CN104275138A - Microwave heating type glass reaction kettle - Google Patents
Microwave heating type glass reaction kettle Download PDFInfo
- Publication number
- CN104275138A CN104275138A CN201310272405.6A CN201310272405A CN104275138A CN 104275138 A CN104275138 A CN 104275138A CN 201310272405 A CN201310272405 A CN 201310272405A CN 104275138 A CN104275138 A CN 104275138A
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- CN
- China
- Prior art keywords
- rotating shaft
- glass reaction
- microwave
- reaction still
- glass
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00139—Controlling the temperature using electromagnetic heating
- B01J2219/00141—Microwaves
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Constitution Of High-Frequency Heating (AREA)
Abstract
The invention relates to a microwave heating type glass reaction kettle which is provided with a glass reaction kettle body and a glass cover body, wherein a center connector and a plurality of functional connectors are arranged on the glass cover body; a stirring rotating shaft is arranged in the center connector of the glass cover body; the glass reaction kettle body and the glass cover body are arranged in a microwave generating cavity; the top surface of the microwave generating cavity is provided with a rotating shaft through pipe and functional connector through pipes respectively corresponding to the positions of the stirring rotating shaft and the functional connectors on the glass cover body; external screw threads are arranged on the outer sides of the rotating shaft through pipe and the functional connector through pipes, and the rotating shaft through pipe and the functional connector through pipes are respectively connected with a rotating shaft wave sealing cover and functional connector wave sealing covers; a rotating shaft through hole which the stirring rotating shaft penetrates out of and rotates in is formed in the middle part of the rotating shaft wave sealing cover. According to the microwave heating type glass reaction kettle, by arranging a special wave sealing mechanism, microwave leakage can be prevented, an operator is prevented from being radiated by microwaves, and thus the personal safety of the operator is ensured.
Description
Technical field:
The present invention relates to reactor equipment technical field, refer in particular to a kind of microwave heated glass reaction still.
Background technology:
Traditional glass reaction still heating normally adopts the mode of conduction oil, need glass reaction still to be designed to double-layer partition formula for this reason, conduction oil is passed in the interval of interlayer, the glass reaction still manufacture craft relative complex of this frame mode, cost is higher, and the heating of its mode of heating is slow and uneven, and material outer in reactor is first heated and the material at the center of leaning on is heated slowly, therefore easily cause the uneven of material reaction, make end product and ideal occur error; In addition, adopt this kind of mode of heating, easily produce and add thermal inertia, namely when temperature of charge rises to design temperature, thermal source cannot be withdrawn in time, causes temperature of charge can continue to be increased beyond design temperature, has a negative impact equally to end product.
On the other hand, microwave heating is existing ripe application in other technologies field, but in glass reaction still, due to glass reaction still special construction and need to stir when using, vacuumize, add the various operation such as material, measurement, the problem of microwave leakage cannot be solved, cause the application of heating using microwave on glass reaction still cannot realize always.
Summary of the invention:
The object of the invention is to overcome the deficiencies in the prior art part, a kind of microwave heated glass reaction still is provided.
The technical scheme that the present invention realizes the employing of its object is: a kind of microwave heated glass reaction still, it has glass reaction still body and a cover glass, cover glass is provided with hub-interface and several functional interface, and in the hub-interface of cover glass, stirring shaft is installed, wherein, described glass reaction still body and cover glass are arranged in a microwave generation cavity, the end face of this microwave generation cavity is respectively equipped with the rotating shaft siphunculus corresponding with stirring shaft in described cover glass and each functional interface position and functional interface siphunculus, be equipped with external screw thread outside described rotating shaft siphunculus and functional interface siphunculus and be connected with rotating shaft envelope ripple lid and functional interface envelope ripple lid, wherein, offer just for the rotating shaft through hole that stirring shaft passes and rotates in the middle part of described rotating shaft envelope ripple lid.
Described rotating shaft through hole is stepped, and accordingly, described stirring shaft is also stepped through rotating shaft through hole.
Be provided with adjustable support seat in described microwave generation cavity, described glass reaction still body is placed on this adjustable support seat.
Whole glass reaction still is placed in microwave generation cavity by the present invention, utilize microwave to the heating material in glass reaction still, principle due to heating using microwave is different from common electric heating or heat-conducting oil heating, not only make material be rapidly heated, and in reactor everywhere material be heated evenly, also do not add thermal inertia, after cutting off the electricity supply, heating using microwave stops immediately, do not have energy to continue to heat up for it, therefore accurately can be warmed up to design temperature, thus make end product reach ideal effect.And the present invention also arranges distinctive Feng Bo mechanism in conjunction with actual, can prevent microwave leakage, avoid operating personnel to be subject to microwave, thus ensure the personal safety of operating personnel; Meanwhile, Feng Bo mechanism also can not affect feeding intake, bleed or ventilating and measuring the operation such as air pressure, temperature glass reaction still, not only safe but also practical.
Accompanying drawing illustrates:
Fig. 1 is structural plan of the present invention schematic diagram;
Fig. 2 is partial schematic diagram of the present invention.
Detailed description of the invention:
Below in conjunction with specific embodiments and the drawings, the present invention is further described.
As shown in Fig. 1 ~ Fig. 2, the microwave heated glass reaction still of one of the present invention, it has glass reaction still body 1 and a cover glass 2, cover glass 2 is provided with hub-interface 21 and several functional interface 22, such as dog-house, bleeding point and measurement mouth etc., can plug seal be added as required or open and use, and in the hub-interface 21 of cover glass 2, stirring shaft 3 is installed, stirring shaft 3 and hub-interface 21 place in cover glass 2 are that airproof rotates and installs, namely reactor inside can be kept while stirring shaft 3 rotates to not exchange information with outside, this airproof rotates installation and belongs to prior art, therefore repeat no more.Improvements of the present invention are: described glass reaction still body 1 and cover glass 2 are arranged in a microwave generation cavity 4, the end face 40 of this microwave generation cavity 4 is respectively equipped with the rotating shaft siphunculus 41 corresponding with stirring shaft 3 in described cover glass 2 and each functional interface 22 position and functional interface siphunculus 42, be equipped with external screw thread outside described rotating shaft siphunculus 41 and functional interface siphunculus 42 and be connected with rotating shaft envelope ripple lid 51 and functional interface envelope ripple lid 52, wherein, offer just for the rotating shaft through hole 510 that stirring shaft 3 passes and rotates in the middle part of described rotating shaft envelope ripple lid 51.In the present invention, microwave generation cavity 4, its end face 40 and rotating shaft siphunculus 41 and functional interface siphunculus 42, rotating shaft envelope ripple lid 51 and functional interface envelope ripple lid 52 all adopt metal material to make, effectively to prevent microwave leakage.The periphery of microwave generation cavity 4 installs several microwave generator () as required in figure slightly, each microwave generator can independently control, how much to determine according to material in glass reaction still all to open or part unlatching, to guarantee that the inner even microwave distribution of glass reaction still body 1 is advisable.
Preferably, described rotating shaft through hole 510 is stepped, and accordingly, described stirring shaft 3 is also stepped through rotating shaft through hole 510 place.Stepped portion potential energy on stair-stepping rotating shaft through hole 510 and corresponding stirring shaft 3 prevents microwave leakage better, also can not affect the rotation of stirring shaft 3 simultaneously.
Adjustable support seat 43 is provided with in described microwave generation cavity 4, described glass reaction still body 1 is placed on this adjustable support seat 43, namely the position of glass reaction still body 1 in microwave generation cavity 4, height can regulate as required, thus make a microwave generation cavity 4 can be applicable to the use of not isometric glass reaction still body, meanwhile, adjustable supporting seat 43 is also conducive to assembling and the location of glass reaction still body.
Whole glass reaction still is placed in microwave generation cavity by the present invention, utilize microwave to the heating material in glass reaction still, principle due to heating using microwave is different from common electric heating or heat-conducting oil heating, not only make material be rapidly heated, and in reactor everywhere material be heated evenly, also do not add thermal inertia, after cutting off the electricity supply, heating using microwave stops immediately, do not have energy to continue to heat up for it, therefore accurately can be warmed up to design temperature, thus make end product reach ideal effect.And the present invention also arranges distinctive Feng Bo mechanism in conjunction with actual, can prevent microwave leakage, avoid operating personnel to be subject to microwave, thus ensure the personal safety of operating personnel; Meanwhile, Feng Bo mechanism also can not affect feeding intake, bleed or ventilating and measuring the operation such as air pressure, temperature glass reaction still, not only safe but also practical.
Claims (3)
1. a microwave heated glass reaction still, it has a glass reaction still body (1) and cover glass (2), cover glass (2) is provided with hub-interface (21) and several functional interface (22), and in the hub-interface (21) of cover glass (2), stirring shaft (3) is installed, it is characterized in that: described glass reaction still body (1) and cover glass (2) are arranged in a microwave generation cavity (4), the end face (40) of this microwave generation cavity (4) is respectively equipped with the rotating shaft siphunculus (41) corresponding with stirring shaft (3) in described cover glass (2) and each functional interface (22) position and functional interface siphunculus (42), be equipped with external screw thread outside described rotating shaft siphunculus (41) and functional interface siphunculus (42) and be connected with rotating shaft envelope ripple lid (51) and functional interface seals ripple lid (52), wherein, described rotating shaft envelope ripple lid (51) middle part offers just for the rotating shaft through hole (510) that stirring shaft (3) passes and rotates.
2. microwave heated glass reaction still according to claim 1, is characterized in that: described rotating shaft through hole (510) is stepped, and accordingly, described stirring shaft (3) is also stepped through rotating shaft through hole (510) place.
3. microwave heated glass reaction still according to claim 1, is characterized in that: be provided with adjustable support seat (43) in described microwave generation cavity (4), and described glass reaction still body (1) is placed on this adjustable support seat (43).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310272405.6A CN104275138A (en) | 2013-07-01 | 2013-07-01 | Microwave heating type glass reaction kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310272405.6A CN104275138A (en) | 2013-07-01 | 2013-07-01 | Microwave heating type glass reaction kettle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104275138A true CN104275138A (en) | 2015-01-14 |
Family
ID=52250770
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310272405.6A Pending CN104275138A (en) | 2013-07-01 | 2013-07-01 | Microwave heating type glass reaction kettle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104275138A (en) |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1698946A (en) * | 2005-04-18 | 2005-11-23 | 江南大学 | Microwave assisted non-aqueous phase enzyme catalytic reacting device |
| CN203400712U (en) * | 2013-07-01 | 2014-01-22 | 东莞市华青节能科技有限公司 | Microwave heating type glass reactor kettle |
-
2013
- 2013-07-01 CN CN201310272405.6A patent/CN104275138A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1698946A (en) * | 2005-04-18 | 2005-11-23 | 江南大学 | Microwave assisted non-aqueous phase enzyme catalytic reacting device |
| CN203400712U (en) * | 2013-07-01 | 2014-01-22 | 东莞市华青节能科技有限公司 | Microwave heating type glass reactor kettle |
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Legal Events
| Date | Code | Title | Description |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20150114 |
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| RJ01 | Rejection of invention patent application after publication |