CN104307415A - Kerogen separation equipment - Google Patents
Kerogen separation equipment Download PDFInfo
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- CN104307415A CN104307415A CN201410633481.XA CN201410633481A CN104307415A CN 104307415 A CN104307415 A CN 104307415A CN 201410633481 A CN201410633481 A CN 201410633481A CN 104307415 A CN104307415 A CN 104307415A
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- separation container
- casing
- kerogen
- kerogen maceration
- magnet
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Abstract
The invention provides kerogen separation equipment, and relates to the technical field of petroleum industry. The kerogen separation equipment comprises a tank body and a cover plate, wherein the cover plate is flexibly connected with the tank body; a separating container and a stirring mechanism corresponding to the separating container are arranged inside the tank body; the stirring mechanism comprises a rotating mechanism, a magnetic body and a magnetic stirring body; the magnetic stirring body is arranged inside the separating container; the rotating mechanism is connected with the magnetic body and drives the magnetic body to rotate; the magnetic body drives the magnetic stirring body to rotate. In the separation process, the kerogen separation equipment provided by the invention can stir uniformly, and is very good in separation effect.
Description
Technical field
The present invention relates to technical field of petroleum industry, in particular to a kind of kerogen maceration equipment.
Background technology
Kerogen is the dispersed organic matter being insoluble to alkali, non-oxidizing acid and organic solvent in sedimentary rock, is the condensation polymer formed under suitable temperature and pressure, accounts for 90% of organic matter in sedimentary rock.In sedimentary rock, kerogenic separation is the conventional project in geochemical analysis means.Kerogenic separation is the method adopting chemistry, physics, and the inorganic mineral in removing rock and Soluble Organic Matter, make insoluble Organic Matter Enrichment.
In prior art, occurred that some are separated kerogenic equipment, but in the whipping process of these equipment when being separated, majority adopts stirring rod to stir, and stir uneven, mixing effect is poor.
In sum, when how to avoid kerogen maceration device separates, stirring uneven problem, is the problem that current those skilled in the art urgently improves or solves.
Summary of the invention
In view of this, the invention provides a kind of kerogen maceration equipment, during to improve kerogen maceration device separates of the prior art, stir uneven problem.
For achieving the above object, the invention provides following technical scheme:
A kind of kerogen maceration equipment, comprise casing and cover plate, described cover plate is flexibly connected with described casing, the rabbling mechanism of separation container and corresponding described separation container is provided with in described casing, described rabbling mechanism comprises rotating mechanism, magnet and magnetic stirring body, described magnetic stirring body is placed in described separation container, and described rotating mechanism connects described magnet and drives described magnet to rotate, and described magnet drives described magnetic stirring body to rotate.
Preferably, in above-mentioned kerogen maceration equipment, described kerogen maceration equipment also comprises the dividing plate being carried out the inner space of described casing separating, the side of the close described cover plate of described dividing plate is the top of described dividing plate, the side away from described cover plate of described dividing plate is the below of described dividing plate, described separation container is placed in the top of described dividing plate, and described rotating mechanism and magnet are placed in the below of described dividing plate.In kerogenic separation process, separation container needs the absorption carrying out heat, and most mode adopted is all utilize liquid heat transfer medium to carry out heat trnasfer to separation container.The inner space of casing is separated by dividing plate, separation container and rotating mechanism, magnet are also because this has been separation, so, under rotating mechanism, magnet just avoid and be in liquid environment for a long time, thus also just avoid the larger spoilage of the rotating mechanism brought thus.
Preferably, in above-mentioned kerogen maceration equipment, described kerogen maceration equipment also comprises the container cover of mating described separation container.In kerogenic separation process, in separation container, acid can be added.The setting of container cover, can reduce the effusion of pernicious gas; Meanwhile, also because separation container have matched container cover, acid can be stopped by container cover by after thermal evaporation, and container cover absorption, by the acid of thermal evaporation, carries out recycling.
Preferably, in above-mentioned kerogen maceration equipment, the air extractor of the gas detached in described casing in described casing, is provided with.Air extractor is set in casing, the pernicious gas produced can be detached in kerogen maceration process, reduce the release of pernicious gas, ensure the security of separation process.
Preferably, in above-mentioned kerogen maceration equipment, described kerogen maceration equipment also comprises the fixed mount of the position of fixing described separation container.Owing to being provided with fixed mount, separation container is when being heated, and the frame that can be fixed is fixed, and avoids separation container and causes owing to rocking inner separate substance to be toppled over.
Preferably, in above-mentioned kerogen maceration equipment, described fixed mount and described casing are for removably connecting.Fixed mount and casing are arranged to removably connect, so, when needs take out separation container, can fixed mount be taken off, but also can heat transfer medium wherein be changed; When needs carry out kerogenic separation, fixed mount is fixed.
Preferably, in above-mentioned kerogen maceration equipment, described casing is plastic box, and described separation container is plastics separation container.Because casing, separation container are arranged respectively to plastic box, plastics separation container, so, for the corrosive gas produced in kerogen maceration process or liquid, plastic box and plastics separation container all can not be corroded.This kind of setting increases the protection to equipment, extends the service life of equipment.
Preferably, in above-mentioned kerogen maceration equipment, during use, be marked with in described casing to the heat transfer medium of described separation container transferring heat, described separation container is placed among described heat transfer medium.In kerogenic separation process, water can be selected as heat transfer medium, and cost is low, is easy to obtain.
Preferably, in above-mentioned kerogen maceration equipment, in described casing, heating tube is provided with.The setting of heating tube, makes kerogen maceration equipment to heat, then the heat transfer medium in casing is carried out to the transmission of heat.This kind is arranged, and makes kerogen maceration equipment more practical.
Preferably, in above-mentioned kerogen maceration equipment, described separation container is multiple, and described rabbling mechanism is multiple.The rabbling mechanism of multiple separation container and correspondence can carry out kerogenic separation simultaneously, and be separated more, separative efficiency is higher.
Relative to prior art, the present invention includes following beneficial effect: the present invention utilizes the magnetic rabbling mechanism of tool to stir the material in separation container.The magnetic stirring body of rabbling mechanism is placed in separation container, drive magnet by rotating mechanism, and magnet drives magnetic stirring body to stir; Simultaneously, under the effect of the heat transfer medium of the outside of separation container, magnetic stirring body is heated also will do tumbling motion, and the rotational motion that tumbling motion drives with magnet combines, and rabbling mechanism will carry out very thoroughly the material in separation container and stir very uniformly.So, the mixing effect of rabbling mechanism is very good, is beneficial to kerogenic separation.
Accompanying drawing explanation
In order to the clearer explanation embodiment of the present invention or technical scheme of the prior art, be briefly described to the accompanying drawing used required in embodiment or description of the prior art below, apparently, accompanying drawing in the following describes is only some embodiments of the present invention, for those of ordinary skill in the art, under the prerequisite not paying creative work, other accompanying drawing can also be obtained according to these accompanying drawings.
Fig. 1 is that the kerogen maceration equipment axis that the embodiment of the present invention one provides measures intention;
Fig. 2 be the separation container that provides of the embodiment of the present invention one with rabbling mechanism coordinate schematic diagram;
Fig. 3 is the schematic top plan view that magnetic stirring body provided by the invention is placed in separation container;
Fig. 4 is that the kerogen maceration equipment axis that the embodiment of the present invention two provides measures intention;
Fig. 5 be the separation container that provides of the embodiment of the present invention two with container cover coordinate schematic diagram;
Fig. 6 be the separation container that provides of the embodiment of the present invention two with rabbling mechanism coordinate schematic diagram;
Fig. 7 is the kerogen maceration equipment schematic diagram that the embodiment of the present invention three provides.
Wherein, the corresponding relation between Reference numeral and component names is as follows:
101-casing; 102-cover plate; 103-separation container; 104-rotating mechanism; 105-magnet; 106-dividing plate; 107-container cover; 108-air extractor; 109-fixed mount; 110-magnetic stirring body; 111-heating tube.
Detailed description of the invention
Petroleum and natural gas derives from depositional organic matter, for the hyle generating petroleum and natural gas, based on the dispersed organic matter in deposit (rock).And kerogen is exactly the dispersed organic matter being insoluble to alkali, non-oxidizing acid and organic solvent in sedimentary rock, it is the main body of depositional organic matter, accounts for the 80%-90% of total organic matter.Kerogenic separation is the conventional project in geochemical analysis means, also have in prior art and carry out for kerogen the equipment that is separated, but through researcher understanding and put into practice discovery in a large number, the kerogenic separation equipment of prior art, uneven to kerogenic stirring, separating effect is poor.Thus, researcher has carried out large quantifier elimination, provides a kind of kerogen maceration equipment, and the rabbling mechanism that this equipment adopts is that magnetic stirring body is placed in separation container, utilizes magnetic, magnetic stirring body is stirred, stirs, good separating effect.
Also by reference to the accompanying drawings the present invention is described in further detail below by specific embodiment.
Fig. 1, Fig. 2 and Fig. 3 show the kerogen maceration equipment that the embodiment of the present invention one provides, comprise casing 101 and cover plate 102, cover plate 102 is flexibly connected with casing 101, the rabbling mechanism of separation container 103 and corresponding separation container 103 is provided with in casing 101, rabbling mechanism comprises rotating mechanism 104, magnet 105 and magnetic stirring body 110, magnetic stirring body 110 is placed in separation container 103, rotating mechanism 104 connects magnet 105 and drives magnet 105 to rotate, and magnet 105 drives magnetic stirring body 110 to rotate.
Cover plate 102 is flexibly connected with casing 101, opens cover plate 102, can present separation container 103.When being separated kerogen, needed raw material is loaded in separation container 103, and the magnetic stirring body 110 of rabbling mechanism is placed in separation container 103, then in casing 101 inject can transferring heat to the heat transfer medium of separation container 103.When being separated, rotating mechanism 104 will drive magnet 105, and magnet 105 drives magnetic stirring body 110 to stir; Simultaneously, under the effect of the heat transfer medium of the outside of separation container 103, magnetic stirring body 110 is heated also will do tumbling motion, and the rotational motion that tumbling motion drives with magnet 105 combines, and rabbling mechanism will carry out very thoroughly the material in separation container 103 and stir very uniformly.So, the mixing effect of rabbling mechanism is very good, is beneficial to kerogenic separation.
Fig. 3, Fig. 4, Fig. 5 and Fig. 6 show the kerogen maceration equipment that the embodiment of the present invention two provides, comprise casing 101 and cover plate 102, cover plate 102 is flexibly connected with casing 101, separation container 103 and rabbling mechanism is provided with in casing 101, rabbling mechanism comprises rotating mechanism 104, magnet 105 and magnetic stirring body 110, magnetic stirring body 110 is placed in separation container 103, rotating mechanism 104 connects magnet 105 and drives magnet 105 to rotate, magnet 105 drives magnetic stirring body 110 to rotate, separation container 103 is multiple, and rabbling mechanism is also multiple.The rabbling mechanism of multiple separation container 103 and correspondence can carry out kerogenic separation simultaneously, and be separated more, separative efficiency is higher.
But, when being separated kerogen, all can injecting heat transfer medium in casing, and generally all can adopt liquid heat transfer medium, if under rotating mechanism 104 and magnet 105 are in liquid environment for a long time, just easily damage.
In view of the foregoing, the kerogen maceration equipment that researcher provides further comprises the dividing plate 106 being carried out the inner space of casing 101 separating, the side of the close cover plate 102 of dividing plate 106 is the top of dividing plate 106, the side away from cover plate 102 of dividing plate 106 is the below of dividing plate 106, separation container 103 is placed in the top of dividing plate 106, and rotating mechanism and magnet 105 are placed in the below of dividing plate 106.In kerogenic separation process, separation container 103 needs the absorption carrying out heat, and most mode adopted is all utilize liquid heat transfer medium to carry out heat trnasfer to separation container 103.The inner space of casing 101 is separated by dividing plate 106, separation container 103 and rotating mechanism 104, magnet 105 are also because this has been separation, so, under rotating mechanism 104, magnet 105 just avoid and be in liquid environment for a long time, thus also just avoid the larger spoilage of the rotating mechanism 104 brought thus.
In kerogenic separation process, in separation container 103, acid can be added.And when being separated, part acid can evaporate under heating environment, cannot use.Thus, researcher is also provided with the container cover 107 of coupling separation container 103.The setting of container cover 107, can reduce the effusion of pernicious gas; Meanwhile, also because separation container 103 have matched container cover 107, acid can be stopped by container cover 107 by after thermal evaporation, and container cover 107 adsorbs the acid by thermal evaporation, carries out recycling.In addition, container cover 107 and cover plate 102 reach double-deck effect of isolating, and pernicious gas cannot be overflowed, avoid staff to suck pernicious gas.
The air extractor 108 of the gas detached in casing 101 is provided with in casing 101.Air extractor 108 is set in casing 101, the pernicious gas produced can be detached in kerogen maceration process, reduce the release of pernicious gas, ensure the security of separation process.
When utilizing separation container 103 to carry out kerogenic separation, liquid heat transfer medium generally all can be adopted to heat separation container 103.Liquid heat transfer medium at a certain temperature, can roll and hold, and separation container 103 is in the liquid environment of rolling, just may topple over.
In view of the foregoing, the kerogen maceration equipment that researcher provides further comprises the fixed mount 109 of the position of fixedly separated container 103.Owing to being provided with fixed mount 109, separation container 103 is when being heated, and the frame 109 that can be fixed is fixed, and avoids separation container and causes owing to rocking inner separate substance to be toppled over.
Fixed mount 109 and casing 101 are for removably connecting.Fixed mount 109 and casing 101 are arranged to removably connect, so, when needs take out separation container 103, fixed mount 109 can be taken off, but also can heat transfer medium wherein be changed; When needs carry out kerogenic separation, fixed mount 109 is fixed.
In the present embodiment, casing 101 is provided with lug, and fixed mount 109 is provided with recess, when needing to take out fixed mount 109, fixed mount 109 is lifted and can be taken out; And when needing to carry out kerogenic separation, fixed mount 109 is put into casing 101, make recess alignment tab, snap in.
Casing 101 is plastic box, and separation container 103 is plastics separation container.In kerogenic separation process, in separation container 103, acid and alkali can be added.Because casing 101, separation container 103 are arranged respectively to plastic box, plastics separation container, so, for the corrosive gas produced in kerogen maceration process or liquid, plastic box and plastics separation container all can not be corroded.This kind of setting increases the protection to kerogen maceration equipment, extends the service life of kerogen maceration equipment.
In the present embodiment, cover plate 102 and casing 101 can utilize turning cylinder, realize being rotationally connected.Certainly, the mode be rotationally connected, not as the restriction be flexibly connected between cover plate 102 with casing 101, also can adopt herein and removably connect, being slidably connected, as arranged chute at casing 101, slide block is set in cover plate 102 coupling, just can realizes being slidably connected therebetween.
Fig. 3 and Fig. 7 shows the kerogen maceration equipment that the embodiment of the present invention three provides, comprise casing 101, cover plate 102, dividing plate 106, fixed mount 109 and air extractor 108, multiple separation container 103 is provided with in casing 101, mate multiple container cover 107 of multiple separation container 103 and multiple rabbling mechanism, rabbling mechanism comprises rotating mechanism 104, magnet 105 and magnetic stirring body 110, magnetic stirring body 110 is placed in separation container 103, rotating mechanism 104 connects magnet 105 and drives magnet 105 to rotate, magnet 105 drives magnetic stirring body 110 to rotate.During use, be marked with in casing 101 to the water of separation container 103 transferring heat, separation container 103 is placed among water.Utilize water to carry out the transmission of heat to separation container 103, be conveniently easy to get.
Rotating mechanism 104, magnet 105 separate with moisture by dividing plate 106, under avoiding them to be in liquid environment for a long time, thus also just avoid the larger spoilage of the rotating mechanism 104 brought thus.And in heating process, the acid added in separation container 103 can be evaporated, container cover 107 just can stop the evaporation of acid, and finally liquefy, be attached in container cover 107, just can reclaim acid, again utilize, utilization rate is high, also more environmental protection.Simultaneously, the air extractor that casing 101 inside is arranged also is based on environmentally friendly consideration, air extractor is communicated with outside reaction tank, the toxic and harmful produced in kerogen maceration process will be pulled out, and be discharged in outside reaction tank carry out comprehensive, react away pernicious gas, avoid the pollution to environment.Fixed mount 109 can prevent separation container 103 toppling in separation process.And casing 101 and separation container 103 all can be arranged to plastics, can prevent by corrosion such as acidic materials.
Heating tube 111 is provided with in casing 101.The setting of heating tube 111, makes kerogen maceration equipment to heat, then the water in casing 101 is carried out to the transmission of heat, and without the need to heating water by other equipment.This kind is arranged, and makes kerogen maceration equipment more practical.
In embodiments of the invention two and embodiment three, casing is plastic box, and separation container is plastics separation container, and in fact, also cover plate, container cover, fixed mount etc. all can be arranged to plastics, prevent from being corroded.
Between dividing plate of the present invention and casing, also can be set to removably connect, so, when being in the rabbling mechanism below dividing plate and having damage, just cover plate can be opened, and take fixed mount and dividing plate apart, maintenance process is carried out to rabbling mechanism, this kind arranges the later maintenance that more take into account kerogen maceration equipment, arranges comprehensively, considers to put in place.
Kerogen maceration equipment of the present invention can utilize circuit, carries out integrated treatment to whole equipment, whole equipment can be controlled by realizing circuit, inputted, just can control rabbling mechanism, air extractor, heating tube etc. by simple button.
Magnetic for band rabbling mechanism applies on kerogen maceration equipment by the present invention, reaches beyond thought excellent effect, and before this, people are not applied on kerogen maceration equipment, and this kind of utilization is a kind of new breakthrough.
The foregoing is only the preferred embodiments of the present invention, be not limited to the present invention, for a person skilled in the art, the present invention can have various modifications and variations.Within the spirit and principles in the present invention all, any amendment done, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.
Claims (10)
1. a kerogen maceration equipment, is characterized in that: comprise casing and cover plate, and described cover plate is flexibly connected with described casing, is provided with the rabbling mechanism of separation container and corresponding described separation container in described casing,
Described rabbling mechanism comprises rotating mechanism, magnet and magnetic stirring body, described magnetic stirring body is placed in described separation container, described rotating mechanism connects described magnet and drives described magnet to rotate, and described magnet drives described magnetic stirring body to rotate.
2. kerogen maceration equipment according to claim 1, it is characterized in that: described kerogen maceration equipment also comprises the dividing plate being carried out the inner space of described casing separating, the side of the close described cover plate of described dividing plate is the top of described dividing plate, the side away from described cover plate of described dividing plate is the below of described dividing plate, described separation container is placed in the top of described dividing plate, and described rotating mechanism and magnet are placed in the below of described dividing plate.
3. kerogen maceration equipment according to claim 1, is characterized in that: described kerogen maceration equipment also comprises the container cover of mating described separation container.
4. kerogen maceration equipment according to claim 1, is characterized in that: the air extractor being provided with the gas detached in described casing in described casing.
5. kerogen maceration equipment according to claim 1, is characterized in that: described kerogen maceration equipment also comprises the fixed mount of the position of fixing described separation container.
6. kerogen maceration equipment according to claim 5, is characterized in that: described fixed mount and described casing are for removably connecting.
7. kerogen maceration equipment according to claim 1, is characterized in that: described casing is plastic box, and described separation container is plastics separation container.
8. kerogen maceration equipment according to claim 1, is characterized in that: during use, and be marked with in described casing to the heat transfer medium of described separation container transferring heat, described separation container is placed among described heat transfer medium.
9. kerogen maceration equipment according to claim 1, is characterized in that: be provided with heating tube in described casing.
10. the kerogen maceration equipment according to any one of claim 1 ~ 9, is characterized in that: described separation container is multiple, and described rabbling mechanism is multiple.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410633481.XA CN104307415A (en) | 2014-11-11 | 2014-11-11 | Kerogen separation equipment |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410633481.XA CN104307415A (en) | 2014-11-11 | 2014-11-11 | Kerogen separation equipment |
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| CN104307415A true CN104307415A (en) | 2015-01-28 |
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| CN201410633481.XA Pending CN104307415A (en) | 2014-11-11 | 2014-11-11 | Kerogen separation equipment |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110346197A (en) * | 2019-06-11 | 2019-10-18 | 中国地质大学（武汉） | A kind of shale support preparation method adsorbing petroleum liquid hydrocarbon |
| CN110836836A (en) * | 2018-08-17 | 2020-02-25 | 中国石油化工股份有限公司 | Kerogen elastic modulus testing method |
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| CN1042418A (en) * | 1989-11-15 | 1990-05-23 | 西南石油学院 | Automatic preparation instrumnet for root of cheese |
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| CN201519565U (en) * | 2009-07-23 | 2010-07-07 | 天津市欧诺仪器仪表有限公司 | Constant-temperature water-bath four-head magnetic stirrer |
| CN201532328U (en) * | 2009-07-06 | 2010-07-21 | 长沙湘智离心机仪器有限公司 | Intelligent kerogen extractor |
| CN201543405U (en) * | 2009-07-23 | 2010-08-11 | 天津市欧诺仪器仪表有限公司 | Thermostatic waterbath six-head magnetic stirrer |
| CN204208494U (en) * | 2014-11-11 | 2015-03-18 | 四川省科源工程技术测试中心 | A kind of kerogen maceration equipment |
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2014
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1042418A (en) * | 1989-11-15 | 1990-05-23 | 西南石油学院 | Automatic preparation instrumnet for root of cheese |
| CN2592268Y (en) * | 2002-12-25 | 2003-12-17 | 郑成 | Digital-display multi-head magnetic-mixing constant temperature water bath boiler |
| CN201532328U (en) * | 2009-07-06 | 2010-07-21 | 长沙湘智离心机仪器有限公司 | Intelligent kerogen extractor |
| CN201519565U (en) * | 2009-07-23 | 2010-07-07 | 天津市欧诺仪器仪表有限公司 | Constant-temperature water-bath four-head magnetic stirrer |
| CN201543405U (en) * | 2009-07-23 | 2010-08-11 | 天津市欧诺仪器仪表有限公司 | Thermostatic waterbath six-head magnetic stirrer |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110836836A (en) * | 2018-08-17 | 2020-02-25 | 中国石油化工股份有限公司 | Kerogen elastic modulus testing method |
| CN110836836B (en) * | 2018-08-17 | 2022-08-16 | 中国石油化工股份有限公司 | Kerogen elastic modulus testing method |
| CN110346197A (en) * | 2019-06-11 | 2019-10-18 | 中国地质大学（武汉） | A kind of shale support preparation method adsorbing petroleum liquid hydrocarbon |
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Application publication date: 20150128 |