CN104190669B - Glassware cleaning method - Google Patents
Glassware cleaning method Download PDFInfo
- Publication number
- CN104190669B CN104190669B CN201410453570.6A CN201410453570A CN104190669B CN 104190669 B CN104190669 B CN 104190669B CN 201410453570 A CN201410453570 A CN 201410453570A CN 104190669 B CN104190669 B CN 104190669B
- Authority
- CN
- China
- Prior art keywords
- glass apparatus
- cleaning method
- cleanout fluid
- hour
- apparatus cleaning
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B9/00—Cleaning hollow articles by methods or apparatus specially adapted thereto
- B08B9/08—Cleaning containers, e.g. tanks
- B08B9/20—Cleaning containers, e.g. tanks by using apparatus into or on to which containers, e.g. bottles, jars, cans are brought
- B08B9/22—Cleaning containers, e.g. tanks by using apparatus into or on to which containers, e.g. bottles, jars, cans are brought the apparatus cleaning by soaking alone
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B3/00—Cleaning by methods involving the use or presence of liquid or steam
- B08B3/04—Cleaning involving contact with liquid
- B08B3/10—Cleaning involving contact with liquid with additional treatment of the liquid or of the object being cleaned, e.g. by heat, by electricity or by vibration
- B08B3/12—Cleaning involving contact with liquid with additional treatment of the liquid or of the object being cleaned, e.g. by heat, by electricity or by vibration by sonic or ultrasonic vibrations
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/004—Surface-active compounds containing F
- C11D1/006—Surface-active compounds containing fluorine and phosphorus
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/24—Organic compounds containing halogen
- C11D3/245—Organic compounds containing halogen containing fluorine
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/39—Organic or inorganic per-compounds
- C11D3/3942—Inorganic per-compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/395—Bleaching agents
- C11D3/3953—Inorganic bleaching agents
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/43—Solvents
Abstract
The invention discloses a glassware cleaning method. The glassware cleaning method comprises the following steps that glassware is placed into cleaning fluid to be soaked for 5 hours to 8 hours, the temperature of the cleaning fluid is controlled to be 30 DEG C to 50 DEG C from the first hour to the third hour in the soaking process, the cleaning fluid is heated to be boiled from the third hour to the fourth hour in the soaking process, and boiling is carried out for 10 min to 20 min; the cleaning fluid is diluted by adding water, the diluted cleaning fluid is placed in an ultrasonic cleaner, the ultrasonic cleaner is connected with a 220V power source, the temperature of the cleaning fluid is set to be 50 DEG C to 60 DEG C at the same time, and the cleaning time is 10 min to 30 min; washing is carried out with clear water or 3% ethyl alcohol is used for wiping; the glassware is placed into a drying oven to be dried or aired naturally. Due to the mode, the glassware cleaning method is good in durability performance, simple in operation procedure and wide in application range, and the glassware can be washed clean.
Description
Technical field
The present invention relates to a kind of cleaning method, more particularly to a kind of glass apparatus cleaning method.
Background technology
In experimentation, usually lead to viscous in glass apparatus in glass apparatus because of the different differences of chemical experiment
Have stain.Meanwhile, if the interior any point that includes is stain in glass apparatus, experimental result may all be had influence on.Therefore, glass
Glass instrument will remain dried and clean, cleaning to be checked whether before testing every time, will clean in time, dry after experiment.But
The method of current cleaning formula of liquid and cleaning can not reach good cleaning performance.
Content of the invention
The invention mainly solves the technical problem of providing a kind of glass apparatus cleaning method, this cleaning method endurance quality
Good, operating procedure is simple, and cleans up, applied widely.
For solving above-mentioned technical problem, one aspect of the present invention is：A kind of glass apparatus cleaning side is provided
Method, comprises following operating procedure：
Impregnation stage：Glass apparatus are placed in cleanout fluid and is soaked, soak time is 5-8 hour, in immersion process
Middle 1-3 hour, the temperature control of cleanout fluid is 30-50 degree Celsius, in 3-4 hour, cleanout fluid is carried out being heated to boiling,
Boiling time is 10-20 minute.
Wash phase：Described cleanout fluid interpolation water is diluted, the water of interpolation and the ratio of cleanout fluid are 1:1, then
Cleanout fluid after dilution is placed in ultrasonic washing unit, glass apparatus is positioned in the solution of ultrasonic washing unit, will surpass
Sound wave cleaning machine turns on the power supply of 220V, and the temperature setting of just cleanout fluid is 50-60 degree Celsius simultaneously, and scavenging period is
10-30 minute.
Processing stage：Glass apparatus are pulled out, is rinsed with clear water or is wiped with 3% ethanol.
Drying stage：Be rinsed after step with clear water, glass apparatus are put in 80-90 degree Celsius of baking oven dry or
Naturally dry.
In a preferred embodiment of the present invention, before described impregnation stage, can first be washed away using suds, suds
Temperature be 30-35 degree Celsius.
In a preferred embodiment of the present invention, in described impregnation stage, described glass apparatus load plastics mesh bag or mould
Soaked in material basket.
In a preferred embodiment of the present invention, processing stage described, the number of times being rinsed with clear water at least 3 times.
In a preferred embodiment of the present invention, described cleanout fluid includes：Solvent, nitrate, concentrated sulphuric acid, surface activity
Agent, ammonium salt, bleach, calcium hypochlorite and tetrafluoroethene；Calculate according to mass percent：Described solvent occupies 40-60 part, nitre
Hydrochlorate 6-8 part, concentrated sulphuric acid 10-20 part, surfactant 1-5 part, ammonium salt 4-8 part, bleach 1-3 part, hypochlorous acid
Calcium 3-5 part and tetrafluoroethene 2-5 part.
In a preferred embodiment of the present invention, described solvent is organic solvent or water, and organic solvent is ethylene glycol, second two
Alcohol list ethylether and/or propylene glycol.
In a preferred embodiment of the present invention, described nitrate is potassium nitrate
In a preferred embodiment of the present invention, described surfactant is phosphate, described phosphate is tripolyphosphate
Sodium, Magcophos and sodium hexameta phosphate.
In a preferred embodiment of the present invention, described ammonium salt is one of ammonium sulfate or ammonium iodide.
In a preferred embodiment of the present invention, described bleach is Dexol and/or sodium hypochlorite.
The invention has the beneficial effects as follows：This cleaning method excellent in durability, operating procedure are simple, and clean up, and are suitable for
Scope is wide.
Specific embodiment
The enforcement it is clear that described will be clearly and completely described to the technical scheme in the embodiment of the present invention below
Example is only a part of embodiment of the present invention, rather than whole embodiments.Based on the embodiment in the present invention, this area is common
All other embodiment that technical staff is obtained under the premise of not making creative work, broadly falls into the model of present invention protection
Enclose.
The embodiment of the present invention includes：
A kind of glass apparatus cleaning method, comprises following operating procedure：
Impregnation stage：Glass apparatus are placed in cleanout fluid and is soaked, soak time is 5-8 hour, in immersion process
Middle 1-3 hour, the temperature control of cleanout fluid is 30-50 degree Celsius, in 3-4 hour, cleanout fluid is carried out being heated to boiling,
Boiling time is 10-20 minute.
Preferably, glass apparatus are placed in cleanout fluid and soaked, soak time is 5 hours, and 1 is little in immersion process
When, the temperature control of cleanout fluid is 30 degrees Celsius, in 3-4 hour, cleanout fluid is carried out being heated to boiling, boiling time is
10 minutes.
Glass apparatus are placed in cleanout fluid and is soaked, soak time is 8 hours, 3 hours in immersion process, will be clear
The temperature control of washing liquid is 50 degrees Celsius, in 3-4 hour, cleanout fluid is carried out being heated to boiling, and boiling time is 20 minutes.
Glass apparatus are placed in cleanout fluid and is soaked, soak time is 7 hours, 2 hours in immersion process, will be clear
The temperature control of washing liquid is 35 degrees Celsius, in 3-4 hour, cleanout fluid is carried out being heated to boiling, and boiling time is 15 minutes.
Wash phase：Described cleanout fluid interpolation water is diluted, the water of interpolation and the ratio of cleanout fluid are 1:1, then
Cleanout fluid after dilution is placed in ultrasonic washing unit, glass apparatus is positioned in the solution of ultrasonic washing unit, will surpass
Sound wave cleaning machine turns on the power supply of 220V, and the temperature setting of just cleanout fluid is 50-60 degree Celsius simultaneously, and scavenging period is
10-30 minute.Preferably, the temperature setting of cleanout fluid is 55 degrees Celsius, scavenging period is 20 minutes.
Processing stage：Glass apparatus are pulled out, is rinsed with clear water or is wiped with 3% ethanol.
Drying stage：It is rinsed after step with clear water, glass apparatus are put in 80,85 or 90 degrees Celsius of baking oven and dry
Do or naturally dry.
Before described impregnation stage, can first be washed away using suds, the temperature of suds is 30-35 degree Celsius.
In described impregnation stage, soaked in described glass apparatus loading plastics mesh bag or plastics basket.
Processing stage described, the number of times being rinsed with clear water at least 3 times, can be 4 times or 5 times.
In a kind of specific embodiment, described cleanout fluid includes：Solvent, nitrate, concentrated sulphuric acid, surfactant,
Ammonium salt, bleach, calcium hypochlorite and tetrafluoroethene；Calculate according to mass percent：Described solvent occupy 40 parts, 8 parts of nitrate,
20 parts of concentrated sulphuric acid, 5 parts of surfactant, 8 parts of ammonium salt, 3 parts of bleach, 5 parts of calcium hypochlorite and 5 parts of tetrafluoroethene.
In a kind of specific embodiment, described cleanout fluid includes：Solvent, nitrate, concentrated sulphuric acid, surfactant,
Ammonium salt, bleach, calcium hypochlorite and tetrafluoroethene；Calculate according to mass percent：Described solvent occupy 60 parts, 6 parts of nitrate,
10 parts of concentrated sulphuric acid, 1 part of surfactant, 4 parts of ammonium salt, 1 part of bleach, 3 parts of calcium hypochlorite and 2 parts of tetrafluoroethene
In a kind of specific embodiment, described cleanout fluid includes：Solvent, nitrate, concentrated sulphuric acid, surfactant,
Ammonium salt, bleach, calcium hypochlorite and tetrafluoroethene；Calculate according to mass percent：Described solvent occupy 50 parts, 7 parts of nitrate,
15 parts of concentrated sulphuric acid, 3 parts of surfactant, 6 parts of ammonium salt, 2 parts of bleach, 4 parts of calcium hypochlorite and 3 parts of tetrafluoroethene
In the above-described embodiments, described solvent is organic solvent or water, and organic solvent is ethylene glycol, ethylene glycol monomethyl ether
And/or propylene glycol.
Described nitrate is potassium nitrate, and described surfactant is phosphate, described phosphate is sodium tripolyphosphate, four phosphorus
Sour sodium and sodium hexameta phosphate, described ammonium salt is one of ammonium sulfate or ammonium iodide, and described bleach is Dexol and/or secondary
Sodium chlorate.
The beneficial effect of glass apparatus cleaning method of the present invention is：
（1）This cleaning method excellent in durability, operating procedure are simple, and clean up, applied widely；
（2）Cleaning formula of liquid rationally and can reach good cleaning performance.
The foregoing is only embodiments of the invention, not thereby limit the present invention the scope of the claims, every using this
Equivalent structure or equivalent flow conversion that bright description is made, or directly or indirectly it is used in the technology neck of other correlations
Domain, is included within the scope of the present invention.
Claims (9)
1. a kind of glass apparatus cleaning method is it is characterised in that comprise following operating procedure：
Impregnation stage：Glass apparatus are placed in cleanout fluid and is soaked, soak time is 5-8 hour, 1-3 in immersion process
Hour, the temperature control of cleanout fluid is 30-50 degree Celsius, in 3-4 hour, cleanout fluid is carried out being heated to boiling, boils
Time is 10-20 minute；
Wash phase：Described cleanout fluid interpolation water is diluted, the water of interpolation and the ratio of cleanout fluid are 1:1, then will be dilute
Cleanout fluid after releasing is placed in ultrasonic washing unit, and glass apparatus are positioned in the solution of ultrasonic washing unit, by ultrasound wave
Cleaning machine turns on the power supply of 220V, is 50-60 degree Celsius by the temperature setting of cleanout fluid simultaneously, and scavenging period is 10-30
Minute；
Processing stage：Glass apparatus are pulled out, is rinsed with clear water or is wiped with 3% ethanol；
Drying stage：It is rinsed after step with clear water, glass apparatus are put into and dries in 80-90 degree Celsius of baking oven or natural
Dry；
Described cleanout fluid includes：Solvent, nitrate, concentrated sulphuric acid, surfactant, ammonium salt, bleach, calcium hypochlorite and tetrafluoro
Ethylene；Calculate according to mass percent：Described solvent occupies 40-60 part, nitrate 6-8 part, concentrated sulphuric acid 10-20 part, surface work
Property agent 1-5 part, ammonium salt 4-8 part, bleach 1-3 part, calcium hypochlorite 3-5 part and tetrafluoroethene 2-5 part.
2. glass apparatus cleaning method according to claim 1 is it is characterised in that before described impregnation stage, first using fertilizer
Soap water is washed away, and the temperature of suds is 30-35 degree Celsius.
3. glass apparatus cleaning method according to claim 1 is it is characterised in that in described impregnation stage, described glass
Soaked in instrument loading plastics mesh bag or plastics basket.
4. glass apparatus cleaning method according to claim 1 is it is characterised in that processing stage described, rinsed with clear water
Number of times at least 3 times.
5. glass apparatus cleaning method according to claim 1 it is characterised in that described solvent be organic solvent or water,
Organic solvent is ethylene glycol, ethylene glycol monomethyl ether and/or propylene glycol.
6. glass apparatus cleaning method according to claim 5 is it is characterised in that described nitrate is potassium nitrate.
7. glass apparatus cleaning method according to claim 6 it is characterised in that described surfactant be phosphate,
Described phosphate is sodium tripolyphosphate, Magcophos and sodium hexameta phosphate.
8. glass apparatus cleaning method according to claim 7 is it is characterised in that described ammonium salt is ammonium sulfate or ammonium iodide
One of.
9. glass apparatus cleaning method according to claim 8 it is characterised in that described bleach be Dexol and/
Or sodium hypochlorite.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410453570.6A CN104190669B (en) | 2014-09-09 | 2014-09-09 | Glassware cleaning method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410453570.6A CN104190669B (en) | 2014-09-09 | 2014-09-09 | Glassware cleaning method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104190669A CN104190669A (en) | 2014-12-10 |
| CN104190669B true CN104190669B (en) | 2017-02-08 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201410453570.6A Active CN104190669B (en) | 2014-09-09 | 2014-09-09 | Glassware cleaning method |
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Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105327875B (en) * | 2015-09-25 | 2017-09-22 | 长治清华机械厂 | A kind of normal temperature metal washing formulation water-base cleaning liquid purging method |
| CN107916185A (en) * | 2017-12-17 | 2018-04-17 | 柳州市晟铂贸易有限公司 | A kind of highly-efficient glass cleaning solution |
| CN108658455A (en) * | 2018-05-03 | 2018-10-16 | 安徽智胜光学科技有限公司 | A kind of production method of high intensity mobile phone screen glass |
| JP7313222B2 (en) * | 2019-07-29 | 2023-07-24 | 三菱重工業株式会社 | How to clean the wings of rotating equipment |
| CN114472383A (en) * | 2022-01-26 | 2022-05-13 | 斯坦德检测集团股份有限公司 | Cleaning method of liner tube for pyrolysis gas chromatograph-mass spectrometer |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2001046991A (en) * | 1999-08-05 | 2001-02-20 | Hitachi Plant Eng & Constr Co Ltd | Method for washing glass substrate |
| JP4880427B2 (en) * | 2006-11-14 | 2012-02-22 | シャープ株式会社 | Cleaning method and cleaning apparatus |
| CN101695696B (en) * | 2009-09-23 | 2011-08-24 | 镇江市港南电子有限公司 | Method for cleaning silicon chip |
| CN101972756B (en) * | 2010-08-30 | 2012-08-15 | 苏州五方光电科技有限公司 | Lens cleaning process during processing |
| CN103624027B (en) * | 2013-11-22 | 2015-09-23 | 青岛市市立医院 | A kind of cleaning of tube chamber class apparatus, sterilization method |
| CN103861854B (en) * | 2014-03-21 | 2016-03-09 | 鼎泰（湖北）生化科技设备制造有限公司 | A kind of supersonic wave cleaning machine rinses basket |
| CN203764597U (en) * | 2014-04-18 | 2014-08-13 | 常雪芹 | Medical ultrasonic cleaner |
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| CN104190669A (en) | 2014-12-10 |
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Address after: 224011, 3, Renmin Road, Long Gang Town, Yancheng City, Jiangsu Patentee after: Jiangsu seagull Glass Co., Ltd. Address before: 224011 No. 3 Renmin Road, Long Gang Town, Jiangsu, Yancheng City Patentee before: Huaou Ind Co., Ltd., Yancheng City |