CN104173593A - Traditional Chinese medicine composition for promoting blood circulation to arrest pain and preparation method of traditional Chinese medicine composition - Google Patents
Traditional Chinese medicine composition for promoting blood circulation to arrest pain and preparation method of traditional Chinese medicine composition Download PDFInfo
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Abstract
The invention discloses a traditional Chinese medicine composition for promoting blood circulation to arrest pain and a preparation method of the traditional Chinese medicine composition. The traditional Chinese medicine composition comprises the following raw materials: phlomis mongolica, sabinavulgaris, fourleaf peperomia herb, lanhihao, radix tetrastigme, scented daphne root, smallfruit fig aerial root, pittosporum root, ardisia maculosa mez, starntonia chinensis, codonacanthus pauciflorus, peach juvenile branchlet, trevesia palmate and auxiliaries, wherein the auxiliaries are prepared from the following raw materials: white flowered bittercress root, white dead nettle, daphne genkwa and luffa root. According to the traditional Chinese medicine composition for promoting blood circulation to arrest pain, the medicines are reasonable in compatibility, strictly selected and combined to complement each other, the content of the active ingredients is high, and the preparation stability is good. The traditional Chinese medicine composition can be used for internally and externally treating diseases such as various fractures, traumatic injuries, rheumatism bone pain, arthralgia and the like by dispelling wind and eliminating dampness, activating blood circulation and eliminating toxicant, achieving antisepsis and anti-inflammation, promoting reunion of fractured bones and promoting blood circulation to arrest pain, and is remarkable in curative effect, convenient to use, low in cost and free of toxic or side effect.
Description
Technical field
The invention belongs to traditional Chinese medical science pharmaceutical technology field, is Chinese medicine composition of a kind of promoting blood circulation and stopping pain and preparation method thereof specifically.
Background technology
Muscles and bones stasis of blood pain, soft tissue injury that traumatic injury causes are common clinical diseases, and how because wound causes, local meridian qi and blood is impaired, circulatory function obstacle, after treatment, still have serious swelling, twinge, be difficult to action.Rheumatic ostalgia is that wind-cold damp pathogen is invaded due to human body, and wind-cold damp pathogen is invaded after human body, causes muscle arteries and veins blocking barrier, and " stagnation of QI and blood may bring about pain " often causes that congestion and swelling pain occurs at the positions such as human synovial, periosteum, muscle thus.The damage of human body, though there be dividing of wound and interior damage, on the surface, it is mainly the damage of local skin and flesh muscles and bones that wound seems, disorderly, to invade the muscle arteries and veins blocking barrier causing similar with wind-cold damp pathogen for the element of the local damage suffering but human body is affected by external force the function that causes internal organs, meridians, QI and blood.
Doctor trained in Western medicine is conventionally implemented the form of antibiosis antiinflammatory, debridement and suturing, traction, open reduction in the various traumatic injury for the treatment of, wound, fracture to patient, do not reach the object of soothing the channels and quicking the network vessels, promoting blood circulation to restore menstrual flow, meridians and blood vessels are vital for the recovery of wound.Rheumatic ostalgia Therapeutic Method has pain relieving western medicine, naturopathy, massage acupuncture and moxibustion therapy, block therapy, operative treatment etc., but said method all has a lot of defects, some side effect are large, and some costs are high, some treatments itself just allow patient suffering can't bear, hurt like hell.Limbs occur that various wounds, fracture and rheumatic ostalgia all can cause blockage of main and collateral channels, and blockage of main and collateral channels QI and blood is not smooth, and freely wound is not difficult to healing to QI and blood, joint is difficult to restore.
Chinese traditional treatment traumatic injury, rheumatic ostalgia have long history, being all mainly to block so that internal organs are impaired for muscles and bones trauma, swelling and pain due to blood stasis, disharmony between QI and blood, blockage of main and collateral channels, rheumatic ostalgia, muscle arteries and veins, there is congestion and swelling pain etc. in the positions such as human synovial, periosteum, muscle.Traditional Chinese medical science extensive knowledge and profound scholarship, the dredge the meridian passage of the traditional Chinese medical science, promoting blood circulation to remove blood stasis, promoting blood circulation and stopping pain, expelling wind and removing dampness, promote exactly the regeneration capacity of human body, evident in efficacy for treatment articular sprain, muscle sprain, blood stasis swelling, disharmony between QI and blood, blockage of main and collateral channels, rheumatic ostalgia, muscle arteries and veins obstruction etc.
The medicament categories of existing treatment traumatic injury and rheumatic ostalgia is various, but the most unsatisfactory curative effect of these medicines, not only the course for the treatment of the long misery that has increased patient, but also have that medical expense is high, cure rate is low, antiinflammatory and the problem such as analgesic effect is not obvious.The present invention provides a kind of new medicament selection for symptoms such as the muscles and bones trauma that the diseases such as traumatic injury, rheumatic ostalgia, fracture cause, swelling and pain due to blood stasis, disharmony between QI and blood, blockage of main and collateral channels, rheumatic ostalgia, muscle arteries and veins obstructions.
Summary of the invention
The object of this invention is to provide a kind of medicine of promoting blood circulation and stopping pain, this medicine expelling wind and removing dampness, promoting blood circulation and detoxication, anti-inflammation, reunion of fractured tendons and bones, promoting blood circulation and stopping pain, can play the object for the treatment of both the principal and secondary aspects of a disease to the treatment of miscellaneous fracture, traumatic injury, rheumatic ostalgia, arthralgia.
Technical scheme of the present invention is as follows:
A Chinese medicine composition for promoting blood circulation and stopping pain, comprises the raw material of following weight fraction: 6～20 parts of Phlomis mongolica Turcz., 18～30 parts of cacumen et folium sabinae vulgaris, 20～40 parts of Semen Sojae Preparatum grass, 9～25 parts of mud Artemisias, 3～15 parts of Radix Apioris Fortunei (Radix Lespedezae Buergeri)s, 15～40 parts of Radix daphnes odoraes, 6～15 parts of Radix Aerio Fici Microcarpae, 20～50 parts of Radix Pittospori Glabratis, 18～60 parts of Herba Ardisiae Maculosaes, 9～15 parts of Caulis et folium stauntoniaes, 12～26 parts of campanilla grass, 12～36 parts of Ramulus Persicae, 3～18 parts of Medulla Trevesiae palmataes, 48～110 parts of auxiliary agents.
Described auxiliary agent is made up of the raw material of following weight portion: 12～30 parts of Radix cardamines leucanthae, 18～40 parts of Herba lamii barbatis, 3～6 parts of Flos Genkwas, 15～34 parts of Radix Luffae.
The preparation method of described auxiliary agent is: take Radix cardamines leucanthae, Herba lamii barbati, Flos Genkwa, Radix Luffae by proportioning; Flos Genkwa cleans up, and mixes thoroughly with vinegar, runs through completely, puts in pot and fries to vinegar exhaustion with slow fire, is micro-yellow, takes out, and dries, and obtains stir-baked FLOS GENKWA with vinegar for subsequent use; Radix Luffae charred medicinal herb with its property retained, burns to outside burned black, and the inside is sallow, makes the carbonization of medical surfaces part, and nexine part can also be tasted original abnormal smells from the patient; The Radix Luffae of the stir-baked FLOS GENKWA with vinegar making, charred medicinal herb with its property retained, Radix cardamines leucanthae, Herba lamii barbati are ground into powder together, and 150～220 orders sieve, and obtain auxiliary agent.
Further, in the preparation process of described stir-baked FLOS GENKWA with vinegar, the consumption of vinegar is 1/4 of Flos Genkwa weight.
A preparation method for the Chinese medicine composition of promoting blood circulation and stopping pain, comprises the following steps:
(1) take Phlomis mongolica Turcz., cacumen et folium sabinae vulgaris, Radix daphnes odorae, Radix Pittospori Glabrati, campanilla grass, Ramulus Persicae, Medulla Trevesiae palmatae by proportioning, all medical materials are rinsed well with mobile tap water, dry, be ground into coarse powder, put into drug-decocting appliance, add the pure water of 8～10 times of amounts, soak 3～10 hours, medical material is fully infiltrated, be beneficial to the fried of medical material effective ingredient; With after the boiled decoction of big fire 10min, then use slow fire instead and decoct 25 minutes, cooling after, filter, obtain filtrate and filtering residue; Filtrate adds ethanol to being 65% containing alcohol amount, carries out cold preservation, precipitation, again filters, and reclaims ethanol, is evaporated to the thick paste that under 50～70 DEG C of conditions, relative density is 1.26～1.38, for subsequent use; Filtering residue is dried, and is again ground into fine powder with pulverizer, and 150～220 orders sieve, and obtain filtering residue powder, for subsequent use;
(2) take Semen Sojae Preparatum grass, mud Artemisia, Radix Apioris Fortunei (Radix Lespedezae Buergeri), Radix Aerio Fici Microcarpae, Herba Ardisiae Maculosae, Caulis et folium stauntoniae by proportioning, all medical materials are rinsed well with mobile tap water, dry, be ground into coarse powder, add the ethanol with respect to 4～7 times of medical material gross weights, reflux, extract, 2～3 times, each 1～2 hour, filter, filtrate merges, and carries out cold preservation, precipitation, again filter, reclaim ethanol, be evaporated to the thick paste that under 50～70 DEG C of conditions, relative density is 1.26～1.38, for subsequent use;
(3) take Radix cardamines leucanthae, Herba lamii barbati, Flos Genkwa, Radix Luffae by proportioning, Flos Genkwa cleans up, and mixes thoroughly with vinegar, and the consumption of vinegar is 1/4 of Flos Genkwa weight, runs through completely, puts in pot and fries to vinegar exhaustion with slow fire, is micro-yellow, takes out, and dries, and obtains stir-baked FLOS GENKWA with vinegar for subsequent use; Radix Luffae charred medicinal herb with its property retained, burns to outside burned black, and the inside is sallow, makes the carbonization of medical surfaces part, and nexine part can also be tasted original abnormal smells from the patient; The Radix Luffae of the stir-baked FLOS GENKWA with vinegar making, charred medicinal herb with its property retained, Radix cardamines leucanthae, Herba lamii barbati are ground into powder together, and 150～220 orders sieve, and obtain auxiliary agent for subsequent use.
(4) by the thick paste of the thick paste of step (1), filtering residue powder, step (2), and the auxiliary agent of step (3) mixes, add the conventional adjuvant of pharmacy to make pharmaceutically acceptable dosage form, obtain the Chinese medicine composition of a kind of promoting blood circulation and stopping pain of the present invention.The conventional adjuvant of described pharmacy comprises magnesium stearate, microcrystalline Cellulose, lactose, pregelatinized Starch, stearic acid, poloxamer, gelatin, glyceryl monostearate, hydrogenated vegetable oil and distilled water.Described dosage form comprises tablet, drop pill.
Further, its determining alcohol of ethanol adding in described step (1) is 75～85%.
Further, its determining alcohol of ethanol adding in described step (2) is 55～65%.
Further, described step (1) is 36～48 hours with (2) middle cold preservation time, and the sedimentation time is 40～60 hours, and filtering is all with vacuum filter, under the condition that is 0.95～1.25MPa, filters in vacuum.Its purity of medicinal liquid through cold preservation processing, precipitation process, again obtaining after filtration treatment is higher, and the effective ingredient content making also higher curative effect is just better.
Further; the preparation method of described tablet is: by the thick paste of the thick paste of step (1), filtering residue powder, step (2); and the auxiliary agent of step (3) mixes; add 0.6～0.7 part of magnesium stearate; add again with respect to the microcrystalline Cellulose of 0.05～0.25 times of the mixture quality obtaining, 0.15～0.35 times of lactose, the pregelatinized Starch of 0.2～0.3 times; mix homogeneously; granulate with granulator; drying machine is dry; tabletting; every weight is 2.0g, obtains tablet.
Further, the preparation method of described drop pill is: be to dissolve into stearic acid liquid under the condition of 75 DEG C in temperature by stearic acid; The part by weight of poloxamer, gelatin, glyceryl monostearate, hydrogenated vegetable oil and distilled water being pressed to 2:4:1:300:500 mixes, and heating, maintains the temperature at 75 DEG C, obtains distilled water mixed liquor; Stearic acid liquid is slowly joined in distilled water mixed liquor according to the part by weight of 1:100, stir simultaneously, obtain substrate after cooling; By the thick paste of the thick paste of step (1), filtering residue powder, step (2), and the auxiliary agent of step (3) mixes, mixture and substrate are joined in gained substrate in the ratio of 1:1, heating and melting mixes, and constantly grind, obtain sticky paste, granulate, after dry, obtain drop pill.
The character of the present invention's each medical material used is as follows:
Phlomis mongolica Turcz.: [nature and flavor] sweet in the mouth; Bitter; Warm in nature.[function cures mainly] expelling wind and removing dampness; Promoting blood circulation and stopping pain.Main air wet arthritis; Flu; Traumatic injury; The body heat of shooting without hitting the target.Cacumen et folium sabinae vulgaris: [nature and flavor] hardship; Pungent; Property is put down.[function cures mainly] expelling wind and removing dampness; Promoting blood circulation and stopping pain.Main air arthralgia due to cold pain; Skin pruritus; Headache; Cough.Radix cardamines leucanthae: [nature and flavor] are pungent; Sweet; Flat.[function cures mainly] preventing phlegm from forming and stopping coughing; Promoting blood circulation and stopping pain.Main pertussis; Chronic bronchitis; Have through uncomfortable; Traumatic injury.Semen Sojae Preparatum grass: [nature and flavor] are light, are slightly cold.[function cures mainly] relaxing muscles and tendons to promote blood circulation; Heat-clearing and toxic substances removing, expelling wind and removing dampness; Preventing phlegm from forming and stopping coughing.Main bones and muscles pain due to rheumatism; Traumatic injury; Furuncle toxic swelling; Pharyngolaryngitis; Stomatitis; Dysentery; Watery diarrhea; Dyspepsia does not disappear; Infantile malnutrition; Epersalgia cough; Asthma; Pertussis.Mud Artemisia: [nature and flavor] are pungent; Slightly warm in nature.[function cures mainly] promoting blood circulation and stopping pain.Main treating swelling and pain by traumatic injury.Radix Apioris Fortunei (Radix Lespedezae Buergeri): [nature and flavor] micro-hardship, flat.[function cures mainly] heat-clearing and toxic substances removing, dispelling pathogenic wind and eliminating phlegm, promoting blood circulation and stopping pain.Cure mainly: diphtheria, children with high fever induced convulsions, dysentery, hepatitis.Venom is controlled in external, tonsillitis, tuberculous lymphadenitis, cervicitis, cellulitis, traumatic injury.Radix daphnes odorae: [nature and flavor] acrid in the mouth; Sweet; Property is put down.[function cures mainly] removing toxic substances; Promoting blood circulation and stopping pain.Main laryngopharynx swelling and pain; Gastric abscess; Traumatic injury; Venom.Radix Aerio Fici Microcarpae: [nature and flavor] bitterness, flat.[function cures mainly] expelling wind and clearing away heat, promoting blood circulation and detoxication.Control influenza, pertussis, measles without adequate eruption, tonsillitis, eye conjunctivitis, eruptive disease stomachache, rheumatic ostalgia, epistaxis, stranguria with blood, traumatic injury." Luchuan book on Chinese herbal medicine ": synthetism, detumescence, pain relieving.Control traumatic injury, break the muscle folding bone.Radix Pittospori Glabrati: [nature and flavor] sweetness and bitterness is pungent, cool.[function cures mainly] tonifying the lung kidney, wind-damp dispelling, promoting blood circulation to remove obstruction in the collateral.Control asthenia and breath with cough, seminal emission premature ejaculation, insomnia, dizziness, hypertension, rheumatic arthralgia, infantile paralysis.Herba lamii barbati: [nature and flavor] are sweet, pungent is flat.[function cures mainly] controls lung-heat hemoptysis, stranguria with blood, leucorrhea, menoxenia, deficiency-heat syndrome in children, traumatic injury, toxic swelling.Cooling blood for hemostasis; Promoting blood circulation and stopping pain; Inducing diuresis and reducing edema.Main lung-heat hemoptysis; Stranguria with blood.Flos Genkwa: [nature and flavor] flower: bitter, acrid, cold; Poisonous.Root bark: pungent, bitter, flat.Poisonous.[function cures mainly] flower: removing fluid-retention by purgation, removing toxic substances parasite killing.For edema distension, breast abdomen hydrops, phlegm retention is gathered, and QI rising in reverse order is breathed with cough, difficulty in urination and defecation; External treatment scabies tinea alba, chilblain.Root bark: subduing swelling and detoxicating, promoting blood circulation and stopping pain.For acute mastitis, carbuncle furuncle and phyma poison, tuberculous lymphadenitis, ascites, rheumatalgia, toothache, traumatic injury.Herba Ardisiae Maculosae: [nature and flavor] fiber crops are bitter, temperature.[function cures mainly] promoting blood circulation and stopping pain; Clearing throat.Main traumatic injury; Fracture; Rheumatic arthralgia; Diphtheria; Laryngopharynx swelling and pain; Gastric ulcer.Caulis et folium stauntoniae: [nature and flavor] are sweet; Warm in nature.[function cures mainly] dispels the wind and network; Promoting blood circulation and stopping pain; Inducing diuresis to remove edema.Main air pain of dampness syndrome; The pain of stomach, intestinal and biliary diseases; Trigeminal neuralgia; Traumatic injury; Dysmenorrhea; Dysuria; Edema.Radix Luffae: [nature and flavor] are sweet is flat.[function cures mainly] promoting blood circulation to remove obstruction in the collateral; Heat-clearing and toxic substances removing.Main migraine; Lumbago; Arthromyodynia; Mastitis; Rhinitis; Sinusitis; Acute throat trouble swells and ache; Discharging fresh blood stool; Anal fistula.Campanilla grass: [nature and flavor] bitter in the mouth; Micro-pungent; Cool in nature.[function cures mainly] clearing away heart-fire; Promoting blood circulation to remove obstruction in the collateral.Main aphtha of the mouth and tongue; Rheumatic arthralgia; Traumatic injury.Ramulus Persicae: [nature and flavor] hardship; Flat.[function cures mainly] promoting blood circulation to remove obstruction in the collateral, removing toxic substances, parasite killing.Main cardiac and abdominal pain, rheumatic arthritis, lumbago, traumatic injury, skin ulcer tinea.Medulla Trevesiae palmatae: [nature and flavor] mildly bitter flavor; Property is put down.[function cures mainly] blood-activating analgetic.Main traumatic injury; Wound; Lumbago.
Beneficial effect of the present invention is embodied in: the Chinese medicine composition of a kind of promoting blood circulation and stopping pain of the present invention, compatibility of drugs rationally, select medicine to forbid, all medicines share, bring out the best in each other, active constituent content is high, better stability of preparation.Can pass through expelling wind and removing dampness, promoting blood circulation and detoxication, anti-inflammation, reunion of fractured tendons and bones, promoting blood circulation and stopping pain, to disease internal and external applications such as miscellaneous fracture, traumatic injury, rheumatic ostalgia, arthralgias, evident in efficacy, and easy to use, with low cost, have no side effect.
Detailed description of the invention
Embodiment 1:
A Chinese medicine composition for promoting blood circulation and stopping pain, comprises the raw material of following weight fraction: 6 parts of Phlomis mongolica Turcz., 18 parts of cacumen et folium sabinae vulgaris, 20 parts of Semen Sojae Preparatum grass, 9 parts of mud Artemisias, 3 parts of Radix Apioris Fortunei (Radix Lespedezae Buergeri)s, 15 parts of Radix daphnes odoraes, 6 parts of Radix Aerio Fici Microcarpae, 20 parts of Radix Pittospori Glabratis, 18 parts of Herba Ardisiae Maculosaes, 9 parts of Caulis et folium stauntoniaes, 12 parts of campanilla grass, 12 parts of Ramulus Persicae, 3 parts of Medulla Trevesiae palmataes, 48 parts of auxiliary agents.
Described auxiliary agent is made up of the raw material of following weight portion: 12 parts of Radix cardamines leucanthae, 18 parts of Herba lamii barbatis, 3 parts of Flos Genkwas, 15 parts of Radix Luffae.
The preparation method of described auxiliary agent is: take Radix cardamines leucanthae, Herba lamii barbati, Flos Genkwa, Radix Luffae by proportioning; Flos Genkwa cleans up, and mixes thoroughly with vinegar, and the consumption of vinegar is 1/4 of Flos Genkwa weight, runs through completely, puts in pot and fries to vinegar exhaustion with slow fire, is micro-yellow, takes out, and dries, and obtains stir-baked FLOS GENKWA with vinegar for subsequent use; Radix Luffae charred medicinal herb with its property retained, burns to outside burned black, and the inside is sallow, makes the carbonization of medical surfaces part, and nexine part can also be tasted original abnormal smells from the patient; The Radix Luffae of the stir-baked FLOS GENKWA with vinegar making, charred medicinal herb with its property retained, Radix cardamines leucanthae, Herba lamii barbati are ground into powder together, and 150 orders sieve, and obtain auxiliary agent.
The preparation method of the tablet of the Chinese medicine composition of described promoting blood circulation and stopping pain is:
(1) take Phlomis mongolica Turcz., cacumen et folium sabinae vulgaris, Radix daphnes odorae, Radix Pittospori Glabrati, campanilla grass, Ramulus Persicae, Medulla Trevesiae palmatae by proportioning, all medical materials are rinsed well with mobile tap water, dry, be ground into coarse powder, put into drug-decocting appliance, add the pure water of 8 times of amounts, soak 3 hours, medical material is fully infiltrated, be beneficial to the fried of medical material effective ingredient; With after the boiled decoction of big fire 10min, then use slow fire instead and decoct 25 minutes, cooling after, filter, obtain filtrate and filtering residue; Filtrate adds ethanol to being 65% containing alcohol amount, and its determining alcohol of the ethanol adding is 75%, carries out cold preservation, precipitation, again filters, and reclaims ethanol, is evaporated to the thick paste that under 50 DEG C of conditions, relative density is 1.26, for subsequent use; Filtering residue is dried, and is again ground into fine powder with pulverizer, and 150 orders sieve, and obtain filtering residue powder, for subsequent use; Wherein, cold preservation time is 36 hours, and the sedimentation time is 40 hours, and filtration is with vacuum filter, under the condition that is 0.95MPa, filters in vacuum.Its purity of medicinal liquid through cold preservation processing, precipitation process, again obtaining after filtration treatment is higher, and the effective ingredient content making also higher curative effect is just better.
(2) take Semen Sojae Preparatum grass, mud Artemisia, Radix Apioris Fortunei (Radix Lespedezae Buergeri), Radix Aerio Fici Microcarpae, Herba Ardisiae Maculosae, Caulis et folium stauntoniae by proportioning, all medical materials are rinsed well with mobile tap water, dry, be ground into coarse powder, add the ethanol with respect to 4 times of medical material gross weights, its determining alcohol of the ethanol adding is 55%, reflux, extract, 2 times, each 1 hour, filters, filtrate merges, carry out cold preservation, precipitation, again filter, reclaim ethanol, be evaporated to the thick paste that under 50 DEG C of conditions, relative density is 1.26, for subsequent use; Wherein, cold preservation time is 36 hours, and the sedimentation time is 40 hours, and filtration is with vacuum filter, under the condition that is 0.95MPa, filters in vacuum.Its purity of medicinal liquid through cold preservation processing, precipitation process, again obtaining after filtration treatment is higher, and the effective ingredient content making also higher curative effect is just better.
(3) take Radix cardamines leucanthae, Herba lamii barbati, Flos Genkwa, Radix Luffae by proportioning, Flos Genkwa cleans up, and mixes thoroughly with vinegar, and the consumption of vinegar is 1/4 of Flos Genkwa weight, runs through completely, puts in pot and fries to vinegar exhaustion with slow fire, is micro-yellow, takes out, and dries, and obtains stir-baked FLOS GENKWA with vinegar for subsequent use; Radix Luffae charred medicinal herb with its property retained, burns to outside burned black, and the inside is sallow, makes the carbonization of medical surfaces part, and nexine part can also be tasted original abnormal smells from the patient; The Radix Luffae of the stir-baked FLOS GENKWA with vinegar making, charred medicinal herb with its property retained, Radix cardamines leucanthae, Herba lamii barbati are ground into powder together, and 150 orders sieve, and obtain auxiliary agent for subsequent use.
(4) by the thick paste of the thick paste of step (1), filtering residue powder, step (2); and the auxiliary agent of step (3) mixes; add 0.6 part of magnesium stearate; add with respect to the microcrystalline Cellulose of 0.05 times of the mixture quality obtaining, 0.15 times of lactose, the pregelatinized Starch of 0.2～0.3 times, mix homogeneously, granulates with granulator again; drying machine is dry; tabletting, every weight is 2.0g, obtains tablet.
Embodiment 2:
A Chinese medicine composition for promoting blood circulation and stopping pain, comprises the raw material of following weight fraction: 13 parts of Phlomis mongolica Turcz., 24 parts of cacumen et folium sabinae vulgaris, 30 parts of Semen Sojae Preparatum grass, 17 parts of mud Artemisias, 9 parts of Radix Apioris Fortunei (Radix Lespedezae Buergeri)s, 27 parts of Radix daphnes odoraes, 10 parts of Radix Aerio Fici Microcarpae, 35 parts of Radix Pittospori Glabratis, 39 parts of Herba Ardisiae Maculosaes, 12 parts of Caulis et folium stauntoniaes, 19 parts of campanilla grass, 24 parts of Ramulus Persicae, 10 parts of Medulla Trevesiae palmataes, 79 parts of auxiliary agents.
Described auxiliary agent is made up of the raw material of following weight portion: 21 parts of Radix cardamines leucanthae, 29 parts of Herba lamii barbatis, 4.5 parts of Flos Genkwas, 24 parts of Radix Luffae.
The preparation method of described auxiliary agent is: take Radix cardamines leucanthae, Herba lamii barbati, Flos Genkwa, Radix Luffae by proportioning; Flos Genkwa cleans up, and mixes thoroughly with vinegar, and the consumption of vinegar is 1/4 of Flos Genkwa weight, runs through completely, puts in pot and fries to vinegar exhaustion with slow fire, is micro-yellow, takes out, and dries, and obtains stir-baked FLOS GENKWA with vinegar for subsequent use; Radix Luffae charred medicinal herb with its property retained, burns to outside burned black, and the inside is sallow, makes the carbonization of medical surfaces part, and nexine part can also be tasted original abnormal smells from the patient; The Radix Luffae of the stir-baked FLOS GENKWA with vinegar making, charred medicinal herb with its property retained, Radix cardamines leucanthae, Herba lamii barbati are ground into powder together, and 185 orders sieve, and obtain auxiliary agent.
The preparation method of the tablet of the Chinese medicine composition of described promoting blood circulation and stopping pain is:
(1) take Phlomis mongolica Turcz., cacumen et folium sabinae vulgaris, Radix daphnes odorae, Radix Pittospori Glabrati, campanilla grass, Ramulus Persicae, Medulla Trevesiae palmatae by proportioning, all medical materials are rinsed well with mobile tap water, dry, be ground into coarse powder, put into drug-decocting appliance, add the pure water of 9 times of amounts, soak 6.5 hours, medical material is fully infiltrated, be beneficial to the fried of medical material effective ingredient; With after the boiled decoction of big fire 10min, then use slow fire instead and decoct 25 minutes, cooling after, filter, obtain filtrate and filtering residue; Filtrate adds ethanol to being 65% containing alcohol amount, and its determining alcohol of the ethanol adding is 80%, carries out cold preservation, precipitation, again filters, and reclaims ethanol, is evaporated to the thick paste that under 60 DEG C of conditions, relative density is 1.32, for subsequent use; Filtering residue is dried, and is again ground into fine powder with pulverizer, and 185 orders sieve, and obtain filtering residue powder, for subsequent use; Wherein, cold preservation time is 42 hours, and the sedimentation time is 50 hours, and filtration is with vacuum filter, under the condition that is 1.10MPa, filters in vacuum.Its purity of medicinal liquid through cold preservation processing, precipitation process, again obtaining after filtration treatment is higher, and the effective ingredient content making also higher curative effect is just better.
(2) take Semen Sojae Preparatum grass, mud Artemisia, Radix Apioris Fortunei (Radix Lespedezae Buergeri), Radix Aerio Fici Microcarpae, Herba Ardisiae Maculosae, Caulis et folium stauntoniae by proportioning, all medical materials are rinsed well with mobile tap water, dry, be ground into coarse powder, add the ethanol with respect to 5.5 times of medical material gross weights, its determining alcohol of the ethanol adding is 60%, reflux, extract, 2 times, each 1.5 hours, filters, filtrate merges, carry out cold preservation, precipitation, again filter, reclaim ethanol, be evaporated to the thick paste that under 60 DEG C of conditions, relative density is 1.32, for subsequent use; Wherein, cold preservation time is 42 hours, and the sedimentation time is 50 hours, and filtration is with vacuum filter, under the condition that is 1.10MPa, filters in vacuum.Its purity of medicinal liquid through cold preservation processing, precipitation process, again obtaining after filtration treatment is higher, and the effective ingredient content making also higher curative effect is just better.
(3) take Radix cardamines leucanthae, Herba lamii barbati, Flos Genkwa, Radix Luffae by proportioning, Flos Genkwa cleans up, and mixes thoroughly with vinegar, and the consumption of vinegar is 1/4 of Flos Genkwa weight, runs through completely, puts in pot and fries to vinegar exhaustion with slow fire, is micro-yellow, takes out, and dries, and obtains stir-baked FLOS GENKWA with vinegar for subsequent use; Radix Luffae charred medicinal herb with its property retained, burns to outside burned black, and the inside is sallow, makes the carbonization of medical surfaces part, and nexine part can also be tasted original abnormal smells from the patient; The Radix Luffae of the stir-baked FLOS GENKWA with vinegar making, charred medicinal herb with its property retained, Radix cardamines leucanthae, Herba lamii barbati are ground into powder together, and 185 orders sieve, and obtain auxiliary agent for subsequent use.
(4) by the thick paste of the thick paste of step (1), filtering residue powder, step (2); and the auxiliary agent of step (3) mixes; add 0.65 part of magnesium stearate; add with respect to the microcrystalline Cellulose of 0.15 times of the mixture quality obtaining, 0.25 times of lactose, the pregelatinized Starch of 0.25 times, mix homogeneously, granulates with granulator again; drying machine is dry; tabletting, every weight is 2.0g, obtains tablet.
Embodiment 3:
A Chinese medicine composition for promoting blood circulation and stopping pain, comprises the raw material of following weight fraction: 20 parts of Phlomis mongolica Turcz., 30 parts of cacumen et folium sabinae vulgaris, 40 parts of Semen Sojae Preparatum grass, 25 parts of mud Artemisias, 15 parts of Radix Apioris Fortunei (Radix Lespedezae Buergeri)s, 40 parts of Radix daphnes odoraes, 15 parts of Radix Aerio Fici Microcarpae, 50 parts of Radix Pittospori Glabratis, 60 parts of Herba Ardisiae Maculosaes, 15 parts of Caulis et folium stauntoniaes, 26 parts of campanilla grass, 36 parts of Ramulus Persicae, 18 parts of Medulla Trevesiae palmataes, 110 parts of auxiliary agents.
Described auxiliary agent is made up of the raw material of following weight portion: 30 parts of Radix cardamines leucanthae, 40 parts of Herba lamii barbatis, 6 parts of Flos Genkwas, 34 parts of Radix Luffae.
The preparation method of described auxiliary agent is: take Radix cardamines leucanthae, Herba lamii barbati, Flos Genkwa, Radix Luffae by proportioning; Flos Genkwa cleans up, and mixes thoroughly with vinegar, and the consumption of vinegar is 1/4 of Flos Genkwa weight, runs through completely, puts in pot and fries to vinegar exhaustion with slow fire, is micro-yellow, takes out, and dries, and obtains stir-baked FLOS GENKWA with vinegar for subsequent use; Radix Luffae charred medicinal herb with its property retained, burns to outside burned black, and the inside is sallow, makes the carbonization of medical surfaces part, and nexine part can also be tasted original abnormal smells from the patient; The Radix Luffae of the stir-baked FLOS GENKWA with vinegar making, charred medicinal herb with its property retained, Radix cardamines leucanthae, Herba lamii barbati are ground into powder together, and 220 orders sieve, and obtain auxiliary agent.
The preparation method of the drop pill of the Chinese medicine composition of described promoting blood circulation and stopping pain is:
(1) take Phlomis mongolica Turcz., cacumen et folium sabinae vulgaris, Radix daphnes odorae, Radix Pittospori Glabrati, campanilla grass, Ramulus Persicae, Medulla Trevesiae palmatae by proportioning, all medical materials are rinsed well with mobile tap water, dry, be ground into coarse powder, put into drug-decocting appliance, add the pure water of 10 times of amounts, soak 10 hours, medical material is fully infiltrated, be beneficial to the fried of medical material effective ingredient; With after the boiled decoction of big fire 10min, then use slow fire instead and decoct 25 minutes, cooling after, filter, obtain filtrate and filtering residue; Filtrate adds ethanol to being 65% containing alcohol amount, and its determining alcohol of the ethanol adding is 85%, carries out cold preservation, precipitation, again filters, and reclaims ethanol, is evaporated to the thick paste that under 70 DEG C of conditions, relative density is 1.38, for subsequent use; Filtering residue is dried, and is again ground into fine powder with pulverizer, and 220 orders sieve, and obtain filtering residue powder, for subsequent use; Wherein, cold preservation time is 48 hours, and the sedimentation time is 60 hours, and filtration is with vacuum filter, under the condition that is 1.25MPa, filters in vacuum.Its purity of medicinal liquid through cold preservation processing, precipitation process, again obtaining after filtration treatment is higher, and the effective ingredient content making also higher curative effect is just better.
(2) take Semen Sojae Preparatum grass, mud Artemisia, Radix Apioris Fortunei (Radix Lespedezae Buergeri), Radix Aerio Fici Microcarpae, Herba Ardisiae Maculosae, Caulis et folium stauntoniae by proportioning, all medical materials are rinsed well with mobile tap water, dry, be ground into coarse powder, add the ethanol with respect to 4～7 times of medical material gross weights, its determining alcohol of the ethanol adding is 65%, reflux, extract, 3 times, each 2 hours, filters, filtrate merges, carry out cold preservation, precipitation, again filter, reclaim ethanol, be evaporated to the thick paste that under 70 DEG C of conditions, relative density is 1.38, for subsequent use; Wherein, cold preservation time is 36～48 hours, and the sedimentation time is 60 hours, and filtration is with vacuum filter, under the condition that is 1.25MPa, filters in vacuum.Its purity of medicinal liquid through cold preservation processing, precipitation process, again obtaining after filtration treatment is higher, and the effective ingredient content making also higher curative effect is just better.
(3) take Radix cardamines leucanthae, Herba lamii barbati, Flos Genkwa, Radix Luffae by proportioning, Flos Genkwa cleans up, and mixes thoroughly with vinegar, and the consumption of vinegar is 1/4 of Flos Genkwa weight, runs through completely, puts in pot and fries to vinegar exhaustion with slow fire, is micro-yellow, takes out, and dries, and obtains stir-baked FLOS GENKWA with vinegar for subsequent use; Radix Luffae charred medicinal herb with its property retained, burns to outside burned black, and the inside is sallow, makes the carbonization of medical surfaces part, and nexine part can also be tasted original abnormal smells from the patient; The Radix Luffae of the stir-baked FLOS GENKWA with vinegar making, charred medicinal herb with its property retained, Radix cardamines leucanthae, Herba lamii barbati are ground into powder together, and 220 orders sieve, and obtain auxiliary agent for subsequent use.
(4) be to dissolve into stearic acid liquid under the condition of 75 DEG C in temperature by stearic acid; The part by weight of poloxamer, gelatin, glyceryl monostearate, hydrogenated vegetable oil and distilled water being pressed to 2:4:1:300:500 mixes, and heating, maintains the temperature at 75 DEG C, obtains distilled water mixed liquor; Stearic acid liquid is slowly joined in distilled water mixed liquor according to the part by weight of 1:100, stir simultaneously, obtain substrate after cooling; By the thick paste of the thick paste of step (1), filtering residue powder, step (2), and the auxiliary agent of step (3) mixes, mixture and substrate are joined in gained substrate in the ratio of 1:1, heating and melting mixes, and constantly grind, obtain sticky paste, granulate, after dry, obtain drop pill.
Clinical typical case:
1. patient Yang: man, 14 years old, because of injured with people's shank of having a fist fight, fracture, sharp ache, local swelling rapidly, disorder of limb ' s activity.Take tablet prepared by the embodiment of the present invention 1, take 1 day pain and just alleviate, take congestive edema after 3 days and start to disappear, after 10 days, congestive edema disappears completely, and pain disappears, and after 15 days, limb activity freely, is cured substantially.
Patient Wei so-and-so: man, 48 years old, because of industrial injury, left foot was injured by a crashing object, the livid purple color ecchymosis of instep, swelling, twinge, owing to failing treatment in time, cause injury scleroma, indistinctly pain, the inconvenience of walking, does not heal for a long time, finally becomes chronic injury.Take tablet prepared by the embodiment of the present invention 2, take pain after 3 days and eliminate gradually, take and harden and leave afterwards for 6 days, movable sensitive after 10 days, substantially cure.
3. patient Lin: female, 74 years old, suffer from rheumatic osteopathia, arthralgia, stiff, enlargement, surrounding skin heating, has the swollen or feeling of numbness of acid sometimes.Take drop pill prepared by the embodiment of the present invention 3, after 3 days, pain just alleviates, and after 15 days, starts detumescence, continues to take after one month and cures.
Finally it should be noted that: above embodiment only, in order to technical scheme of the present invention to be described, is not intended to limit; Although the present invention is had been described in detail with reference to previous embodiment, those of ordinary skill in the art is to be understood that: its technical scheme that still can record previous embodiment is modified, or part technical characterictic is wherein equal to replacement; And these amendments or replacement do not make the essence of appropriate technical solution depart from the spirit and scope of embodiment of the present invention technical scheme.
Claims (8)
1. a Chinese medicine composition for promoting blood circulation and stopping pain, is characterized in that comprising the raw material of following weight fraction: 6～20 parts of Phlomis mongolica Turcz., 18～30 parts of cacumen et folium sabinae vulgaris, 20～40 parts of Semen Sojae Preparatum grass, 9～25 parts of mud Artemisias, 3～15 parts of Radix Apioris Fortunei (Radix Lespedezae Buergeri)s, 15～40 parts of Radix daphnes odoraes, 6～15 parts of Radix Aerio Fici Microcarpae, 20～50 parts of Radix Pittospori Glabratis, 18～60 parts of Herba Ardisiae Maculosaes, 9～15 parts of Caulis et folium stauntoniaes, 12～26 parts of campanilla grass, 12～36 parts of Ramulus Persicae, 3～18 parts of Medulla Trevesiae palmataes, 48～110 parts of auxiliary agents; Described auxiliary agent is made up of the raw material of following weight portion: 12～30 parts of Radix cardamines leucanthae, 18～40 parts of Herba lamii barbatis, 3～6 parts of Flos Genkwas, 15～34 parts of Radix Luffae; The preparation method of described auxiliary agent is: Flos Genkwa cleans up, and mixes thoroughly with vinegar, runs through completely, puts in pot and fries to vinegar exhaustion with slow fire, is micro-yellow, takes out, and dries, and obtains stir-baked FLOS GENKWA with vinegar for subsequent use; Radix Luffae charred medicinal herb with its property retained, burns to outside burned black, and the inside is sallow; The Radix Luffae of the stir-baked FLOS GENKWA with vinegar making, charred medicinal herb with its property retained, Radix cardamines leucanthae, Herba lamii barbati are ground into powder together, obtained auxiliary agent.
2. the Chinese medicine composition of a kind of promoting blood circulation and stopping pain according to claim 1, is characterized in that in the preparation process of described stir-baked FLOS GENKWA with vinegar, the consumption of vinegar is 1/4 of Flos Genkwa weight.
3. according to the preparation method of the Chinese medicine composition of a kind of promoting blood circulation and stopping pain described in claim 1～2, it is characterized in that comprising the following steps:
(1) take Phlomis mongolica Turcz., cacumen et folium sabinae vulgaris, Radix daphnes odorae, Radix Pittospori Glabrati, campanilla grass, Ramulus Persicae, Medulla Trevesiae palmatae by proportioning, all pulverizing medicinal materials become coarse powder, put into drug-decocting appliance, add the pure water of 8～10 times of amounts, soak 3～10 hours, medical material is fully infiltrated, be beneficial to the fried of medical material effective ingredient; With after the boiled decoction of big fire 10min, then use slow fire instead and decoct 25 minutes, cooling after, filter, obtain filtrate and filtering residue; Filtrate adds ethanol to being 65% containing alcohol amount, carries out cold preservation, precipitation, again filters, and reclaims ethanol, is concentrated into the thick paste that under 50～70 DEG C of conditions, relative density is 1.26～1.38, for subsequent use; Filtering residue is dried, and pulverizes, and 150～220 orders sieve, and obtain filtering residue powder, for subsequent use;
(2) take Semen Sojae Preparatum grass, mud Artemisia, Radix Apioris Fortunei (Radix Lespedezae Buergeri), Radix Aerio Fici Microcarpae, Herba Ardisiae Maculosae, Caulis et folium stauntoniae by proportioning, all pulverizing medicinal materials become coarse powder, add the ethanol with respect to 4～7 times of medical material gross weights, reflux, extract, 2～3 times, each 1～2 hour, filter, filtrate merges, and carries out cold preservation, precipitation, again filter, reclaim ethanol, be concentrated into the thick paste that under 50～70 DEG C of conditions, relative density is 1.26～1.38, for subsequent use;
(3) take Radix cardamines leucanthae, Herba lamii barbati, Flos Genkwa, Radix Luffae by proportioning, Flos Genkwa cleans up, and mixes thoroughly with vinegar, and the consumption of vinegar is 1/4 of Flos Genkwa weight, runs through completely, puts in pot and fries to vinegar exhaustion with slow fire, is micro-yellow, takes out, and dries, and obtains stir-baked FLOS GENKWA with vinegar for subsequent use; Radix Luffae charred medicinal herb with its property retained, burns to outside burned black, and the inside is sallow; The Radix Luffae of the stir-baked FLOS GENKWA with vinegar making, charred medicinal herb with its property retained, Radix cardamines leucanthae, Herba lamii barbati are ground into powder together, and 150～220 orders sieve, and obtain auxiliary agent for subsequent use.
(4) by the thick paste of the thick paste of step (1), filtering residue powder, step (2), and the auxiliary agent of step (3) mixes, add the conventional adjuvant of pharmacy to make pharmaceutically acceptable dosage form, obtain the Chinese medicine composition of a kind of promoting blood circulation and stopping pain of the present invention.Described dosage form comprises tablet, drop pill.
4. the preparation method of the Chinese medicine composition of a kind of promoting blood circulation and stopping pain according to claim 3, is characterized in that its determining alcohol of ethanol adding in described step (1) is 75～85%.
5. the preparation method of the Chinese medicine composition of a kind of promoting blood circulation and stopping pain according to claim 3, is characterized in that its determining alcohol of ethanol adding in described step (2) is 55～65%.
6. the preparation method of the Chinese medicine composition of a kind of promoting blood circulation and stopping pain according to claim 3, it is characterized in that the middle cold preservation time in described step (1) and (2) is 36～48 hours, sedimentation time is 40～60 hours, filtering is all with vacuum filter, under the condition that is 0.95～1.25MPa, filters in vacuum.
7. the preparation method of the Chinese medicine composition of a kind of promoting blood circulation and stopping pain according to claim 3, the preparation method that it is characterized in that described tablet is: by the thick paste of the thick paste of step (1), filtering residue powder, step (2), and the auxiliary agent of step (3) mixes, add 0.6～0.7 part of magnesium stearate, add again with respect to the microcrystalline Cellulose of 0.05～0.25 times of the mixture quality obtaining, 0.15～0.35 times of lactose, the pregelatinized Starch of 0.2～0.3 times, mix homogeneously, granulate, dry, tabletting, every weight is 2.0g, obtains tablet.
8. the preparation method of the Chinese medicine composition of a kind of promoting blood circulation and stopping pain according to claim 3, is characterized in that the preparation method of described drop pill is: be to dissolve into stearic acid liquid under the condition of 75 DEG C in temperature by stearic acid; The part by weight of poloxamer, gelatin, glyceryl monostearate, hydrogenated vegetable oil and distilled water being pressed to 2:4:1:300:500 mixes, and heating, maintains the temperature at 75 DEG C, obtains distilled water mixed liquor; Stearic acid liquid is slowly joined in distilled water mixed liquor according to the part by weight of 1:100, stir coolingly simultaneously, obtain substrate; By the thick paste of the thick paste of step (1), filtering residue powder, step (2), and the mixing of the auxiliary agent of step (3), join in gained substrate in the ratio of 1:1, heating and melting mixes, and constantly grinds, and obtains sticky paste, granulate, after being dried, obtain drop pill.
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