CN104324530B - Waste alcohol precipitation separation device in casing slag - Google Patents
Waste alcohol precipitation separation device in casing slag Download PDFInfo
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- CN104324530B CN104324530B CN201410579876.6A CN201410579876A CN104324530B CN 104324530 B CN104324530 B CN 104324530B CN 201410579876 A CN201410579876 A CN 201410579876A CN 104324530 B CN104324530 B CN 104324530B
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Abstract
The present invention relates to a kind of heparin precipitation and its waste alcohol segregation apparatus.It includes being desorbed tank, alcohol precipitation tank, waste alcohol storage tank, air accumulator and vacuum pump, desorption tank lower end is connected to alcohol precipitation tank upper end by pipeline, alcohol precipitation tank upper end is equipped with vacuum-pumping tube, the other end of vacuum-pumping tube connects air accumulator upper end, side, air accumulator upper end connects vacuum pump by pipeline, alcohol precipitation tank side is near lower end position waste alcohol recovery tube, waste alcohol recovery tube leads to waste alcohol storage tank upper end, and equipped with delivery pump on waste alcohol recovery tube, alcohol precipitation tank lower end is equipped with precipitation delivery pipe, equipped with drain valve on precipitation delivery pipe, precipitation delivery pipe lower end is equipped with precipitation recycling bin.Advantage is desorption liquid can either to be made the most sufficiently to be transported to settling tank improve production efficiency, effectively ethanol can be separated with heparin precipitation mixed solution on the basis of reducing power set again, reclaim waste alcohol solution in time, play energy-saving and emission-reduction and effectively reduce production cost effect.
Description
Technical field
The present invention relates to heparin precipitation and its waste alcohol separation field, be specifically related to a kind of heparin precipitation and its waste alcohol segregation apparatus.
Background technology
In heparin production process, it is adsorbed with the resin of heparin after desorption, during ethanol precipitation heparin, desorption liquid arrives settling tank and takes long enough to affect production efficiency and desorption liquid and be not easily accessible settling tank in being adsorbed in resin, affects yield, and repetitive operation just increases production cost;After ethanol precipitation terminates, waste alcohol separates in production general by the way of centrifugal with heparin precipitation, but containing substantial amounts of salt in precipitated liquid, bigger to centrifugation apparatus corrosivity, and centrifugal postheparin easily loses when reclaiming, dismounting centrifugation apparatus operation is the most troublesome, and the power of centrifugation apparatus is relatively big, increases production cost.
Summary of the invention
In order to solve the problems referred to above, the present invention proposes a kind of heparin precipitation and its waste alcohol segregation apparatus, design the most ingenious, easy to use, desorption liquid can either be made the most sufficiently to be transported to settling tank and to improve production efficiency, waste alcohol can be effectively made to separate with heparin after precipitation terminates again, simple to operate, and production cost can be effectively reduced.
In order to reach foregoing invention purpose, the present invention proposes techniques below scheme:
Heparin precipitation and its waste alcohol segregation apparatus, it includes being desorbed tank, alcohol precipitation tank, waste alcohol storage tank, air accumulator and vacuum pump, desorption tank lower end is connected to alcohol precipitation tank upper end by pipeline, alcohol precipitation tank upper end is equipped with vacuum-pumping tube, the other end of vacuum-pumping tube connects air accumulator upper end, side, air accumulator upper end connects vacuum pump by pipeline, alcohol precipitation tank side is near lower end position waste alcohol recovery tube, waste alcohol recovery tube leads to waste alcohol storage tank upper end, and equipped with delivery pump on waste alcohol recovery tube, alcohol precipitation tank lower end is equipped with precipitation delivery pipe, equipped with drain valve on precipitation delivery pipe, precipitation delivery pipe lower end is equipped with precipitation recycling bin.
nullDescribed alcohol precipitation tank includes driving motor、Shaft、Paddle、Manhole、Tank body,Tank body upper end is cylindric tank body,Lower end is cone-shaped tank body,Cone-shaped tank body is connected to cylindric tank body lower end,Cylindric tank body upper end is equipped with driving motor,Motor lower end is driven to connect shaft,Shaft gos deep into tank interior through tank body upper end,Equipped with paddle on the shaft of tank interior,Lower end, cylindric tank body side is equipped with waste alcohol recovery tube,Waste alcohol recovery tube leads to waste alcohol storage tank upper end,And equipped with delivery pump on waste alcohol recovery tube,Side, cylindric tank body upper end connects desorption tank by pipeline,Cylindric tank body upper end opposite side connects air accumulator by vacuum-pumping tube,Cylindric tank body upper end also has manhole,Manhole cover it is stamped on manhole,Cone-shaped tank body lower end is equipped with precipitation delivery pipe,Equipped with drain valve on precipitation delivery pipe,Precipitation delivery pipe lower end is equipped with precipitation recycling bin.
Described side, air accumulator upper end connects vacuum-pumping tube, and vacuum-pumping tube gos deep into tank body of air storage tank inner bottom part through air accumulator upper end, and side, air accumulator upper end connects also by pipeline vacuum pump, and air accumulator lower end is equipped with residul discharging valve.Equipped with observing visor on vacuum-pumping tube.
It is an advantage of the invention that design is the most ingenious, easy to use, desorption liquid can either be made the most sufficiently to be transported to settling tank and to improve production efficiency, effectively ethanol can be separated with heparin precipitation mixed solution on the basis of reducing power set again, reclaim waste alcohol solution in time, play energy-saving and emission-reduction and effectively reduce production cost effect.
Accompanying drawing explanation
Fig. 1 is the schematic diagram of the present invention.
Detailed description of the invention
In order to the present invention is further described, introduce below in conjunction with Figure of description:
Referring to the drawings 1, heparin precipitation and its waste alcohol segregation apparatus, it includes being desorbed tank 1, alcohol precipitation tank 2, waste alcohol storage tank 3, air accumulator 4 and vacuum pump 5, desorption tank 1 lower end is connected to alcohol precipitation tank 2 upper end by pipeline, alcohol precipitation tank 2 upper end is equipped with vacuum-pumping tube, the other end of vacuum-pumping tube connects air accumulator 4 upper end, side, air accumulator 4 upper end connects vacuum pump 5 by pipeline, alcohol precipitation tank 2 side is near lower end position waste alcohol recovery tube, waste alcohol recovery tube leads to waste alcohol storage tank 3 upper end, and equipped with delivery pump 6 on waste alcohol recovery tube, alcohol precipitation tank 2 lower end is equipped with precipitation delivery pipe, equipped with drain valve 7 on precipitation delivery pipe, precipitation delivery pipe lower end is equipped with precipitation recycling bin 8.
nullDescribed alcohol precipitation tank 2 includes driving motor 21、Shaft 22、Paddle 23、Manhole 24、Tank body,Tank body upper end is cylindric tank body 25,Lower end is cone-shaped tank body 26,Cone-shaped tank body 26 is connected to cylindric tank body 25 lower end,Cylindric tank body 25 upper end is equipped with driving motor 21,Motor 21 lower end is driven to connect shaft 22,Shaft 22 gos deep into tank interior through tank body upper end,Equipped with paddle 23 on the shaft 22 of tank interior,Lower end, cylindric tank body 25 side is equipped with waste alcohol recovery tube,Waste alcohol recovery tube leads to waste alcohol storage tank 3 upper end,And equipped with delivery pump 6 on waste alcohol recovery tube,Side, cylindric tank body 25 upper end connects desorption tank 1 by pipeline,Cylindric tank body 25 upper end opposite side connects air accumulator 4 by vacuum-pumping tube,Cylindric tank body 25 upper end also has manhole 24,Manhole cover it is stamped on manhole,Cone-shaped tank body 26 lower end is equipped with precipitation delivery pipe,Equipped with drain valve 7 on precipitation delivery pipe,Precipitation delivery pipe lower end is equipped with precipitation recycling bin 8.
Described side, air accumulator 4 upper end connects vacuum-pumping tube, and vacuum-pumping tube gos deep into tank body of air storage tank inner bottom part through air accumulator 4 upper end, and side, air accumulator upper end connects also by pipeline vacuum pump 5, and air accumulator 4 lower end is equipped with residul discharging valve 41.Equipped with observing visor 42 on vacuum-pumping tube.
nullWhen the present invention uses,Vacuum pump starts evacuation to air accumulator,The most indirectly being also pumped into negative pressure in alcohol precipitation tank,So the desorption liquid in desorption tank is under negative-pressure sucking effect,In suction alcohol precipitation tank,When being observed until not having liquid to pass through by the observation visor being arranged in vacuum-pumping pipeline,Stop vacuum pump,Blind off a line valve,Alcohol precipitation tank starts driving motor and starts to precipitate heparin,After stirring 20 to 30 minutes,Stop stirring,Solution is made to start layering,It is deposited to cone-shaped tank body,Waste alcohol solution is on upper strata,So open manhole,The most floating one layer of impurity is fished for away,Start the delivery pump on waste alcohol recovery tube,Waste alcohol solution is transported in waste alcohol storage tank,Etc. pending recycling,Finally the drain valve on precipitation delivery pipe is opened,Precipitation solution containing a small amount of waste alcohol is put into precipitation recycling bin,Precipitation recovery etc. is pending,Process finishes bundle,Manhole cover is closed,Drain valve cuts out,Delivery pump also ensures to stop,Whole device can carry out next round repeated work.
Claims (3)
1. heparin precipitation and its waste alcohol segregation apparatus, it includes being desorbed tank, alcohol precipitation tank, waste alcohol storage tank, air accumulator and vacuum pump, it is characterized in that being desorbed tank lower end is connected to alcohol precipitation tank upper end by pipeline, alcohol precipitation tank upper end is equipped with vacuum-pumping tube, the other end of vacuum-pumping tube connects air accumulator upper end, side, air accumulator upper end connects vacuum pump by pipeline, alcohol precipitation tank side is provided with waste alcohol recovery tube near lower end position, waste alcohol recovery tube leads to waste alcohol storage tank upper end, and equipped with delivery pump on waste alcohol recovery tube, alcohol precipitation tank lower end is equipped with precipitation delivery pipe, equipped with drain valve on precipitation delivery pipe, precipitation delivery pipe lower end is equipped with precipitation recycling bin.
nullHeparin the most according to claim 1 precipitation and its waste alcohol segregation apparatus,It is characterized in that described alcohol precipitation tank includes driving motor、Shaft、Paddle、Manhole、Tank body,Tank body upper end is cylindric tank body,Lower end is cone-shaped tank body,Cone-shaped tank body is connected to cylindric tank body lower end,Cylindric tank body upper end is equipped with driving motor,Motor lower end is driven to connect shaft,Shaft gos deep into tank interior through tank body upper end,Equipped with paddle on the shaft of tank interior,Lower end, cylindric tank body side is equipped with waste alcohol recovery tube,Waste alcohol recovery tube leads to waste alcohol storage tank upper end,And equipped with delivery pump on waste alcohol recovery tube,Side, cylindric tank body upper end connects desorption tank by pipeline,Cylindric tank body upper end opposite side connects air accumulator by vacuum-pumping tube,Cylindric tank body upper end also has manhole,Manhole cover it is stamped on manhole,Cone-shaped tank body lower end is equipped with precipitation delivery pipe,Equipped with drain valve on precipitation delivery pipe,Precipitation delivery pipe lower end is equipped with precipitation recycling bin.
Heparin the most according to claim 1 precipitation and its waste alcohol segregation apparatus, it is characterized in that described side, air accumulator upper end connects vacuum-pumping tube, vacuum-pumping tube gos deep into tank body of air storage tank inner bottom part through air accumulator upper end, side, air accumulator upper end connects also by pipeline vacuum pump, air accumulator lower end is equipped with residul discharging valve, equipped with observing visor on vacuum-pumping tube.
Priority Applications (1)
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CN201410579876.6A CN104324530B (en) | 2014-10-27 | 2014-10-27 | Waste alcohol precipitation separation device in casing slag |
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CN201410579876.6A CN104324530B (en) | 2014-10-27 | 2014-10-27 | Waste alcohol precipitation separation device in casing slag |
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CN104324530A CN104324530A (en) | 2015-02-04 |
CN104324530B true CN104324530B (en) | 2016-08-03 |
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CN112517572A (en) * | 2020-11-24 | 2021-03-19 | 刘睿峥 | System and method for mixing, cleaning and deslagging medium in settling tank |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102989203A (en) * | 2012-08-21 | 2013-03-27 | 泰州市蓝海环保科技有限公司 | Mud and water separating equipment |
CN203244812U (en) * | 2013-03-20 | 2013-10-23 | 南通天龙畜产品有限公司 | Heparin sodium precipitation and separation device |
CN203613131U (en) * | 2013-10-28 | 2014-05-28 | 如皋市坝新肠衣有限公司 | Heparin sodium production device |
CN203710747U (en) * | 2014-01-22 | 2014-07-16 | 广元市申达实业有限公司 | Heparin sodium sediment separation tank |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
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JP2000312805A (en) * | 1999-04-28 | 2000-11-14 | Houshou:Kk | Turbid water treatment device |
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Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102989203A (en) * | 2012-08-21 | 2013-03-27 | 泰州市蓝海环保科技有限公司 | Mud and water separating equipment |
CN203244812U (en) * | 2013-03-20 | 2013-10-23 | 南通天龙畜产品有限公司 | Heparin sodium precipitation and separation device |
CN203613131U (en) * | 2013-10-28 | 2014-05-28 | 如皋市坝新肠衣有限公司 | Heparin sodium production device |
CN203710747U (en) * | 2014-01-22 | 2014-07-16 | 广元市申达实业有限公司 | Heparin sodium sediment separation tank |
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