CN104278543A - Dye comprising negative ion particles - Google Patents

Dye comprising negative ion particles Download PDF

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Publication number
CN104278543A
CN104278543A CN201410474643.XA CN201410474643A CN104278543A CN 104278543 A CN104278543 A CN 104278543A CN 201410474643 A CN201410474643 A CN 201410474643A CN 104278543 A CN104278543 A CN 104278543A
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dyestuff
germanium
effect
dye
anionic particle
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CN104278543B (en
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李忠
韩霞
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Shenzhen Xuhangsheng Technology Co ltd
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Abstract

The invention discloses a dye comprising negative ion particles. The negative ion particle material comprises the following components by weight percent: 25-30% of aluminium oxide, 0.2-0.5% of organic germanium powder, 2% of sapphire powder, 25-35% of silicon dioxide, 5-10% of magnesium oxide, 10-15% of boron trioxide, 8-15% of iron trioxide, 0.5-1.5% of sodium oxide, 0.1-0.5% of phosphorus pentoxide, 0.2-0.5% of titanium dioxide, 8% of ferric oxide, 2% of calcium oxide, 2% of periclase and 5% of activated carbon. A fabric prepared from the dye can be used for making female underwear or physical therapy health care clothing; after the fabric prepared from the dye is used for a long time, the incidence of the female breast diseases can be effectively reduced; furthermore, the fabric prepared from the dye has the functions of improving the microcirculation, relieving the pain of soft tissues and improving the organism immunity, and is remarkable in effect.

Description

A kind of dyestuff comprising anionic particle
Technical field
The present invention relates to a kind of dyestuff, particularly relate to a kind of dyestuff for textiles.
Background technology
Germanium belongs to 4B race in the periodic table of elements, is carbon element race element, element mark: Ge, atom sequence number: 32, atomic weight: 72.59, dissolved click: 958 DEG C, fluidizing point: 2700 DEG C, proportion: 5.325 (25 DEG C), organic germanium is a kind of element that human body needs, and it has several functions.Because it has dehydrogenation enriched in oxygen function, the oxygen that physical efficiency keeps sufficient can be made, thus safeguard the health of human body.In human body, the decomposition of food is undertaken by oxygen, in food decomposable process, needs to consume a large amount of oxygen, generates water and carbon dioxide simultaneously.If there is no sufficient oxygen, just likely body is given rise to diseases.And organic germanium can be taken the hydrogen ion in human body out of external, decrease the demand of body to oxygen, thus be conducive to health.
After organic germanium enters human body, can be evenly distributed in each organ-tissue, within 24 hours, excrete completely, belong to the trace element that can not accumulate in the body, its toxicity is extremely low, has no side effect.The each organ cell of human body produces refuse in life process, a part excretes through excretory system, some is present in each organ with the form of free radical, form pathology, organ dysfunction is caused to decline unhealthful, organic germanium can with this part combined with radical after excrete, strengthen organ life.
Clinical research finds, is had good therapeutic action at present by the HAPPY organic germanium that people extensively approve to various diseases.Be mainly reflected in: antitumor, treatment senile dementia, strengthen immunologic function, delay senility, Prevention and Curation artery sclerosis, reduce blood viscosity, resisting rheumatoid disease arthritis, regulate endocrine, analgesic antiphlogistic, hypotensive, treatment osteoporosis, regulate endocrine, aspect such as treatment chronic hepatitis etc.Germanium is also life essential trace element.
Organic germanium has very strong ability of dehydrogenation in human body, can prevent cell ageing, strengthens body immunity.Germanium also has antitumor, anti-inflammatory, the physiological action such as antiviral.According to Japanese scholars, organic germanium is a kind of broad-spectrum anti-cancer drug, and treatment pulmonary metastasis, liver cancer, reproductive system cancer and leukaemia is all effective.According to Sweden and the U.S., organic germanium treatment malignant lymphoma, oophoroma, cervix cancer, colorectal cancer, prostate cancer and black cancer is all effective.Therefore, organic germanium is described as " patron saint of human health ".
Germanium is by a small amount of energy (body temperature) generation effect, but other semiconductor must through a large amount energy (high temperature, electric current, voltage), have 32 electronics around germanium atom core, 4 electronics on outermost track do irregular movement.Once temperature rises, an electronics on outermost track will leave the right or normal track because of irriate.And the electronics having departed from track contributes to adjusting biological ionic equilibrium, make the abnormal restoring of health neuron circuit normal, there is prevention and improve the sense of discomfort of health and massage the effects such as hot spring effect.Germanium also has the function of the abnormal current potential of adjustment human body, and when cancer cell current potential acutely rises, Ge element can capture the electronics of cancer cell, and its current potential is declined, and suppresses the deterioration of illness.The semiconductor function of germanium metal can promote body temperature, thus stimulates circulation, and lessens fatigue; Medicinal health effect of germanium: strengthen natural curability, improve whole body physique, prevent aging, pre-anti-cancer, eliminate tumour, hepatopathy, asthma, blood pressure adjustment, toxin, vegetative dystonie etc. the chronic disease got rid of in body.
Germanium can be anticancer, and germanium is the material having the effect of powerful startup white blood cell, and it can make the super oxygen supply in health increase, and leukocytic susceptibility also improves greatly thereupon.Although cancer cell current potential is close to normal cell, always have a gap with normal cell, because leukocytic identification sensitivity improves, cancer cell just escapes only leukocytic having engulfed.
Germanium is again the interferon that brings out of interferon is can the material of virus replication, and germanium then can bring out human body and produce more interferon, and then opposing virus, and prevents virus diffusion or increase.
Germanium facilitates the tremendous development of electronics industry after having found the semiconductor property of Ge element as doctor Ba Ding of submetallic 1948 AT&T Labies of the U.S. and doctor Xiao Ke.While electronics industry development, the human body that scientist and physician utilize Ge element semiconductor property to carry out playing its effect in life entity corrects the research of medical science scope.
The majesty correcting the research of medical science scope to human body about Ge element is Japanese Korean and Japanese doctor, and he has not only delivered the numerous studies comprising write books " germanium and I " and has reported, and on the body of the research and treatment difficult card patient of having dedicated germanium all one's life to.And have developed organic germanium compounds in 1975 first in the whole world, thus obtain the Nobel Prize.
Research through the research group that northeastern Japan University Hospital portion professor Shi Tian leads confirms, if take life entity immunologic active material-germanium, will produce immune substance interferon in life entity.The process that the cancer cell that research group also successfully have taken the patient taking germanium is destroyed, and play in Japanese national TV station (NHK-TV).
The Sang Dela of Britain in 1998. ancient mambo scholar publishes thesis on medical association's magazine, simple and clear and delivered to draw a conclusion: " germanium has raising immunity, supply oxygen, eliminates pernicious gas, and the therapeutic treatment effects such as heavy metal are understood in analgesia.Show in the research of detoxication, it has and to be absorbed fast by toxin and to get rid of external effect.By clinical medicine experiment and hundreds of secondary individual clinical trial certificate germanium for cancer, hepatitis, arthritis, the various diseases such as bone porous card, particularly for Adult chronic's disease, there is good result for the treatment of, but also confirm that there is antitumaous effect and immune effect, and also there is the fact of certain effect to the treatment of AIDS and prevention, in the middle of testing at present.
The scientist of current countries in the world and physicians also do not untie the Mysterious Veil of Ge element completely, and confirm numerous effect in the clinical trial of more than 140 year in the past, its main contents are as follows:
(1) semiconductor effect (effect of control agent inner cell current direction)
The maximum feature of germanium has dielectric character, exists with submetallic form.This characteristic can improving intracellular current direction of germanium is exactly the factor of disease therapy, so can be referred to as " miracle element ".
(2) dehydrogenation
The hydrogen produced in digestion process is CATION, is completely useless to human body.And this hydrogen ion can make human body become acidification, thus become the reason that various disease grows.Germanium replaces oxygen be combined with hydrogen and generate moisture and get rid of external, thus makes physique become alkalescent and prevent disease prevents aging.
(3) supply oxygen
Human body cell needs repeatedly to carry out metabolism constantly, and now nutrient and oxygen are absolutely necessary.If lack oxygen will cause chronic anthracemia, anaemia, blood vessel blockage, heart disease, low blood pressure, cell senescence, the diseases such as phrenoblabia.
The experiment of physician shows, germanium can to human body supply oxygen, therefore, and can the various human diseases that caused by chronic oxygen deficiency disease of prevention and therapy.
(4) effect of body immunity is strengthened
Human body has two kinds of immune systems substantially, and a kind of is the system utilizing white blood cell to be eliminated by the pathogen in body; Another kind utilizes antibody effect, forms B-lymph corpuscle by T-lymph corpuscle, is then combined with pathogen and kills the system of germ.Therefore catch and just mean the lymphocytic minimizing of T-, and germanium can increase the lymphocytic quantity of T-, and can cancer cell be prevented, toxicant, virus.Thus protection human body is not encroached on.
(5) inducing interferon is formed
Inducing interferon is the protein containing sugar, is one of B.R.M activating substance of immune system (generate) of producing of cell, be nineteen fifty-seven by Britain's gram Sa and Lin De mambo scholar find anticancer, antiviral substance.Interferon is the material of most effect in the middle of the material facing upward only cancer cell breeding that finds up to now.The assistant rattan doctor of Japan points out in clinical trial report, and germanium brings out the generation of interferon in human body; Show that the growing amount of interferon in the injection rate of organic germanium and human body is directly proportional row according to the experiment of autumn leaves professor.
(6) detoxication and the effect of eliminating heavy metal
Germanium has the strong oxygen atom of oxidisability, can adsorb after toxicant also produces chemical reaction with it and generate other innocuous substances, thus play detoxication due to this chemical characteristic.Particularly to mercury, aluminium, the Environmental Hormones such as the heavy metals such as cadmium and two grace English (formal name used at school 2 oxygen) pollute and have obvious detoxication.The people of smoking is easily poisoning in cadmium, so have obvious detoxication for smoker.
(7) pain effect is removed
Certain position of human body if there is pain phenomenon, brain will produce be called as peptase hormone temporarily face upward system its pain, if the drug effect of analgestic goes down, pain can recur.Although germanium does not have the moment effect of analgestic, slowly can present effect, and any side effect will not be produced.
(8) effect of natural curability is strengthened
The mankind and all biologies start just have natural curability from birth, this is because injured or have the instinct role returning to original state when there is exception.Germanium has the effect strengthening natural curability in human body, so have effect for the treatment of to cancer and various difficult disease.
(9) effect of enhancing metabolism
Germanium, to the oxygen of cell tissue supply high-quality, thus excites metabolism, is separated sick cell, promotes diuresis, prevents acidification, prevents aging etc.And entering after in body, harmful substance is got rid of external in 20 ~ 30 hours, so pharmacological action is only had not have poisoning or other side effects completely.
As mentioned above, although Ge element is many useful to human body, the mode mainly through meal supplement enters human body, but the research conclusion of U.S. food Drug Administration is, " is likely detrimental to health when germanium is used as dietary supplements.Temporarily there is no the technical scheme of the open organic germanium external application of document at present.
Summary of the invention
The object of the invention is to overcome the deficiencies in the prior art, provide a kind of dyestuff that can comprise anionic particle, to enable organic germanium external application.
The present invention is achieved by the following technical solutions: a kind of dyestuff comprising anionic particle, and this dyestuff is prepared in accordance with the following methods:
(1) one by one ore dressing is carried out respectively to each component raw material in anionic particle material, after pulverizing grinding, cross 1800 ~ 2200 mesh sieves; Described anionic particle material by weight, comprises following component: alundum (Al2O3) 25% ~ 30%, organic germanium powder 0.2% ~ 0.5%, sapphire powder 2%, silica 25% ~ 35%, magnesia 5% ~ 10%, boron trioxide 10% ~ 15%, di-iron trioxide 8% ~ 15%, sodium oxide molybdena 0.5% ~ 1.5%, phosphorus pentoxide 0.1% ~ 0.5%, titanium dioxide 0.2% ~ 0.5%, iron oxide 8%, calcium oxide 2%, periclase 2%, active carbon 5%;
(2) first add in a component raw material after another component raw material mixes wherein, then add the 3rd component and mix, then add other each component raw material by that analogy successively and obtain final composite material;
(3) after 1500 ~ 2000 DEG C of high-temperature calcinations, be ground to particle diameter after being stirred by the final composite material that step (2) obtains and be less than or equal to 100nm, obtain anionic particle material;
(4) by direct dyes furnishing pulpous state, add soda ash liquid, heat and stir, dissolve to dyestuff, then obtained anionic particle material is added in dyestuff, by weight percentage, dyestuff 85 ~ 90%, anionic particle material 4 ~ 10%, soda ash liquid 2 ~ 3%.
Preferably, described fiber is selected from one or more in cotton, fiber crops, silk and Down Fiber.
Preferably, described direct dyes quality purity 99%.
Operation principle of the present invention is: the anion material in dyestuff has permanent spontaneous electrode, the electrostatic field that it is the two poles of the earth that the surrounding of particles of material exists with C axle axial plane.Under electrostatic field, hydrone generation electrolysis, forms bioactive molecule H3O+, attracts impurity, dirt in water, purifies water; OH-and water molecules form anion, improve the living environment of people; Electric field has suction-operated to charged particle, can adsorption of dust, purifies air.Anion material of the present invention also has high mechanochemistry stability, compared with the suction-operated of zeolite, montmorillonite etc., anion material of the present invention does not have saturation limit, sustainable use, recycling rate of waterused is high, has good development prospect at environmental area.
Composition in anion powder has pyroelectricity and piezoelectricity, therefore when there being temperature and pressure to change, (even if small change) can cause the electrical potential difference between composition crystal, this electrostatic is up to 1,000,000 electron-volts, thus air is ionized, be electronically attached to contiguous water and oxygen molecule and make it be converted into negative aeroion by what hit, be i.e. negative oxygen ion.
At normal temperatures, once faint change occurs for environmental pressure or temperature, namely its interior molecules vibrates enhancing, dipole moment changes, namely warm-up movement makes polar molecule be energized into higher energy level, when its downward transition, just unnecessary energy is pulled away with the form of photon.Therefore, anion material of the present invention outwardly launches the change that ultrared power comes from ambient temperature and pressure, and the essence of this process is the energy exchange processes occurred between anion material of the present invention and environment.
Composition in anion material powder of the present invention take boracic as the aluminium of feature, sodium, iron, the silicate material of lithium circulus, because of its pyroelectricity and piezoelectricity, its polar ion is made to cause dipole moment to change the electromagnetic radiation producing far infrared band in equilbrium position vibration, add to (such as fiber) in product, make it by the free ion of self, impurity ion and ionic substance, impurity and two, three phonon sympathetic responses produce radiation, affect and organicly to vibrate with the ionic bond polarity of inorganic molecule interlinkage, define stronger radiation broadband, anion material powder of the present invention is more than 90% to far emissivity.
The mechanism of the permanent anion releasing of anion material of the present invention is owing to the electrolysis of anion material of the present invention to water: H2O electrolysis is OH-and H+, and hydrogen ion obtains electronics by the weak current between anion material electrode of the present invention; 2H++2e → H2 ↑, hydroxide ion and water molecules form negative aeroion; OH-+nH2O → OH-(H2O) n is according to this theory, and the concentration of anion material anion releasing of the present invention is relevant with its spontaneous polarization effect power, and necessary condition is the moisture in air.
The maximum feature of the monocrystal be combined to form by the various compositions of anion material of the present invention is can the weak current of permanent generation 0.06mA, with the current capacity by human nerve seemingly, impel blood circulation smooth and easy.Have the unexistent advantage of other single raw mineral materials, its characteristic is roughly divided into following five kinds:
(1) anion is produced
Anion is also called to have and regulates the effect of human body ionic equilibrium, body and mind can be made to loosen, activating cell, improves the effects such as nature cure rate, and can suppress the oxidation of health or aging, modern environment has many essential factors impelling cation to generate, health is often in tension, and therefore, anion is the material that modern is indispensable, in addition, anion also has effect of deodorizing.
(2) brine electrolysis
After water electrolysis, the active function at interface, the stabilization of chlorine, the passivation (preventing red iron rust generate and red water occurs) of iron, the reducing of water, various effect such as removal silica and binding (microorganism aggregate) etc. can be obtained.Anion material of the present invention and water react, and just can process fluidization lotion and all very unmanageable problem of chemical substance.
(3) hydrone bundle is reduced
Hydrone (H2O) non-singleton, its molecule can be combined with each other, and forms molecular beam.The water that molecular beam is less can remove chlorine or impurity, and taste is good, and can improve the penetrability of health.
(4) emitting far infrared ray (infrared rays that wavelength is 4 ~ 14 microns)
Far infrared can penetrate into deep somatic position, and warm cell, stimulates circulation, and makes metabolism smooth and easy.Anion material far infrared emissivity of the present invention nearly 100%, numerical value is high compared with other mineral.
(5) containing effective trace mineral
Anion material of the present invention contains various natural mineral matter, wherein has many mineral matters necessary with the mankind identical.By the effect of weak current, mineral matter is easily absorbed, and is splendid mineral origin.
It is the radiant heat warm-heat effect of 93% and biological activity effect of resonance resonant absorption effect generation that germanium has by far infrared emissivity, and germanium is containing in the middle of numerous materials of far infrared, is the material to human body most ideal effect.Germanium ion in cell tissue promotes activation and metabolism, thus by the deposit in body, heavy metal, the materials such as toxin, by sweat, stool and urine, skin is drained external rapidly.Therefore, not only blood is converted to low alkalinity, and the resurrection of cell tissue and the generation of hormone can be promoted.If inorganic Ge and skin contact at normal temperatures, because of the ripple effect of the characteristic of semiconductor generation germanium ion of germanium, will thus promote the flowing of micro-electric current in body.Meanwhile, the irregular abnormal position in body (causing pain and disease) is made rapidly to recover.Germanium has the characteristic of significant ion exchange, and therefore catharsis and centrifugation are very outstanding.Removing effect stench and the facility that purifies water playing brilliance, acid ground can be made to be converted to alkalescence, and can grow by Promoting plant growth.Because of the characteristic of semiconductor of germanium, make to produce adelphotaxy between each different wave length, thus insalubrious water vein waves and electron waves produce cut-out effect.
The clothing of dyeing of the present invention is emitting far-infrared with anion releasing two kinds of function synergic effects, than the activity of simple function more exciting human cell, promote blood circulation of human body and metabolism, be desirable health care material, can be made into the product such as health-care underclothes, healthy bedding.
The clothing of dyeing of the present invention has emitting far-infrared, with the weak current mated with human body and electrostatic, produce the characteristics such as anion, at the pressure of body weight, under the effect of temperature, give full play to the function of its piezo-electric effect and pyroelectric effect and the far infrared effect produced continuously, launch the far infrared mated with human body, produce negative ion effect etc., expansible blood capillary, reduce blood viscosity, speed velocity of blood flow, make platelet disaggregation in blood, red blood cell beading assembles disappearance, neutrophil leucocyte is also impelled to enliven, thus improve microcirculation in body, strengthen metabolism, promote that body function recovers, body microcirculation is improved, thus impel histocyte to activate, immunologic function improves, tissue and bone joint pain etc. can be alleviated, to neurasthenia, osteoarthropathy, cerebral infarctions etc. all have certain adjuvant treatment effect, can be used as a kind of simple and effective physics auxiliary treatment means.
The anion about 80% of the clothing release of dyeing of the present invention can be absorbed by human body skin, the anion concentration in body increase can in and oxygen radical, change acidic constitution, play and delay senility and the effect of dispelling fatigue.Its bioelectrical effect can improve blood circulation and the microcirculation of body, thus strengthens metabolism, adjustment nervous function, reduce blood viscosity, it, with the characteristic of weak current and electrostatic, can change the surface charging such as red blood cell, blood platelet situation, thus plays the effect reducing blood viscosity.Improve cardiac function, enhanced machine vitality of subject, eliminate body and be harmful to and undesirable element, activation histocyte, enhanced machine body immunity function, facilitates the balance of body internal and external environment.
Detailed description of the invention
Elaborate to embodiments of the invention below, the present embodiment is implemented under premised on technical solution of the present invention, give detailed embodiment and concrete operating process, but protection scope of the present invention is not limited to following embodiment.
Embodiment 1
Comprise a dyestuff for anionic particle, this dyestuff is prepared in accordance with the following methods:
(1) one by one ore dressing is carried out respectively to each component raw material in anionic particle material, after pulverizing grinding, cross 1800 mesh sieves; Described anionic particle material by weight, comprises following component: alundum (Al2O3) 30%, organic germanium powder 0.4%, sapphire powder 2%, silica 26%, magnesia 5%, boron trioxide 10%, di-iron trioxide 8%, sodium oxide molybdena 1%, phosphorus pentoxide 0.2%, titanium dioxide 0.4%, iron oxide 8%, calcium oxide 2%, periclase 2%, active carbon 5%;
(2) first add after organic germanium powder mixes in alundum (Al2O3), then add sapphire powder and mix, then add other each component raw material by that analogy successively and obtain final composite material;
(3) after 1500 DEG C of high-temperature calcinations, be ground to particle diameter after being stirred by the final composite material that step (2) obtains and be less than or equal to 100nm, obtain anionic particle material;
(4) by direct dyes furnishing pulpous state, add soda ash liquid, heat and stir, dissolve to dyestuff, then obtained anionic particle material is added in dyestuff, by weight percentage, dyestuff 90%, anionic particle material 7%, soda ash liquid 2%.
Fabric can be put into dyestuff to dye, by weight, add salt 1%, control temperature is 40 ~ 80 DEG C, and bath raio is 1:15, and the time is 10 ~ 20 minutes; Then, after being dyeed by fabric, technique obtains the fabric containing anion routinely.
Technique routinely, can be processed as health-care physiotherapeutic clothing, as underwear etc. by obtained fabric.
The fabric silk fiber fabric of the present embodiment.Direct dyes quality purity 99%.
Embodiment 2
Comprise a dyestuff for anionic particle, this dyestuff is prepared in accordance with the following methods:
(1) one by one ore dressing is carried out respectively to each component raw material in anionic particle material, after pulverizing grinding, cross 1800 mesh sieves; Described anionic particle material by weight, comprises following component: alundum (Al2O3) 30%, organic germanium powder 0.4%, sapphire powder 2%, silica 26%, magnesia 5%, boron trioxide 10%, di-iron trioxide 8%, sodium oxide molybdena 1%, phosphorus pentoxide 0.2%, titanium dioxide 0.4%, iron oxide 8%, calcium oxide 2%, periclase 2%, active carbon 5%;
(2) first add after organic germanium powder mixes in alundum (Al2O3), then add sapphire powder and mix, then add other each component raw material by that analogy successively and obtain final composite material;
(3) after 1850 DEG C of high-temperature calcinations, be ground to particle diameter after being stirred by the final composite material that step (2) obtains and be less than or equal to 100nm, obtain anionic particle material;
(4) by direct dyes furnishing pulpous state, add soda ash liquid, heat and stir, dissolve to dyestuff, then obtained anionic particle material is added in dyestuff, by weight percentage, dyestuff 85%, anionic particle material 10%, soda ash liquid 3%.
Fabric can be put into dyestuff to dye, by weight, add salt 2%, control temperature is 40 ~ 80 DEG C, and bath raio is 1:30, and the time is 10 ~ 20 minutes; Then, after being dyeed by fabric, technique obtains the fabric containing anion routinely.
Technique routinely, can be processed as health-care physiotherapeutic clothing, as underwear etc. by obtained fabric.
Described fabric is one or more in cotton, fiber crops, silk or Down Fiber.Direct dyes quality purity 99%.
The clothing obtained to embodiment 1 ~ 2 dyestuff, measures its negative ion concentration as table 1.
Table 1 negative ion concentration measured value
? Negative ion concentration (individual/cm 3)
Embodiment 1 16028
Embodiment 2 15026
As shown in table 2 ~ 7, the obtained women underwear of embodiment 1 ~ 2 or health-care physiotherapeutic clothing, for the patient of mammary gland disease and diabetic and normal person, wear every day 8 hours, use the half a year above time, soft tissue pain remission rate is 100%, cold limbs, not good enough and weak improvement of sleeping all reaches more than 90%, numbness in hands and feet and the smelly improvement rate of pin reach more than 80%, effectively can alleviate the pain symptom of female mammary gland disease, simultaneously, for improving microcirculation, alleviate soft tissue pain, eliminate body to be harmful to and undesirable element, activation histocyte, enhanced machine body immunity function, there is significant effect.It, with the characteristic of weak current and electrostatic, can change the surface charging such as red blood cell, blood platelet situation, thus plays the effect reducing blood viscosity.
Body cardinal symptom improvement rate (%) after the fabric that table 2 uses embodiment 1 to prepare
Cardinal symptom Number of cases First month Second month Six month
Headache is dizzy 30 57.4 72.8 82.9
Cold limbs 10 83.5 93.4 93.4
Neck ache 15 52.4 56.4 57.1
Sleep bad 30 86.5 92.3 93.6
Have a pain in the back 10 44.2 46.1 52.9
Tiredness 20 88.1 87.6 96.6
Nervous uncomfortable in chest 16 26.7 25.9 32.8
Arthralgia 20 61.8 64.0 68.1
Numb in every limb 15 81.9 83.9 93.4
Pin is smelly 10 71.2 77.6 88.5
Body cardinal symptom improvement rate (%) after the fabric that table 3 uses embodiment 2 to prepare
Cardinal symptom Number of cases First month Second month Six month
Headache is dizzy 30 60.1 74.1 82.7
Cold limbs 10 79.9 85.9 95.9
Neck ache 15 52.5 51.2 55.5
Sleep bad 30 83.6 89.5 93.8
Have a pain in the back 10 39.2 46.9 53.4
Tiredness 20 87.3 87.6 96.7
Nervous uncomfortable in chest 16 24.3 29.1 32.1
Arthralgia 20 59.6 63.9 64.8
Numb in every limb 15 82.3 81.9 92.6
Pin is smelly 10 71.9 79.6 90.3
The change of the blood pressure and blood lipoid before and after the fabric that table 4 uses embodiment 1 to prepare
The change of the blood pressure and blood lipoid before and after the fabric that table 5 uses embodiment 2 to prepare
The fabric that table 6 uses embodiment 1 to prepare is on the impact of the autonomic nervous function of diabete peripheral herve pathology
Note: with enter group before compare, *p < 0.05; Compare between group, p < 0.05.
The fabric that table 7 uses embodiment 2 to prepare is on the impact of the autonomic nervous function of diabete peripheral herve pathology
Note: with enter group before compare, *p < 0.05; Compare between group, p < 0.05.

Claims (3)

1. comprise a dyestuff for anionic particle, it is characterized in that: this dyestuff is prepared in accordance with the following methods:
(1) one by one ore dressing is carried out respectively to each component raw material in anionic particle material, after pulverizing grinding, cross 1800 ~ 2200 mesh sieves; Described anionic particle material by weight, comprises following component: alundum (Al2O3) 25% ~ 30%, organic germanium powder 0.2% ~ 0.5%, sapphire powder 2%, silica 25% ~ 35%, magnesia 5% ~ 10%, boron trioxide 10% ~ 15%, di-iron trioxide 8% ~ 15%, sodium oxide molybdena 0.5% ~ 1.5%, phosphorus pentoxide 0.1% ~ 0.5%, titanium dioxide 0.2% ~ 0.5%, iron oxide 8%, calcium oxide 2%, periclase 2%, active carbon 5%;
(2) first add in a component raw material after another component raw material mixes wherein, then add the 3rd component and mix, then add other each component raw material by that analogy successively and obtain final composite material;
(3) after 1500 ~ 2000 DEG C of high-temperature calcinations, be ground to particle diameter after being stirred by the final composite material that step (2) obtains and be less than or equal to 100nm, obtain anionic particle material;
(4) by direct dyes furnishing pulpous state, add soda ash liquid, heat and stir, dissolve to dyestuff, then obtained anionic particle material is added in dyestuff, by weight percentage, dyestuff 85 ~ 90%, anionic particle material 4 ~ 10%, soda ash liquid 2 ~ 3%.
2. dyestuff as claimed in claim 1, is characterized in that: described fiber be selected from cotton, fiber crops, silk and Down Fiber one or more.
3. dyestuff according to claim 1, is characterized in that: described direct dyes quality purity 99%.
CN201410474643.XA 2014-09-17 2014-09-17 A kind of dyestuff including anionic particle Expired - Fee Related CN104278543B (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105862470A (en) * 2016-05-27 2016-08-17 无锡润新染料有限公司 Inorganic compound dye and preparation method thereof
CN107119467A (en) * 2017-06-13 2017-09-01 安徽宜民服饰有限公司 A kind of environmentally friendly dyeing and printing process of dress ornament
CN107237178A (en) * 2017-06-13 2017-10-10 安徽宜民服饰有限公司 A kind of environmentally friendly coloring agent for clothes

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