CN104209185B - Magnetic material catalyst separating device and system - Google Patents
Magnetic material catalyst separating device and system Download PDFInfo
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- CN104209185B CN104209185B CN201410420799.XA CN201410420799A CN104209185B CN 104209185 B CN104209185 B CN 104209185B CN 201410420799 A CN201410420799 A CN 201410420799A CN 104209185 B CN104209185 B CN 104209185B
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- magnetisable material
- material catalyst
- rod sleeve
- magnetisable
- bar magnet
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- 239000003054 catalyst Substances 0.000 title claims abstract description 157
- 239000000696 magnetic material Substances 0.000 title claims abstract description 18
- 239000000463 material Substances 0.000 claims description 241
- 238000000926 separation method Methods 0.000 claims description 58
- 238000005204 segregation Methods 0.000 claims description 44
- 239000011159 matrix material Substances 0.000 claims description 17
- 239000011797 cavity material Substances 0.000 claims description 11
- 239000003795 chemical substances by application Substances 0.000 claims description 10
- 239000012530 fluid Substances 0.000 claims description 6
- 230000003044 adaptive effect Effects 0.000 claims description 5
- 238000000034 method Methods 0.000 abstract description 16
- 230000000694 effects Effects 0.000 abstract description 12
- 238000004519 manufacturing process Methods 0.000 abstract description 11
- 238000004062 sedimentation Methods 0.000 abstract description 8
- 238000001914 filtration Methods 0.000 abstract description 6
- 239000000126 substance Substances 0.000 abstract description 6
- 239000002245 particle Substances 0.000 abstract description 3
- 239000011344 liquid material Substances 0.000 abstract description 2
- 238000004064 recycling Methods 0.000 abstract description 2
- 238000001179 sorption measurement Methods 0.000 abstract description 2
- 238000003889 chemical engineering Methods 0.000 abstract 2
- 238000003754 machining Methods 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
- 239000000047 product Substances 0.000 description 6
- 241000196324 Embryophyta Species 0.000 description 5
- 238000005516 engineering process Methods 0.000 description 3
- 239000008187 granular material Substances 0.000 description 3
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- 229910000564 Raney nickel Inorganic materials 0.000 description 2
- 238000009903 catalytic hydrogenation reaction Methods 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 230000003203 everyday effect Effects 0.000 description 2
- 239000004744 fabric Substances 0.000 description 2
- 238000005984 hydrogenation reaction Methods 0.000 description 2
- 230000008676 import Effects 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 239000000725 suspension Substances 0.000 description 2
- 241000208340 Araliaceae Species 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 1
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 description 1
- 235000003140 Panax quinquefolius Nutrition 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- NPXOKRUENSOPAO-UHFFFAOYSA-N Raney nickel Chemical compound [Al].[Ni] NPXOKRUENSOPAO-UHFFFAOYSA-N 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 238000012824 chemical production Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 238000006298 dechlorination reaction Methods 0.000 description 1
- 230000001934 delay Effects 0.000 description 1
- 208000002925 dental caries Diseases 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 235000008434 ginseng Nutrition 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
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- Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The invention relates to the technical field of chemical engineering production equipment, in particular to a magnetic material catalyst separating device and system. On the basis of the magnetic adsorption principle, the aim of clearing away magnetic material catalysts mixed in chemical liquid materials can be achieved. According to the device and system, the machining process of chemical engineering products required to use the magnetic material catalysts is improved, the sedimentation time of a sedimentation process is shortened, in the filtering process, a user does not need to filter out the magnetic material catalysts again, work burdens of filtering equipment are reduced, and the production efficiency is improved. When a magnetic rod sleeve pipe array absorbs the magnetic material catalysts in a full-load mode, the aim of separating the magnetic material catalysts can be achieved by taking out the magnetic rod sleeve pipe array from a magnetic material catalyst separating cavity can be achieved. The aim of secondarily recycling magnetic material catalyst particles can be achieved by taking out a permanent magnet magnetic stick or performing power-failure treatment on an electromagnet can be achieved. The better separating effect can be achieved by enabling a plurality of magnetic material catalyst separating devices to be connected in series for use.
Description
Technical field
The present invention relates to technical field of chemical production equipment, be specially a kind of magnetisable material catalyst
Segregation apparatus and system.
Background technology
Chemical Manufacture industry of the prior art can use multiple magnetisable material catalyst, in magnetic
Material catalyst actually used during for reaching preferably catalytic effect, generally use magnetic
Property material catalyst pulverize after use.If the magnetisable material catalyst after pulverizing is in use
Running into the effect of the external force such as mechanical friction, granularity can further be refined, and even refines
It is suspended in solution to graininess, after the magnetisable material catalyst granules that these are refined is
Removing catalyst operation in continuous production technology brings technical barrier, it is impossible to being refined of separation
Magnetisable material catalyst granules can enter next technological process with solution, affect product quality,
Even damage final processed finished products.The magnetisable material catalyst that granularity is the least, clears up difficulty
More for complexity, the cleaning equipment of additional adds production therefore and on production line
Cost, reduces production efficiency.
It is to utilize that the cleaning generally used in prior art separates the method for magnetisable material catalyst
Subsider settles, and concrete structure example is as shown in Figure 1.Deep-cone settling groove shown in Fig. 1
Structure includes: material inlet 1, air vent 2, overfall 3, material feeding cone 4, pop valve 5, discharge dress
Put 6 and manhole 7.If after sedimentation operation, still suffer from the magnetisable material catalyst of small particle size,
Usual then filter plant as shown in Figure 2 need to be added after precipitation apparatus.Filtration shown in Fig. 2
The structure of equipment includes: water inlet 8, strainer cover 9, cushion chamber 10, filter element 11, filter
Cylinder 12, filter mounting 13 and outlet 14.Due to subsider effect of settling with sedimentation time
Between be directly proportional, by ensureing that this technique of being used of end product quality of chemical products greatly reduces
The production efficiency of chemical products；In order to ensure the end product quality of chemical products, if continuing in sedimentation
Filter plant is added after equipment, in addition to extra increase produces hardware input cost, filter plant
In the replacing of consumable goods filter element again increase the input of production cost.
Summary of the invention
(1) to solve the technical problem that
(1) magnetic suck principle is utilized to provide a kind of magnetisable material catalyst separation device, by magnetic
Material catalyst is adsorbed in the outer surface of bar magnet assembly, reaches to remove in chemistry liquid material and mixes
The purpose of magnetisable material catalyst.
(2) simplify magnetisable material catalyst separating technology of the prior art, reduce production cost,
Improve production efficiency.
(2) technical scheme
In order to solve above-mentioned technical problem, the invention provides a kind of magnetisable material catalyst and separate
Device, it is characterised in that described magnetisable material catalyst separation device includes: segregation apparatus base
Body and bar magnet assembly；
Described segregation apparatus matrix includes: material overfall, magnetisable material catalyst disengagement chamber,
Material inlet and be used for opening and close described segregation apparatus matrix and realize picking and placeing described bar magnet assembly
Segregation apparatus cover plate；Described magnetisable material catalyst disengagement chamber is multiple identical parallel to each other
Pipe-like cavity formed multi-pipeline array；The cavity of described magnetisable material catalyst disengagement chamber
Material is non-magnet_conductible material；Described material inlet and material overfall are catalyzed with described magnetisable material
Agent disengagement chamber connects；
Described bar magnet assembly includes: magnetic rod sleeve Guan Zhen and bar magnet；Described magnetic rod sleeve Guan Zhen is
The many cannula array being made up of the multiple identical magnetic rod sleeve shelved parallel to each other, each described
Magnetic rod sleeve accommodates a bar magnet；Described magnetic rod sleeve Guan Zhen is made up of non-magnet_conductible material；Described
The sleeve pipe caliber of magnetic rod sleeve Guan Zhen is adaptive with the outside dimension of described bar magnet；Described magnetic rod sleeve
Guan Zhen is anchored on magnetisable material catalyst disengagement chamber by clamp device；Described magnetic rod sleeve Guan Zhen
The axis of any one magnetic rod sleeve is corresponding to described magnetisable material catalyst disengagement chamber to be inserted
The axis of the pipeline entered coincides.
Preferably, it is additionally provided with between described material inlet and magnetisable material catalyst disengagement chamber
Material buffer chamber；Described material buffer chamber connects with described material inlet；Described material buffer chamber
It is connected with described magnetisable material catalyst disengagement chamber.
Preferably, described material inlet is positioned at the bottom in described material buffer chamber；Described material delays
Rush chamber and be positioned at the bottom of described magnetisable material catalyst disengagement chamber；Described segregation apparatus cover plate is positioned at
The top of described magnetisable material catalyst disengagement chamber；Described material overfall is positioned at described separation and fills
Put the upper end of base side walls, concordant with the lower surface of described segregation apparatus cover plate.
Preferably, described magnetisable material catalyst separation device also includes: fluid attemperating unit；
Described fluid attemperating unit is wrapped in the chamber outer wall of described magnetisable material catalyst disengagement chamber；Institute
State fluid attemperating unit to include: temperature control medium A interface, temperature control medium chuck layer and temperature control medium
B interface；Described temperature control medium chuck layer is the cavity taking up temperature control medium；Described temperature control medium A
Interface is positioned at the bottom of described temperature control medium chuck layer side；Described temperature control medium B interface is positioned at
The top of described temperature medium chuck layer side.
Preferably, described bar magnet diameter 25mm；The sleeve pipe caliber 27 of described magnetic rod sleeve Guan Zhen
mm；Pipe thickness 0.5mm of the magnetic rod sleeve of described magnetic rod sleeve Guan Zhen；Described magnetisable material
The caliber of the single pipeline of catalyst disengagement chamber is 76mm.
Preferably, described bar magnet is the bar magnet of 15000gs；Described magnetisable material catalyst separates
The caliber of the single pipeline in chamber is less than 60mm with the difference of the external diameter of described bar magnet.
Preferably, described material inlet is provided with flow speed control valve and drains valve.
Preferably, described non-magnet_conductible material is PP.
Preferably, described bar magnet is permanent magnet or electric magnet.
In order to solve above-mentioned technical problem, the invention provides a kind of magnetisable material catalyst and separate
System, it is characterised in that described multistage magnetisable material catalyst separation system is urged by magnetisable material
Agent separation apparatuses in series forms；Adjacent two magnetisable material catalyst separation devices, are positioned at
The material overfall of the magnetisable material catalyst separation device of level is urged with the magnetisable material being positioned at subordinate
The material inlet of agent segregation apparatus is connected.
(3) beneficial effect
A kind of magnetisable material catalyst separation device of the present invention simplifies in prior art and needs
Use the processing technique of the chemical products of magnetisable material catalyst, shorten sedimentation process institute necessary
Sedimentation time, improve production efficiency；
A kind of magnetisable material catalyst separation device of the present invention, need not in filtering technique
Filter magnetisable material catalyst again, alleviate the homework burden of filtering technique, it is not necessary to the most more
Change filter element, and then reduce the use cost of filter plant, extend the use longevity of filter plant
Life.
Bar magnet assembly of the present invention adsorbs magnetisable material at full capacity in magnetic rod sleeve Guan Zhen urges
By reaching separation after taking out magnetic rod sleeve Guan Zhen from magnetisable material catalyst disengagement chamber during agent
The purpose of magnetisable material catalyst；Again by taking out permanent magnet bar magnet or to electric magnet power down process
Just can realize carrying out secondary to by magnetic-adsorption effect isolated magnetisable material catalyst granules
Recycling, lock out operation is simple, and separating effect is reliable.
The present invention is provided with material buffer between material inlet and magnetisable material catalyst disengagement chamber
Chamber, significantly slow down material and enters the flow velocity of magnetisable material catalyst disengagement chamber；The most also reach
Make the dispersed technique effect opened of material, make material separate uniformly through magnetisable material catalyst
Each disengagement chamber in chamber, and then make material obtain fully with the set tube wall of magnetic rod sleeve Guan Zhen
Contact, contribute to the optimum efficiency reaching to utilize magnetic field separation magnetisable material catalyst.
The present invention is provided with fluid temperature control dress at the chamber outer wall of magnetisable material catalyst disengagement chamber
Put, expand the range of application of magnetisable material catalyst separation device.
One magnetisable material catalyst separation system of the present invention uses multiple magnetisable material catalyst
Separation apparatuses in series uses, and can reach more preferably magnetisable material catalyst separating effect.
Accompanying drawing explanation
In order to be illustrated more clearly that the embodiment of the present invention or technical scheme of the prior art, below
The accompanying drawing used required in embodiment or description of the prior art will be briefly described, aobvious and
Easily insight, the accompanying drawing in describing below is only some embodiments of the present invention, for this area
From the point of view of those of ordinary skill, on the premise of not paying creative work, it is also possible to according to these
Accompanying drawing obtains other accompanying drawing.
Fig. 1 is deep-cone settling groove structural representation in prior art；
Fig. 2 is water filter structural representation in prior art；
Fig. 3 is according to magnetic in one magnetisable material catalyst separation device embodiment one of the present invention
Material catalyst segregation apparatus structural representation.
Fig. 4 is according to bar magnet in one magnetisable material catalyst separation device embodiment one of the present invention
Horizontal magnetisable material catalyst separation device structural representation.
Fig. 5 is according to material in one magnetisable material catalyst separation device embodiment one of the present invention
Import and the magnetisable material catalyst separation device structural representation of material overfall side arrangement.
Fig. 6 is according to inclusion in one magnetisable material catalyst separation device embodiment two of the present invention
The magnetisable material catalyst separation device structural representation of material cushion chamber device.
Fig. 7 is according to containing stream in one magnetisable material catalyst separation device embodiment three of the present invention
The segregation apparatus structural representation of body attemperating unit；
Fig. 8 is according to bar magnet in one magnetisable material catalyst separation device embodiment three of the present invention
Sleeve pipe pipe battle array structural representation；
Fig. 9 is according to cylinder in one magnetisable material catalyst separation device embodiment three of the present invention
Shape bar magnet schematic diagram；
Figure 10 is according to bar magnet in one magnetisable material catalyst separation device embodiment three of the present invention
Insert magnetic rod sleeve pipe battle array effect schematic diagram；
Figure 11 is according to magnetic in one magnetisable material catalyst separation device embodiment three of the present invention
Material catalyst disengagement chamber cross-sectional plan view；
Figure 12 is one magnetisable material catalyst separation device embodiment four catalytic hydrogenation work of the present invention
Skill separates the process chart of Raney's nickel catalyst.
In figure: 1, material inlet；2, air vent；3, overfall；4, material feeding cone；5, urgent
Valve；6, discharge device；7, manhole；8, water inlet；9, strainer cover；10, cushion chamber；
11, filter element；12, filter cylinder；13, filter mounting；14, outlet；15, thing
Material overfall；16, temperature control medium A interface；17, temperature control medium chuck layer；18, material buffer
Chamber；19, temperature control medium B interface；20, magnetisable material catalyst disengagement chamber；21, material inlet；
22, magnetic rod sleeve Guan Zhen；23, bar magnet；24, segregation apparatus cover plate.
Detailed description of the invention
Below in conjunction with Figure of description and embodiment, the detailed description of the invention of the present invention is made into one
Step describes in detail.Following example are merely to illustrate the present invention, but can not be used for limiting the present invention
Scope.
Embodiment one:
Shown in Fig. 3～Fig. 5, one magnetisable material catalyst separation device of the present invention, it is positioned at separation
The magnetisable material catalyst disengagement chamber 20 of device intrinsic silicon and bar magnet assembly are optional horizontal or perpendicular
It is fastenedly connected with segregation apparatus matrix after placing；Described magnetisable material catalyst separation device bag
Include: segregation apparatus matrix and bar magnet assembly；
Described segregation apparatus matrix includes: material overfall 15, magnetisable material catalyst disengagement chamber
20, material inlet 21 and be used for opening and close described segregation apparatus matrix and realize picking and placeing described magnetic
The segregation apparatus cover plate 24 of rod assembly；Described magnetisable material catalyst disengagement chamber 20 is multiple identical
The multi-pipeline array that formed of pipe-like cavity parallel to each other；Described magnetisable material catalyst divides
Cavity material from chamber 20 is non-magnet_conductible material；Described material inlet 21 and material overfall 15
Connect with described magnetisable material catalyst disengagement chamber 20；
Described bar magnet assembly includes: magnetic rod sleeve pipe battle array 22 and bar magnet 23；Described magnetic rod sleeve pipe
Battle array 22 is the many cannula array being made up of the multiple identical magnetic rod sleeve shelved parallel to each other, often
Individual described magnetic rod sleeve accommodates a bar magnet；Described magnetic rod sleeve pipe battle array 22 is by non-magnet_conductible material system
Become；The sleeve pipe caliber of described magnetic rod sleeve pipe battle array 22 is adaptive with the outside dimension of described bar magnet 23；
Described magnetic rod sleeve pipe battle array 22 is anchored on magnetisable material catalyst disengagement chamber 20 by clamp device；
The axis of described magnetic rod sleeve any one magnetic rod sleeve of pipe battle array 22 and described magnetisable material catalyst
The axis of the pipeline being inserted into accordingly in disengagement chamber 20 coincides.
Embodiment two:
Shown in Fig. 6, the invention provides a kind of magnetisable material catalyst separation device, described magnetic
Material catalyst segregation apparatus includes: segregation apparatus matrix and bar magnet assembly；
Described segregation apparatus matrix includes: material overfall 15, material buffer chamber 18, Magnetic Materials
Matter catalyst disengagement chamber 20, material inlet 21 and be used for opening and close described segregation apparatus matrix
Realize picking and placeing the segregation apparatus cover plate 24 of described bar magnet assembly；Described magnetisable material catalyst separates
Chamber 20 is the multi-pipeline array that multiple identical pipe-like cavity parallel to each other is formed；Described magnetic
The cavity material of property material catalyst disengagement chamber 20 is non-magnet_conductible material；Described material buffer chamber 18
Connect with described material inlet 21；Described material buffer chamber 18 is divided with described magnetisable material catalyst
It is connected from chamber 20；Described magnetisable material catalyst disengagement chamber 20 is with described material overfall 15 even
Logical；Described material inlet 21 is positioned at the bottom in described material buffer chamber 18；Described material buffer chamber
18 bottoms being positioned at described magnetisable material catalyst disengagement chamber 20；Described segregation apparatus cover plate 24
Top in described magnetisable material catalyst disengagement chamber 20；Described material overfall 15 is positioned at described；
The upper end of segregation apparatus base side walls, concordant with the lower surface of described segregation apparatus cover plate 24.
Described bar magnet assembly includes: magnetic rod sleeve pipe battle array 22 and bar magnet 23；Described magnetic rod sleeve pipe
Battle array 22 is the many cannula array being made up of the multiple identical magnetic rod sleeve shelved parallel to each other, often
Individual described magnetic rod sleeve accommodates a bar magnet；Described magnetic rod sleeve pipe battle array 22 is by non-magnet_conductible material system
Become；The sleeve pipe caliber of described magnetic rod sleeve pipe battle array 22 is adaptive with the outside dimension of described bar magnet 23；
Described magnetic rod sleeve pipe battle array 22 is anchored on magnetisable material catalyst disengagement chamber 20 by clamp device；
The axis of described magnetic rod sleeve any one magnetic rod sleeve of pipe battle array 22 and described magnetisable material catalyst
The axis of the pipeline being inserted into accordingly in disengagement chamber 20 coincides；Described bar magnet 23 diameter
25mm；Sleeve pipe caliber 27 mm of described magnetic rod sleeve pipe battle array 22；Described magnetic rod sleeve pipe battle array 22
Pipe thickness 0.5mm of magnetic rod sleeve；The single pipe of described magnetisable material catalyst disengagement chamber 20
The caliber in road is 76mm；Described bar magnet 23 is the bar magnet of 15000gs；Described magnetisable material is catalyzed
The caliber of the single pipeline of agent disengagement chamber 20 is less than 60mm with the difference of the external diameter of described bar magnet 23；Institute
State material inlet 21 be provided with flow speed control valve and drain valve；Described non-magnet_conductible material is PP；Described magnetic
Rod is permanent magnet or electric magnet.
Embodiment three:
Shown in Fig. 7, the invention provides a kind of magnetisable material catalyst separation device, described magnetic
Property material catalyst segregation apparatus includes: segregation apparatus matrix and bar magnet assembly；
Described segregation apparatus matrix includes: material overfall 15, temperature control medium A interface 16, control
Temperature medium chuck layer 17, material buffer chamber 18, temperature control medium B interface 19, magnetisable material are urged
Agent disengagement chamber 20, material inlet 21 and be used for opening and close described segregation apparatus matrix and realize
Pick and place the segregation apparatus cover plate 24 of described bar magnet assembly；Described magnetisable material catalyst disengagement chamber 20
The multi-pipeline array formed for multiple identical pipe-like cavitys parallel to each other；Described Magnetic Materials
Matter catalyst disengagement chamber viewgraph of cross-section is as shown in figure 11；Described magnetisable material catalyst disengagement chamber
The cavity material of 20 is non-magnet_conductible material；Described temperature control medium B interface 19 height is higher than described
Temperature control medium A interface 16；Described material buffer chamber 18 connects with described material inlet 21；Institute
State material buffer chamber 18 to be connected with described magnetisable material catalyst disengagement chamber 20；Described magnetic
Material catalyst disengagement chamber 20 connects with described material overfall 15；Described material inlet 21
Bottom in described material buffer chamber 18；Described material buffer chamber 18 is positioned at described magnetisable material
The bottom of catalyst disengagement chamber 20；Described segregation apparatus cover plate 24 is positioned at described magnetisable material and urges
The top of agent disengagement chamber 20；Described material overfall 15 is positioned at described segregation apparatus matrix side
The upper end of wall, concordant with the lower surface of described segregation apparatus cover plate 24.
Described bar magnet assembly includes: magnetic rod sleeve pipe battle array 22 and bar magnet 23；Shown in Fig. 8, described
Magnetic rod sleeve pipe battle array 22 is the many sets being made up of the multiple identical magnetic rod sleeve shelved parallel to each other
Pipe array, each described magnetic rod sleeve accommodates a bar magnet；Bar magnet profile is as shown in Figure 9；Institute
State magnetic rod sleeve pipe battle array 22 to be made up of non-magnet_conductible material；The sleeve pipe of described magnetic rod sleeve pipe battle array 22
Caliber is adaptive with the outside dimension of described bar magnet 23；Fill the described magnetic rod sleeve pipe battle array effect of bar magnet
Fruit figure is as shown in Figure 10；Described magnetic rod sleeve pipe battle array 22 is fixed on by card buckle-like clamp device
Magnetisable material catalyst disengagement chamber 20；Described magnetic rod sleeve any one magnetic rod sleeve of pipe battle array 22
The axis phase of axis and the corresponding pipeline being inserted in described magnetisable material catalyst disengagement chamber 20
Overlap；Described bar magnet 23 diameter 25mm, length 500mm；Described magnetic rod sleeve pipe battle array 22
Sleeve pipe caliber 27 mm, the deep 600mm of sleeve pipe pipe；The bar magnet set of described magnetic rod sleeve pipe battle array 22
Pipe thickness 0.5mm of pipe；The pipe of the single pipeline of described magnetisable material catalyst disengagement chamber 20
Footpath is 76mm；Described bar magnet 23 is the bar magnet of 15000gs；Described material inlet 6 is provided with
Flow speed control valve and drain valve；Described non-magnet_conductible material is PP, and described bar magnet is permanent magnet.
Material enters segregation apparatus matrix from material inlet, is arrived by material buffer chamber and separates dress
Put baseline top, overflow from material overfall.Tubular conduit in the middle of material buffer chamber is magnetic
The place that material catalyst impurity and bar magnet are fully contacted, is also the key position of lock out operation.
According to the different qualities of material, the selection of temperature control medium also differs.Choosing due to temperature control medium
Selecting difference, the import and export direction of temperature control medium is the most different.Such as: selecting steam is temperature control medium,
Steam enters from temperature control medium B interface, discharges from temperature control medium A interface；If selecting water to do temperature control
Medium, water enters from temperature control medium A interface, discharges from temperature control medium B interface.
Embodiment four:
Process chart shown in Figure 12, on a kind of phenyl ring, the phenols of band chlorine carries out raney ni catalysis and adds
During hydrogen, dechlorination becomes the most chloride another kind of phenol.One magnetisable material catalyst of the present invention
Segregation apparatus 29 present position in whole technique is transfer head tank 28 and neutralizes between still 30.
This catalytic hydrogenation is carried out in a high-pressure hydrogenation still 25, has reacted and has been delivered to afterwards
Subsider 26, settles most of oarse-grained catalyst in subsider, passes through bottom valve
Discharge, the catalyst particle of suspension by membrane pump 27 be transported to after transfer head tank 28 through
Magnetisable material catalyst separation device 29 separates, and the material after separation is urged by magnetisable material
The overfall of agent segregation apparatus 29 is transported to neutralize in still 30.
Separating effect is described as follows:
Every batch of hydrogenation reaction duration moon 6h, every crowd of charging 800kg, described Raney's nickel catalyst feeds
2.5kg, reactor 4 groups, about carry out 16 batch reactions every day.
Wherein catalyst every batch about 1.8-2kg can be discharged by subsider, and about every day has
10kg catalyst is reclaimed after being adsorbed by bar magnet.
Dividing water system and organic system by the material of magnetisable material catalyst separation device 29, washing accounts for
70%, organic system accounts for 30%.The catalyst suspension trace of water system, can ignore, and remains in material
Catalyst be exactly the weight ratio of about 1% described above.After process, catalyst content is also micro-
Amount, by the organic system after segregation apparatus of 1kg is carried out 0.1 micron filter cloth filtration treatment,
Residual catalyst meansigma methods 2.3g (content 0.23%) on filter cloth, separating effect is ideal,
Visible in subsider sedimentation after material, by magnetisable material catalyst separation device 29 it
After, adsorbable impurity has all obtained very effective separation.
Embodiment five:
Multiple magnetisable material catalyst separation devices are used in series, constitute a kind of magnetisable material and urge
Agent piece-rate system, described magnetisable material catalyst separation system can reach more preferably Magnetic Materials
Matter catalyst separating effect.During serial operation, adjacent two magnetisable material catalyst separation devices,
It is positioned at the material overfall 15 of the magnetisable material catalyst separation device of higher level and the magnetic being positioned at subordinate
The material inlet 21 of property material catalyst segregation apparatus is connected.
Embodiment of above is merely to illustrate the present invention, rather than limitation of the present invention.Although ginseng
Being described in detail the present invention according to embodiment, those of ordinary skill in the art should manage
Solve, technical scheme is carried out various combination, amendment or equivalent, does not takes off
From the spirit and scope of technical solution of the present invention, all should contain in scope of the presently claimed invention
In the middle of.
Claims (9)
1. a magnetisable material catalyst separation device, it is characterised in that described magnetisable material is urged
Agent segregation apparatus includes: segregation apparatus matrix, bar magnet assembly and fluid attemperating unit；
Described segregation apparatus matrix includes: material overfall (15), magnetisable material catalyst separate
Chamber (20), material inlet (21) and be used for opening and close described segregation apparatus matrix and realize taking
Put the segregation apparatus cover plate (24) of described bar magnet assembly；Described magnetisable material catalyst disengagement chamber
(20) it is the multi-pipeline array that formed of multiple identical pipe-like cavity parallel to each other；Described
The cavity material of magnetisable material catalyst disengagement chamber (20) is non-magnet_conductible material；Described material enters
Mouth (21) and material overfall (15) are with described magnetisable material catalyst disengagement chamber (20) even
Logical；
Described bar magnet assembly includes: magnetic rod sleeve Guan Zhen (22) and bar magnet (23)；Described bar magnet
Sleeve pipe Guan Zhen (22) is the many sets being made up of the multiple identical magnetic rod sleeve shelved parallel to each other
Pipe array, each described magnetic rod sleeve accommodates a bar magnet；Described magnetic rod sleeve Guan Zhen (22)
It is made up of non-magnet_conductible material；The sleeve pipe caliber of described magnetic rod sleeve Guan Zhen (22) and described bar magnet
(23) outside dimension is adaptive；Described magnetic rod sleeve Guan Zhen (22) is fastened by clamp device
In magnetisable material catalyst disengagement chamber (20)；Described magnetic rod sleeve Guan Zhen (22) any one magnetic
The axis of rod sleeve pipe is to described magnetisable material catalyst disengagement chamber (20) corresponding to be inserted into
The axis of pipeline coincides；
Described fluid attemperating unit is wrapped in the chamber of described magnetisable material catalyst disengagement chamber (20)
External wall, including: temperature control medium A interface (16), temperature control medium chuck layer (17) and temperature control
Medium B interface (19)；Described temperature control medium chuck layer (17) is the cavity taking up temperature control medium；
Described temperature control medium A interface (16) is positioned at the end of described temperature control medium chuck layer (17) side
End；Described temperature control medium B interface (19) is positioned at described temperature medium chuck layer (17) side
Top.
A kind of magnetisable material catalyst separation device the most according to claim 1, its feature
It is, between described material inlet (21) and magnetisable material catalyst disengagement chamber (20) also
It is provided with material buffer chamber (18)；Described material buffer chamber (18) and described material inlet (21)
Connection；Described material buffer chamber (18) and described magnetisable material catalyst disengagement chamber (20) phase
Connection.
A kind of magnetisable material catalyst separation device the most according to claim 2, its feature
Being, described material inlet (21) is positioned at the bottom of described material buffer chamber (18)；Described
Material buffer chamber (18) is positioned at the bottom of described magnetisable material catalyst disengagement chamber (20)；Institute
State segregation apparatus cover plate (24) and be positioned at the top of described magnetisable material catalyst disengagement chamber (20)；
Described material overfall (15) is positioned at the upper end of described segregation apparatus base side walls, with described point
Concordant from the lower surface of device cover plate (24).
A kind of magnetisable material catalyst separation device the most according to claim 3, its feature
It is, described bar magnet (23) diameter 25mm；The sleeve pipe pipe of described magnetic rod sleeve Guan Zhen (22)
Footpath 27mm；Pipe thickness 0.5mm of the magnetic rod sleeve of described magnetic rod sleeve Guan Zhen (22)；
The caliber of the single pipeline of described magnetisable material catalyst disengagement chamber (20) is 76mm.
A kind of magnetisable material catalyst separation device the most according to claim 4, its feature
Being, described bar magnet (23) is the bar magnet of 15000gs；Described magnetisable material catalyst separates
The caliber of the single pipeline in chamber (20) is less than 60mm with the difference of the external diameter of described bar magnet (23).
A kind of magnetisable material catalyst separation device the most according to claim 5, its feature
Being, described material inlet (21) is provided with flow speed control valve and drains valve.
7. according to a kind of magnetisable material catalyst separation device described in any one of claim 2～6,
It is characterized in that, described non-magnet_conductible material is PP.
8. according to a kind of magnetisable material catalyst separation device described in any one of claim 2～6,
It is characterized in that, described bar magnet is permanent magnet or electric magnet.
9. a magnetisable material catalyst separation system, it is characterised in that include by claim
The multistage Magnetic Materials that magnetisable material catalyst separation device described in 1～8 any one is in series
Matter catalyst separation system；Adjacent two magnetisable material catalyst separation devices, are positioned at higher level's
Material overfall (15) and the magnetisable material being positioned at subordinate of magnetisable material catalyst separation device
The material inlet (21) of catalyst separation device is connected.
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| CN201410420799.XA CN104209185B (en) | 2014-08-25 | 2014-08-25 | Magnetic material catalyst separating device and system |
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| CN104209185B true CN104209185B (en) | 2017-01-11 |
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| US9352331B1 (en) * | 2015-09-26 | 2016-05-31 | Allnew Chemical Technology Company | Filters for paramagnetic and diamagnetic substances |
| CN105617752B (en) * | 2016-01-29 | 2018-04-10 | 宁德东恒机械有限公司 | A kind of permanent-magnet filtration device |
| CN108640400A (en) * | 2018-05-08 | 2018-10-12 | 吉林建筑大学 | A kind of method and apparatus of the quick overlay film of water process magnetic photocatalyst |
| CN110698039A (en) * | 2019-09-18 | 2020-01-17 | 彩虹（合肥）液晶玻璃有限公司 | Magnetic grid device and liquid crystal glass substrate production system |
| CN110702887A (en) * | 2019-10-22 | 2020-01-17 | 中国水务投资有限公司 | Magnetic resin loss rate measuring device and measuring method |
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