
Hydrops circle in 23-3 gap 24 one deck
Hydrops circle in 26 3 layers, hydrops circle in 25 2 layers
The outer hydrops circle of hydrops circle 28 one deck in 27 4 layers
29 2 layers of outer hydrops circle, 30 3 layers of outer hydrops circle
31 4 layers of outer hydrops circle, 32 5 layers of outer hydrops circle
Collection vapour coil 34 hole in 33
Detailed description of the invention
Now the invention will be further described by reference to the accompanying drawings.
With reference to figure 1, injecting type hypergravity bed of the present invention comprises: spray chassis 1, jet chamber's housing 2, jet chamber's base 3, heater 4, post bake circle 5, injection apparatus, outer hydrops circle, interior hydrops circle, Ji Qiquan; Wherein, described jet chamber housing 2 is arranged on described jet chamber base 3; In described jet chamber housing 2, described injection chassis 1 is arranged on jet chamber's base 3, a described heater 4 is then arranged on and sprays on chassis 1, around a heater 4, spray on chassis 1 and also injection apparatus is installed, a described heater 4 is provided with interior hydrops coil support 23, this interior hydrops coil support 23 is for installing interior hydrops circle, jet chamber's housing 2 inwall is provided with outer hydrops circle, be provided with at the top of jet chamber's housing 2 and volatilely export 9 mutually, close on the inwall at top, Ji Qiquan is installed at jet chamber's housing 2.
Below all parts in injecting type hypergravity bed is described further.
With reference to figure 4, described injection chassis 1 is a disk, has a hole in the middle part of it, as Heating medium hole 10, and on injection chassis 1, also has the hole for the hole 34 by jetting fluid import 11 and phase recovery port 12 of volatilizing as difficulty.
Described jet chamber housing 2 is containers of two ends round platform, intermediate cylindrical, and its maximum gauge is 1200mm, high 1600mm, as shown in Figure 3, bolt 17 can be adopted shell flange 18, end bearing flange 19 to be connected and fixed with injection chassis 1 and be integrated.
With reference to figure 2, Fig. 3 and Fig. 5, circlewise, it comprises nozzle 14 to described injection apparatus, nozzle carrier 15, nozzle are installed ring pipe 13, nozzle and installed annular pipe support 16 and jetting fluid import 11; Described nozzle is installed ring pipe 13 inside and is communicated with, and jetting fluid import 11 and nozzle are installed ring pipe 13 and be communicated with; The mixing jetting liquid with certain pressure installs flowing in ring pipe 13 at nozzle after entering injection apparatus by jetting fluid import 11, finally can be sprayed by each nozzle 14, formation liquid grain pearl.Described nozzle is installed annular pipe support 16 and is fixed on injection chassis 1 for nozzle being installed ring pipe 13, and described nozzle carrier 15 sprays chassis 1 for being fixed on by nozzle 14.In the present embodiment, in this injection apparatus, nozzle 14, nozzle carrier 15 and nozzle install each own 8 of annular pipe support 16, and in other embodiments, their quantity can change as required.In addition, in the present embodiment, described nozzle 14 is with rotating room, and in other embodiments, described nozzle 14 also can Bu Dai rotating room.The nozzle diameter of nozzle 14 is 0.3---5mm.
With reference to figure 2, Fig. 3, Fig. 7 (a) and Fig. 7 (b), a described heater 4 comprises: 4-5 and inner bag 4-8 at the bottom of Heating medium 4-1, sidewall 4-4, cover of heater 4-6, heater; Wherein, at the bottom of described sidewall 4-4, cover of heater 4-6, heater, 4-5 forms the cavity of an inner hollow, and the cavity of this inner hollow is called for short cavity, and inner bag 4-8 is positioned at this cavity; Heating medium 4-1 is communicated with inner bag 4-8, and inner bag 4-8 also has inner bag hole 4-9.Described cover of heater 4-6 centre is high, both sides are low, and it has the tapering of 10-20 °, is beneficial to condensate liquid dirty.Have in the edge of cover of heater 4-6 and slip liquid along 4-2, this slips liquid along 4-2 except having thermolysis, can also prevent condensate liquid from again being blown thermal evaporation by heating agent.The bottom of Heating medium 4-1 is communicated with flow rate of heat medium controller 6, controls appropriate heating agent flow into a heater 4 from heating source by flow rate of heat medium controller 6, to provide just to the heat needed.Described sidewall 4-4 has multiple hole, to export 4-3 as the first heating agent.The bottom of cavity that 4-5 is formed at the bottom of by described sidewall 4-4, cover of heater 4-6, heater, the periphery of cavity Heating medium 4-1 also have the second heating agent outlet 4-7.Heating medium 4-1 and the second heating agent outlet 4-7 all has Valve controlling, when heating agent sprays into, the valve opening of Heating medium 4-1, the valve closing of the second heating agent outlet 4-7, heating agent enters inner bag 4-8 through Heating medium 4-1, then enter in described cavity by inner bag hole 4-9, sprayed in hypergravity bed by the first heating agent outlet 4-3 on sidewall 4-4, finally flow back to heating source.In this course, the air outside heating agent and a heater 4 does exchange heat.The heating agent mentioned in the application can be steam, also can be heat conduction wet goods heat transfer substance.
Described interior hydrops circle is arranged on interior hydrops coil support 23, in the present embodiment, as illustrated in figures 1 and 8, described interior hydrops circle to comprise in one deck in 24, two layers, hydrops circle in 25, three layers, hydrops circle hydrops circle 27 in hydrops circle 26 and four layers, in these, the infundibulate varied in size all made by hydrops circle, and the interval keeping certain is each other arranged on the column 23-1 of interior hydrops coil support 23 according to order from top to bottom.Described column 23-1 has multiple, by retainer ring 23-2, these columns 23-1 is connected into support shape.The bottom of interior hydrops coil support 23 also has gap 23-3, and this gap makes the liquid trickled on interior hydrops coil support 23 scatter for droplet-like, can not form liquid level, contributes to increasing mass-and heat-transfer surface area.In these, hydrops circle all adopts fish scale sieve plate to make, and as is illustrated by figs. 11 and 12, down, this is beneficial to lower of condensate liquid dispersion to the fish scale tripe of fish scale sieve plate, instead of forms subsurface flow, if form liquid level will be unfavorable for heat transfer.Lip(ped) sieve hole size on fish scale sieve plate is between 10*10mm, and interval is also between 10mm, and fish scale tripe height 5mm, each fish scale tripe is staggered.The non-edging of lower limb of fish scale sieve plate, this contributes to liquid equally and scatters for droplet-like, can not form liquid level, increases mass-and heat-transfer surface area.
Described outer hydrops circle is positioned on the inwall of jet chamber's housing 2, and in the present embodiment, as shown in Figure 1, outer hydrops circle comprises the outer outer hydrops circle of 28, two layers, hydrops circle 29, three layers of outer hydrops circle 30, four layers of outer hydrops circle 31, the five layers of outer hydrops circle 32 of one deck; These outer hydrops circles all make annular, as shown in Fig. 9, Figure 10 and Figure 13, these outer hydrops circles all adopt fish scale sieve plate to make, the fish scale tripe of fish scale sieve plate down, its lower limb is not edging, and the lip(ped) sieve hole size on fish scale sieve plate is between 10*10mm, and interval is also between 10mm, fish scale tripe height 5mm, each fish scale tripe is staggered.
Described post bake circle 5 provides heat power for the volatile rising body of escaping out that evaporates mutually, and therefore see Fig. 1, its position is in bed body middle and upper part.As shown in figure 14, post bake circle 5 comprises Heating medium 5-1, heating agent outlet 5-4, ring pipe 5-2, puff prot 5-3; Heating medium 5-1 and heating agent outlet 5-4 all has Valve controlling.In the present embodiment, the valve closing of heating agent outlet 5-4.Heating agent is flowed by ring pipe 5-2 after being entered by Heating medium 5-1, eventually passes puff prot 5-3 and sprays, achieve post bake.
Described Ji Qiquan comprises outer collection vapour circle 21 and interior collection vapour circle 22, and this is conducive to the contact increasing condensate liquid and condensation object, and the condensation being conducive to condensate liquid is descending.As shown in Figure 6, described interior collection vapour circle 22 is fixed on the inwall at jet chamber's housing 2 top by interior collection vapour coil 33, collects vapour circle 21 outward and is then directly connected with the inwall at jet chamber's housing 2 top.Volatile mutually by after described Ji Qiquan collection, the more volatile outlet 9 mutually through jet chamber's housing 2 top is volatilized away.
It is more than the structure explanation to injecting type hypergravity bed of the present invention.Operationally, the mixing material by temperature, pressure, flow-control enters from the jetting fluid import 11 of injection apparatus injecting type hypergravity bed of the present invention, sprays from nozzle 14, forms countless liquid pearl; With this simultaneously, be stressed, the heating agent (as water vapour) of flow-control enters from the Heating medium 4-1 of a heater, spray from the heating agent spout 4-3 of a heater 4, the heating agent of ejection heats to countless mixed liquor pearl, impels its volatile component (as alcohol) to be evaporated to steam and rises.The steam that volatile component is formed in uphill process also can give other liquid pearls heat, and heat own reduce, if there is no second heating apparatus, a part of volatile component steam will condensation descending, so arrange post bake circle 5.The liquid pearl risen constantly is evaporated because of volatile component, liquid bead footpath constantly reduces, the liquid pearl do not gone up, main component is difficult volatile matter (as water), fall after rise under gravity, dispelled by the liquid pearl of continuation rising and steam collision again, major part is received descending by the multilayer hydrops circle of surrounding.Like this, mixed liquor forms a large amount of liquid pearl and is suitably heated in this hypergravity bed, volatile component is separated with difficult volatile ingredient, volatile component exports 9 discharges mutually by volatile, reclaimed by the condenser condenses be connected to above this hypergravity bed, descending difficult volatile ingredient enters container from recovery port 12 and drains or rectifying separation again.
It should be noted last that, above embodiment is only in order to illustrate technical scheme of the present invention and unrestricted.Although with reference to embodiment to invention has been detailed description, those of ordinary skill in the art is to be understood that, modify to technical scheme of the present invention or equivalent replacement, do not depart from the spirit and scope of technical solution of the present invention, it all should be encompassed in the middle of right of the present invention.
Claims (9)
1. an injecting type hypergravity bed, it is characterized in that, comprising: spray chassis (1), jet chamber's housing (2), jet chamber's base (3), heater (4), post bake circle (5), injection apparatus, outer hydrops circle, interior hydrops circle, Ji Qiquan; Wherein,
Described jet chamber housing (2) is arranged on described jet chamber base (3), in described jet chamber housing (2), the described injection chassis (1) being provided with difficult volatilization phase recovery port (12) is arranged on jet chamber's base (3), a described heater (4) is then arranged on sprays on chassis (1), around a heater (4), spray on chassis (1) and also injection apparatus is installed, a described heater (4) is provided with interior hydrops coil support (23), this interior hydrops coil support (23) is provided with interior hydrops circle, the inwall of jet chamber's housing (2) is provided with outer hydrops circle, volatile outlet (9) is mutually provided with at the top of jet chamber's housing (2), close on the inwall at top, Ji Qiquan is installed at jet chamber's housing (2).
2. injecting type hypergravity bed according to claim 1, it is characterized in that, described injection apparatus circlewise, comprising: nozzle (14), nozzle carrier (15), nozzle install ring pipe (13), nozzle installs annular pipe support (16) and jetting fluid import (11); Wherein,
Described nozzle installation ring pipe (13) is installed annular pipe support (16) by described nozzle and is fixed in injection chassis (1), its inner connection, jetting fluid import (11) and nozzle are installed ring pipe (13) and are communicated with, and nozzle (14) is fixed on to spray on chassis (1) and install ring pipe (13) with described nozzle by nozzle carrier (15) and is communicated with;
The mixing jetting liquid with certain pressure installs flowing in ring pipe (13) at nozzle after entering injection apparatus by jetting fluid import (11), is finally sprayed by each nozzle (14), formation liquid grain pearl.
3. injecting type hypergravity bed according to claim 2, is characterized in that, described nozzle (14) is with rotating room.
4. injecting type hypergravity bed according to claim 1, it is characterized in that, a described heater (4) comprising: (4-5) and inner bag (4-8) at the bottom of Heating medium (4-1), sidewall (4-4), cover of heater (4-6), heater; Wherein,
At the bottom of described sidewall (4-4), cover of heater (4-6), heater, (4-5) forms the cavity of an inner hollow, and the cavity of this inner hollow is called for short cavity, and described inner bag (4-8) is positioned at this cavity; Heating medium (4-1) is communicated with inner bag (4-8), and inner bag (4-8) also has inner bag hole (4-9); Described cover of heater (4-6) centre is high, both sides are low, and it has the tapering of 10-20 °, has slip liquid along (4-2) in the edge of cover of heater (4-6); Described sidewall (4-4) has multiple hole, to export (4-3) as the first heating agent; The bottom of cavity that (4-5) is formed at the bottom of by described sidewall (4-4), cover of heater (4-6), heater, the periphery of Heating medium (4-1) also have the second heating agent outlet (4-7), and described Heating medium (4-1) and the second heating agent export (4-7) all has Valve controlling; When heating agent sprays into, the valve opening of Heating medium (4-1), the valve closing of the second heating agent outlet (4-7), heating agent enters inner bag (4-8) through Heating medium (4-1), then enter in described cavity by inner bag hole (4-9), sprayed in hypergravity bed by the first heating agent outlet (4-3) on sidewall (4-4), finally flow back to heating source.
5. injecting type hypergravity bed according to claim 1, it is characterized in that, described interior hydrops circle comprises hydrops circle (24) in one deck, hydrops circle (25) in two layers, hydrops circle (27) in hydrops circle (26) and four layers in three layers, hydrops circle funneling in these, the interval keeping certain is each other arranged on interior hydrops coil support (23) according to order from top to bottom; In each, hydrops circle all adopts fish scale sieve plate to make, and down, each fish scale tripe is staggered the fish scale tripe of described fish scale sieve plate.
6. injecting type hypergravity bed according to claim 5, is characterized in that, gap (23-3) is arranged at the bottom of described interior hydrops coil support (23), the non-edging of lower limb of described fish scale sieve plate.
7. injecting type hypergravity bed according to claim 1, it is characterized in that, described outer hydrops circle comprises the outer hydrops circle (28) of one deck, two layers of outer hydrops circle (29), three layers of outer hydrops circle (30), four layers of outer hydrops circle (31), five layers of outer hydrops circle (32); These outer hydrops circles all become annular, and adopt fish scale sieve plate to make, and down, each fish scale tripe is staggered the fish scale tripe of described fish scale sieve plate.
8. injecting type hypergravity bed according to claim 1, it is characterized in that, described post bake circle (5) comprises Heating medium (5-1), heating agent outlet (5-4), ring pipe (5-2), puff prot (5-3); Described Heating medium (5-1) and heating agent outlet (5-4) all have Valve controlling.
9. injecting type hypergravity bed according to claim 1, it is characterized in that, described Ji Qiquan comprises outer Ji Qiquan (21) and interior Ji Qiquan (22), described interior Ji Qiquan (22) is fixed on the inwall at jet chamber's housing (2) top by interior collection vapour coil (33), and outer Ji Qiquan (21) is then directly connected with the inwall at jet chamber's housing (2) top.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410526390.6A CN104338341B (en) | 2014-09-30 | 2014-09-30 | A kind of injecting type hypergravity bed |
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| CN201410526390.6A CN104338341B (en) | 2014-09-30 | 2014-09-30 | A kind of injecting type hypergravity bed |
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| CN104338341A CN104338341A (en) | 2015-02-11 |
| CN104338341B true CN104338341B (en) | 2015-12-30 |
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| DE1078148B (en) * | 1957-07-20 | 1960-03-24 | Philips Nv | Gas separation column with a device for distributing liquid gas |
| DD215240A1 (en) * | 1983-06-02 | 1984-11-07 | Petrolchemisches Kombinat | Liquid-gas CONTACT DEVICE |
| RU2087518C1 (en) * | 1993-10-11 | 1997-08-20 | Геннадий Сергеевич Юр | Method and installation for processing liquid hydrocarbon raw material |
| CN1215620A (en) * | 1997-10-27 | 1999-05-05 | 王成 | Plate tower for mass-transfer process with thermal reaction |
| CN2465756Y (en) * | 2001-02-26 | 2001-12-19 | 符知民 | Jet atomizing flash tower |
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Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1078148B (en) * | 1957-07-20 | 1960-03-24 | Philips Nv | Gas separation column with a device for distributing liquid gas |
| DD215240A1 (en) * | 1983-06-02 | 1984-11-07 | Petrolchemisches Kombinat | Liquid-gas CONTACT DEVICE |
| RU2087518C1 (en) * | 1993-10-11 | 1997-08-20 | Геннадий Сергеевич Юр | Method and installation for processing liquid hydrocarbon raw material |
| CN1215620A (en) * | 1997-10-27 | 1999-05-05 | 王成 | Plate tower for mass-transfer process with thermal reaction |
| CN2465756Y (en) * | 2001-02-26 | 2001-12-19 | 符知民 | Jet atomizing flash tower |
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