Solvent regeneration tower tower top condensing system and lamella heat exchanger used
Technical field
The invention belongs to heat transfer technology field, relate to a kind of arrangement of solvent regeneration tower tower top condensing system and lamella heat exchanger used, belong to heat transfer unit (HTU) technical field.
Background technology
Solvent regeneration tower (abbreviation regenerator) is the rectifying column configuration of an employing fractional distilling tube, liquid phase infinite reflux.Enter most of sour gas that the still liquid of solvent regeneration tower contains and resolve in tower, then enter Regenerator Bottom Reboiler and be further heated desorb, solvent liquid is fully regenerated; A large amount of gas phase medias of tower top are cooled to liquid phase by refrigerant in overhead condenser simultaneously, then by natural back flow (as Fig. 1) or two kinds of forms of forced refluence (as Fig. 2), the liquid phase medium of condensation are back to tower top.Natural back flow is to utilize high potential difference between overhead condenser and tower refluxing opening to realize the backflow of cooling medium, and forced refluence adopts pump that transmitting power is provided.
Above-mentioned existing regeneration overhead condenser is deposited deficiency both ways: (1) forced refluence mode technology arrangement complexity.Natural back flow technological process is relatively simple, and the layout absolute altitude of still comparing forced refluence mode overhead condenser must be high higher than the regeneration overhead standard laid down by the ministries or commissions of the Central Government, and heat exchanger wants cube little, lightweight.(2) overhead condenser seriously corroded.Regenerator tower overhead gas enters condenser, the CO in medium
2-H
2s-H
2o can cause homogeneous corrosion, hydrogen blister, hydrogen embrittlement and the stress corrosion cracking of heat exchanger inside.Heat exchanger internal corrosion is serious, and service life is short, needs frequent parking maintenance and replacing, greatly reduces plant capacity, and maintenance of equipment expense raises.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of solvent regeneration tower tower top condensing system and lamella heat exchanger used; Lamella heat exchanger has little, the lightweight feature of volume, can directly support the top that is arranged on regenerator; Thereby make solvent regeneration tower tower top condensing system of the present invention can adopt natural back flow mode the liquid phase medium of condensation to be back to the top of regenerator.
In order to solve the problems of the technologies described above, the invention provides a kind of lamella heat exchanger, comprise cylinder shell, plate core group, baffle, plate journey inlet nipple, plate journey outlet ozzle, shell side inlet nipple, shell side outlet ozzle, pressure strip, plate core flange face and shell flange face; At the front end of cylinder shell, shell flange face is set, the rear end of cylinder shell is sealed end;
Plate is circular corrugated cardboard sheet, and 1 circular medium import and 1 circular media outlet are set respectively on plate, and described medium import, the line of centres of media outlet and the central point of plate are located along the same line;
(each plate to being faced between two by two plates 11, two plate 11 fronts are to front) the circumferential edges along 2 medium imports weld and weld along the circumferential edges of 2 media outlets simultaneously, thereby the corresponding sealing of the medium import that makes 2 plates coincide, the media outlet of 2 plates also corresponding sealing coincide; Gap between right 2 plates of each plate forms shell side runner;
Thereby several plates between form plate core group 2 along excircle welding: 2 adjacent plates are to upper, respectively get a slice and face the plate that adjacent panels is right, excircle seal welding by these 2 plates along plate, thus make the gap between 2 right plates of 2 adjacent plates form plate journey runner (17);
In plate core group, the center line of all medium imports coincides, and all medium imports are connected to form medium inlet road; In plate core group, the center line of all media outlets coincides, and all media outlets are connected to form media outlet pipeline;
The two ends of plate core group are fixedly linked with plate core flange face and pressure strip respectively, the center line of plate core group and plate core flange face and pressure strip coincide (, 3 arranged concentric).
Baffle is arc, and the length of baffle equals the length of plate core group;
In plate core group a baffle is each side set, weld with plate core flange face, pressure strip respectively at the two ends of every baffle, the medial surface of baffle and plate core group keep the gap of 5~10mm, thereby make plate core flange face, plate core group, pressure strip and 2 baffles form a welding integral; Plate core group, pressure strip and 2 baffles in this welding integral are loaded in cylinder shell, and the rear end (, sealed end) of pressure strip and cylinder shell keeps the fit-up gap of 5~20mm; The lateral surface of baffle is close to the inwall of cylinder shell; Shell flange face and plate core flange face are fixedly linked;
Be respectively equipped with shell side inlet nipple, shell side outlet ozzle at the upper lower wall surface of cylinder shell; Shell side inlet nipple, shell side outlet ozzle all with the intracavity inter-connection of cylinder shell; And the line (line of centres) between shell side inlet nipple, shell side outlet ozzle and the line (line of centres) between 2 baffles are " ten " word shape;
Plate journey inlet nipple and plate journey outlet ozzle are set respectively on plate core flange face; Plate journey inlet nipple is connected with medium inlet road, and plate journey outlet ozzle is connected with media outlet pipeline.
Improvement as lamella heat exchanger of the present invention:
The line of centres of the ripple on plate and medium import, media outlet forms angle α; Angle α for example can be 50~70 °.
Each plate to by two plates 11 between two in the face of time, the both sides of the line of centres that is positioned at medium import and media outlet of the angle α symmetry on two plates; Ripple interlaced arrangement on these two plates, it is staggered netted that shell side runner is.
Further improvement as lamella heat exchanger of the present invention:
The both sides of the line of centres that be positioned at medium import and media outlet of 2 adjacent plates to the angle α symmetry on be above welded to each other two plates; Ripple interlaced arrangement on these two plates, it is staggered netted that plate journey runner is.
Further improvement as lamella heat exchanger of the present invention:
Described plate core flange face is rounded, and the diameter of described plate core flange face is than the large 40~150mm of the diameter of plate;
Described pressure strip is rounded, and the diameter of described pressure strip equals the diameter of plate.
Further improvement as lamella heat exchanger of the present invention:
Described baffle is that radian is the arc of π/6~π/4.
Further improvement as lamella heat exchanger of the present invention:
Described plate is the corrugated cardboard sheet that titanium material is made, and the degree of depth h of the ripple on plate is 2.5mm~4mm, and the width L of ripple is 10mm~15mm;
The present invention also provides the solvent regeneration tower tower top condensing system that utilizes above-mentioned lamella heat exchanger to be prepared from simultaneously, and this solvent regeneration tower tower top condensing system comprises the lamella heat exchanger and point flow container that are arranged on successively from top to bottom regenerator top;
Divide the sidewall of flow container to be respectively equipped with from top to bottom exhaust outlet and phegma ozzle, be provided with the liquid seal device of overflow pipe in the bottom of point flow container;
The gas vent of regenerator is connected with shell side inlet nipple (be positioned at the sidewall near tower top, this belongs to prior art), and shell side outlet ozzle is connected with phegma ozzle; The external cooling water of plate journey inlet nipple.
Improvement as solvent regeneration tower tower top condensing system of the present invention:
Thermal medium (being tower overhead gas) in regenerator 300 enters shell side inlet nipple from gas vent; This thermal medium is condensed after by shell side runner, and the two-phase fluid of condensation flows in point flow container by phegma ozzle from shell side outlet ozzle flows out;
Cooling water slave plate journey inlet nipple in medium inlet road enters plate journey runner, the cooling water after intensification finally after media outlet pipeline slave plate journey outlet ozzle flow out.
Beneficial effect of the present invention is specific as follows:
(1) arrangement of this kind of cooling system, in the built-in cold condenser of regeneration overhead, adopts natural back flow mode the liquid phase medium of condensation to be back to point flow container that is positioned at regenerator top, and technological process is simple.And because lamella heat exchanger adopts titanium plate, good corrosion resistance, can greatly reduce the replacement frequency of equipment, reduces to greatest extent mounting cost and the maintenance cost of device, and assurance device long period safe and reliable operation.
(2) be provided with the liquid seal device of overflow pipe in condensate outlet setting, ensure that condensate liquid can discharge heat-exchange tube smoothly, prevent thermal medium gas backflow in tower simultaneously.
(3) heat exchange plate (plate) adopts the corrugated plating can enhanced heat exchange, and heat exchange efficiency is high.
Brief description of the drawings
Below in conjunction with accompanying drawing, the specific embodiment of the present invention is described in further detail.
Fig. 1 is the natural back flow arrangement (prior art) of overhead condenser;
Fig. 2 is the forced refluence arrangement (prior art) of overhead condenser;
Fig. 3 is the schematic diagram of the solvent regeneration tower tower top condensing system that is arranged on regenerator top of the present invention;
Fig. 4 is the structural representation (for explosive view) of the lamella heat exchanger in Fig. 3;
Fig. 5 is the front view (front elevation) of the plate 11 in Fig. 4;
Fig. 6 is that partial schematic diagram is looked on the right side of Fig. 5;
Fig. 7 is the rearview (reverse side figure) of Fig. 5;
Fig. 8 is the fundamental diagram of Fig. 3.
In figure, 1-cylinder shell; 2-plate core group; 3-baffle; 4-plate journey inlet nipple; 5-plate journey outlet ozzle; 6-shell side inlet nipple; 7-shell side outlet ozzle; 8-pressure strip; 9-plate core flange face; 10-shell flange face; 11-plate; 12-screwed hole; The import of 13-medium; 14-media outlet; 15-medium inlet road; 16-media outlet pipeline; 17-plate journey runner; 18--shell side runner;
20-exhaust outlet; 30-phegma ozzle; 40-is with the liquid seal device of overflow pipe; 50-gas vent; 100-lamella heat exchanger; 200-divides flow container; 300-regenerator.
Detailed description of the invention
Below in conjunction with drawings and Examples, the specific embodiment of the present invention is further described, following examples are only for technical scheme of the present invention is more clearly described, and can not limit the scope of the invention with this.
Embodiment 1, a kind of lamella heat exchanger, as shown in Figure 4, comprise cylinder shell 1, plate core group 2, baffle 3, plate journey inlet nipple 4, plate journey outlet ozzle 5, shell side inlet nipple 6, shell side outlet ozzle 7, pressure strip 8, plate core flange face 9, shell flange face 10.
The front end of cylinder shell 1 is provided with shell flange face 10, and the rear end of cylinder shell 1 is sealed end.
Specific as follows:
Plate 11 is as shown in Fig. 5, Fig. 6 and Fig. 7, and plate 11 is corrugated cardboard sheet (preferentially selecting the corrugated cardboard sheet of making for titanium material), and the degree of depth h of ripple is set in 2.5mm~4mm, and the width L of ripple is set in 10mm~15mm; In plate 11 upper, 1 circular 13 and 1 circular media outlet 14 of medium import is set respectively.The line of centres of described medium import 13, media outlet 14 and the central point of plate 11 are located along the same line.The line of centres of the ripple on plate 11 and medium import 13, media outlet 14 forms angle α.
(each plate to being faced between two by two plates 11, two plate 11 fronts are to front) the circumferential edges along 2 medium imports 13 weld and weld along the circumferential edges of 2 media outlets 14 simultaneously, now, the corresponding sealing of the medium import 13 of 2 plates 11 coincide, and the media outlet 14 of 2 plates 11 also corresponding sealing coincide.Gap between right 2 plates 11 of each plate forms shell side runner 18;
Remarks explanation: Fig. 5 is the front view of plate 11, and Fig. 7 is the reverse view of plate 11,
The meaning that two plates 11 are faced is between two exactly: the both sides of the line of centres that is positioned at medium import 1, media outlet 14 of the angle α symmetry on two plates 11.Form thus the interlaced arrangement of ripple and ripple.Therefore shell side runner 18 is staggered netted.
Thereby several plates between form plate core group 2 along excircle welding; Specific as follows: 2 adjacent plates, to upper, respectively got a slice and faced the plate 11 that adjacent panels is right, the excircle seal welding by these 2 plates 11 along plate 11, thus make the gap between above-mentioned 2 plates 11 form plate journey runner 17.Now, the both sides of the line of centres that is positioned at medium import 13 and media outlet 14 of the angle α symmetry on above-mentioned two plates 11 that are welded to each other.Ripple interlaced arrangement on these two plates 11, therefore plate journey runner 17 is also staggered netted.
In plate core group 2, the center line of all medium imports 13 coincides, and all medium imports 13 are connected to form medium inlet road 15; In like manner, in plate core group 2, the center line of all media outlets 14 coincides, and all media outlets 14 are connected to form media outlet pipeline 16.
Weld with plate core flange face 9 and pressure strip 8 respectively at the two ends of plate core group 2, the size that the excircle of plate core flange face 9 is greater than plate 11 (, generally, the diameter of plate core flange face 9 is than the large 40~150mm of the diameter of plate 11), and the excircle of pressure strip 8 is with the excircle of plate 11 measure-alike (, the diameter of the diameter=plate 11 of pressure strip 8).Plate core group 2 and plate core flange face 9 and pressure strip 8 arranged concentric (, 3 center line coincides).
The arc that baffle 3 is π/6~π/4 for radian, the length of length=plate core group 2 of this arc; Be provided with altogether 2 baffles 3.
Plate core group 2 a baffle 3 is each side set, the two ends of every baffle 3 are connected by the mode of welding with plate core flange face 9, pressure strip 8 respectively.This model core flange face 9, plate core group 2, pressure strip 8, baffle 3 (totally 2) has just formed a welding integral.Plate core group 2 in this welding integral, 8 and 2 baffles 3 of pressure strip are loaded in cylinder shell 1, and the rear end (, sealed end) of pressure strip 8 and cylinder shell 1 keeps the fit-up gap of 5~20mm; The lateral surface of baffle 3 is close to the inwall of cylinder shell 1.The gap that the medial surface of baffle 3 and plate core group 2 keep 5~10mm; Shell flange face 10 is provided with screwed hole 12, and plate core flange face 9 is provided with the screwed hole corresponding with screwed hole 12, and therefore, shell flange face 10 can be realized and being connected by bolt with plate core flange face 9.
Be respectively equipped with shell side inlet nipple 6, shell side outlet ozzle 7 at the upper lower wall surface of cylinder shell 1; Described shell side inlet nipple 6, shell side outlet ozzle 7 respectively with the intracavity inter-connection of cylinder shell 1., the line between shell side inlet nipple 6, shell side outlet ozzle 7 and the line between 2 baffles 3 are " ten " word shape.
On plate core flange face 9, be respectively equipped with plate journey inlet nipple 4 and plate journey outlet ozzle 5; Plate journey inlet nipple 4 is connected with medium inlet road 15, and plate journey outlet ozzle 5 is connected with media outlet pipeline 16.
Embodiment 2, the solvent regeneration tower tower top condensing system that utilizes the lamella heat exchanger described in embodiment 1 to be prepared from, as shown in Figure 3: this solvent regeneration tower tower top condensing system comprises to be installed successively from top to bottom (can realize installations by the mode of conventional reinforcing support member) at the lamella heat exchanger 100 at regenerator 300 tops and divides a flow container 200; The sidewall of the close tower top of regenerator 300 is provided with gas vent 50.
Divide the sidewall of flow container 200 to be respectively equipped with from top to bottom exhaust outlet 20 and phegma ozzle 30, be provided with the liquid seal device 40 (belonging to routine techniques) of overflow pipe in the bottom of point flow container 200.The fluid-tight of certain altitude (being generally set as 400~600mm in the present invention) simultaneously can also prevent thermal medium gas backflow (belonging to routine techniques) in tower.
Remarks explanation: this 400~600mm refers to overflow pipe and divides the tie point of flow container 200 to the distance of overflow pipe bottom.
Phegma ozzle 30 is connected with shell side outlet ozzle 7; Can discharge smoothly to ensure condensate liquid.Gas vent 50 is connected with shell side inlet nipple 6.
Plate journey inlet nipple 4 external cooling waters.
Operation principle following (as shown in Figure 8):
1, shell side runner:
Thermal medium (being tower overhead gas) in regenerator 300 rises at the bottom of tower, through lower resistance part (the regenerator autogamy in regenerator 300, belong to prior art, in Fig. 3, made drawing and omitted processing) rise to tower top, enter shell side inlet nipple 6 from gas vent 50;
Due to plate core group 2 a baffle 3 is each side set, therefore, gas can directly not flow to shell side outlet ozzle 7 along the inwall of cylinder shell 1, but by each plate to formed shell side runner 18 after, then gather to shell side outlet ozzle 7; The two-phase fluid of condensation flows out from shell side outlet ozzle 7; The two-phase fluid of this condensation flows in point flow container 200 from phegma ozzle 30;
2, plate journey runner:
Cooling water slave plate journey inlet nipple 4 flows in plate core group 2, enters respectively in the plate journey runner 17 of plate core group 2 after the shunting in medium inlet road 15, and the cooling water after intensification is finally collected rear slave plate journey outlet ozzle 5 by media outlet pipeline 16 and flowed out.
Remarks explanation: the cooling water of plate journey runner 17 and the tower overhead gas of shell side runner 18 form adverse current (wall-type heat exchange is carried out in the both sides at plate 11), take away latent heat and sensible heat that tower overhead gas discharges, congealing in tower overhead gas point is condensed into liquid state (being condensate liquid).In tower overhead gas, also containing some on-condensible gas, component is generally H
2s, COS, N
2, CO
2deng, be referred to as sour gas.Condensate liquid enters in point flow container 200 and separates with the two-phase fluid of sour gas composition.Condensate liquid is gravitate in point flow container 200, enters overflow pipe by condensate outlet, is back to the tower tray (for parts in tower disc type regenerator) in regenerator 300.Sour gas after gas-liquid separation, is expelled to torch from exhaust outlet 20.
Remarks explanation: torch is the common apparatus in petrochemical plant, purposes is discharge after chemical gases that some can be polluted atmosphere is burnt.
In order to ensure the reliability of solvent regeneration tower tower top condensing system, should make two media (tower overhead gas and cooling water) not contact, do not leak, equipment must seal closely.This condenser heat transfer element is titanium plate (being that plate 11 is titanium plate), thereby forms plate pair by the circumferential edges of fully-automatic laser welding medium import and export 13 and the circumferential edges of media outlet 14 between two plates 11; Plate between weld plate 11 by fully-automatic laser excircle finally form plate core group 2.The present invention, owing to using full-welding plate-type version, makes this condenser in performance heat-exchangers of the plate type efficient heat transfer performance, has ensured sealing property, has improved bearing capacity, and device security is reliable.
And traditional overhead condenser adopts shell-and-tube heat exchanger more, volume is large, and Heavy Weight cannot be arranged as one with regenerator, and independent bracket basis need to be set conventionally.And lamella heat exchanger of the present invention has that heat transfer efficiency is high, densification and the advantage such as lightweight, make it can be arranged in the top of regenerator 300, become one with regenerator 300, and do not need independent external supporting structure.
After testing, the heat transfer coefficient of lamella heat exchanger 100 of the present invention is 2~4 times of common tube shell heat exchanger.
Finally, it is also to be noted that, what more than enumerate is only several specific embodiments of the present invention.Obviously, the invention is not restricted to above embodiment, can also have many distortion.All distortion that those of ordinary skill in the art can directly derive or associate from content disclosed by the invention, all should think protection scope of the present invention.