CN104162294A - Micro bubble remover and preparation method thereof - Google Patents
Micro bubble remover and preparation method thereof Download PDFInfo
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- CN104162294A CN104162294A CN201410349091.XA CN201410349091A CN104162294A CN 104162294 A CN104162294 A CN 104162294A CN 201410349091 A CN201410349091 A CN 201410349091A CN 104162294 A CN104162294 A CN 104162294A
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Abstract
The invention discloses a micro bubble remover, which is characterized by being composed of the following components in parts by weight: 5 to 15 parts of white carbon black, 70 to 90 parts of silicone oil, 5 to 15 parts of silicone resin, and 5 to 15 parts of dispersant. At the same time, the invention further discloses a preparation method of the micro bubble remover. The micro bubble remover has the advantages of little using amount and long lasting effect, can form a membrane on the oil surface after removing the micro bubbles to insulate the oil from the air, and thus has a certain protective effect on oil products. At the same time, the preparation method is scientific and consumes little energy, and no impurity, which can affect the quality of oil products, is brought in during the whole production process.
Description
Technical field
The invention belongs to chemical field, be specifically related to a kind of microvesicle scavenger and preparation method thereof.
Background technology
Air can be long-term with very trickle state exist among oil product, to the production of lubricating oil, store, and use can cause following harm.It is large that lubricating oil and air contact area become, and impels oil product accelerated oxidation rotten, reduction of service life.In addition, airborne moisture enters in the middle of oil product, and the compressibility of lubricating oil is increased, and oil pump decrease in efficiency makes fuel feeding undesired or make oil supply system generation vapour lock, badly damaged oil supply system.Reduce to the lubricating oil being filled with in container, build-up of pressure transmits unstable, and cooling capacity declines, and affects operating efficiency precision and speed.
Show that according to the study the solubility of bubble in oil product is to be inversely proportional to the size of bubble, the less solubility of bubble is larger, will be in oil product in the time being less than below 5 microns exist for a long time, it is very large research topics that these harmful effects to oil quality are eliminated in the existence of removing these microvesicles.
Summary of the invention
Goal of the invention: the object of the invention is to for the deficiencies in the prior art, a kind of microvesicle scavenger is provided.
Another object of the present invention is to provide the preparation method of above-mentioned microvesicle scavenger.
Technical scheme: in order to reach foregoing invention object, the present invention is specifically achieved like this: a kind of microvesicle scavenger, comprises the component of following parts by weight: 5～15 parts of white carbons, 70～90 parts of silicone oil, 5～15 parts of silicones and 5～15 parts of dispersants.
Wherein, the preferred dimethicone of described silicone oil.
Wherein, described dispersant is that AEO (MOA-3) and polyethylene glycol (PEG600) mix 1:2～3 in mass ratio.
Wherein, described silicones is formed by methyltriethoxy silane oxygen alkane hydrolytie polycondensation.
The method of preparing above-mentioned microvesicle scavenger, comprises the following steps:
(1) white carbon is placed on and in Muffle furnace, carries out activation processing, temperature 500～550 degree, constant temperature 3～6 hours, is then down to 400 degree for subsequent use;
(2) silicone oil is put into more than container stirs and be warming up to 150 degree, added white carbon activate, maintenance temperature stirring 3～5 hours;
(3) be cooled to 100 degree, slowly add silicones, control temperature at 100 degree and carry out granularity arrangement 2～4 hours;
(4) add dispersant, cooling while stirring, until discharging after room temperature.
Beneficial effect: compared with conventional art, addition of the present invention is little, and effect is lasting, and can form a skim and completely cut off contacting of air and oil product removing after oil product bubble again oil product surface, oil product storage is played to certain protective effect; Meanwhile, preparation method's science of the present invention, power consumption is few, and whole preparation process is not brought impurity into and is had influence on oil product.
Detailed description of the invention
Embodiment 1:
Getting parts by weight is that 5 parts of white carbons, 70 parts of dimethicones, 15 parts of silicones and 5 parts of dispersants are for subsequent use; White carbon is placed on and in Muffle furnace, carries out activation processing, temperature 500～550 degree, constant temperature 3～6 hours, is then down to 400 degree for subsequent use; Silicone oil is put into more than container stirs and be warming up to 150 degree, added white carbon activate, keep temperature to stir 3～5 hours, be cooled to 100 degree, slowly add silicones, control temperature is at 100 degree and carry out granularity arrangement 2～4 hours; Add dispersant, cooling while stirring, until discharging after room temperature.Wherein, described dispersant is AEO and polyethylene glycol 1:2 mixing in mass ratio; Described silicones is formed by methyltriethoxy silane oxygen alkane hydrolytie polycondensation.
Embodiment 2:
Getting parts by weight is that 8 parts of white carbons, 80 parts of dimethicones, 6 parts of silicones and 8 parts of dispersants are for subsequent use; White carbon is placed on and in Muffle furnace, carries out activation processing, temperature 500～550 degree, constant temperature 3～6 hours, is then down to 400 degree for subsequent use; Silicone oil is put into more than container stirs and be warming up to 150 degree, added white carbon activate, keep temperature to stir 3～5 hours, be cooled to 100 degree, slowly add silicones, control temperature is at 100 degree and carry out granularity arrangement 2～4 hours; Add dispersant, cooling while stirring, until discharging after room temperature.Wherein, described dispersant is AEO and polyethylene glycol 1:3 mixing in mass ratio; Described silicones is formed by methyltriethoxy silane oxygen alkane hydrolytie polycondensation.
Embodiment 3:
Getting parts by weight is that 10 parts of white carbons, 76 parts of dimethicones, 9 parts of silicones and 10 parts of dispersants are for subsequent use; White carbon is placed on and in Muffle furnace, carries out activation processing, temperature 500～550 degree, constant temperature 3～6 hours, is then down to 400 degree for subsequent use; Silicone oil is put into more than container stirs and be warming up to 150 degree, added white carbon activate, keep temperature to stir 3～5 hours, be cooled to 100 degree, slowly add silicones, control temperature is at 100 degree and carry out granularity arrangement 2～4 hours; Add dispersant, cooling while stirring, until discharging after room temperature.Wherein, described dispersant is AEO and polyethylene glycol 1:2 mixing in mass ratio; Described silicones is formed by methyltriethoxy silane oxygen alkane hydrolytie polycondensation.
Embodiment 4:
Getting parts by weight is that 12 parts of white carbons, 85 parts of dimethicones, 10 parts of silicones and 12 parts of dispersants are for subsequent use; White carbon is placed on and in Muffle furnace, carries out activation processing, temperature 500～550 degree, constant temperature 3～6 hours, is then down to 400 degree for subsequent use; Silicone oil is put into more than container stirs and be warming up to 150 degree, added white carbon activate, keep temperature to stir 3～5 hours, be cooled to 100 degree, slowly add silicones, control temperature is at 100 degree and carry out granularity arrangement 2～4 hours; Add dispersant, cooling while stirring, until discharging after room temperature.Wherein, described dispersant is AEO and polyethylene glycol 1:3 mixing in mass ratio; Described silicones is formed by methyltriethoxy silane oxygen alkane hydrolytie polycondensation.
Embodiment 5:
Getting parts by weight is that 15 parts of white carbons, 90 parts of dimethicones, 5 parts of silicones and 5 parts of dispersants are for subsequent use; White carbon is placed on and in Muffle furnace, carries out activation processing, temperature 500～550 degree, constant temperature 3～6 hours, is then down to 400 degree for subsequent use; Silicone oil is put into more than container stirs and be warming up to 150 degree, added white carbon activate, keep temperature to stir 3～5 hours, be cooled to 100 degree, slowly add silicones, control temperature is at 100 degree and carry out granularity arrangement 2～4 hours; Add dispersant, cooling while stirring, until discharging after room temperature.Wherein, described dispersant is AEO and polyethylene glycol 1:3 mixing in mass ratio; Described silicones is formed by methyltriethoxy silane oxygen alkane hydrolytie polycondensation.
Embodiment 6:
Getting parts by weight is that 9 parts of white carbons, 88 parts of dimethicones, 14 parts of silicones and 13 parts of dispersants are for subsequent use; White carbon is placed on and in Muffle furnace, carries out activation processing, temperature 500～550 degree, constant temperature 3～6 hours, is then down to 400 degree for subsequent use; Silicone oil is put into more than container stirs and be warming up to 150 degree, added white carbon activate, keep temperature to stir 3～5 hours, be cooled to 100 degree, slowly add silicones, control temperature is at 100 degree and carry out granularity arrangement 2～4 hours; Add dispersant, cooling while stirring, until discharging after room temperature.Wherein, described dispersant is AEO and polyethylene glycol 1:2 mixing in mass ratio; Described silicones is formed by methyltriethoxy silane oxygen alkane hydrolytie polycondensation.
Embodiment 7:
Getting parts by weight is that 14 parts of white carbons, 86 parts of dimethicones, 6 parts of silicones and 7 parts of dispersants are for subsequent use; White carbon is placed on and in Muffle furnace, carries out activation processing, temperature 500～550 degree, constant temperature 3～6 hours, is then down to 400 degree for subsequent use; Silicone oil is put into more than container stirs and be warming up to 150 degree, added white carbon activate, keep temperature to stir 3～5 hours, be cooled to 100 degree, slowly add silicones, control temperature is at 100 degree and carry out granularity arrangement 2～4 hours; Add dispersant, cooling while stirring, until discharging after room temperature.Wherein, described dispersant is AEO and polyethylene glycol 1:3 mixing in mass ratio; Described silicones is formed by methyltriethoxy silane oxygen alkane hydrolytie polycondensation.
Claims (5)
1. a microvesicle scavenger, is characterized in that, comprises the component of following parts by weight: 5～15 parts of white carbons, 70～90 parts of silicone oil, 5～15 parts of silicones and 5～15 parts of dispersants.
2. microvesicle scavenger according to claim 1, is characterized in that described silicone oil is dimethicone.
3. microvesicle scavenger according to claim 1, is characterized in that, described dispersant is that AEO and polyethylene glycol mix 1:2～3 in mass ratio.
4. microvesicle scavenger according to claim 1, is characterized in that, described silicones is that methyltriethoxy silane oxygen alkane hydrolytie polycondensation forms.
5. the method for preparing the arbitrary described microvesicle scavenger of claim 1～4, is characterized in that, comprises the following steps:
(1) white carbon is placed on and in Muffle furnace, carries out activation processing, temperature 500～550 degree, constant temperature 3～6 hours, is then down to 400 degree for subsequent use;
(2) silicone oil is put into more than container stirs and be warming up to 150 degree, added white carbon activate, maintenance temperature stirring 3～5 hours;
(3) be cooled to 100 degree, slowly add silicones, control temperature at 100 degree and carry out granularity arrangement 2～4 hours;
(4) add dispersant, cooling while stirring, until discharging after room temperature.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410349091.XA CN104162294A (en) | 2014-07-21 | 2014-07-21 | Micro bubble remover and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410349091.XA CN104162294A (en) | 2014-07-21 | 2014-07-21 | Micro bubble remover and preparation method thereof |
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| CN104162294A true CN104162294A (en) | 2014-11-26 |
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| CN201410349091.XA Pending CN104162294A (en) | 2014-07-21 | 2014-07-21 | Micro bubble remover and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105983252A (en) * | 2015-01-29 | 2016-10-05 | 吕锡池 | Plant oil-based defoamer and preparation method of same |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102343165A (en) * | 2011-10-20 | 2012-02-08 | 山东大易化工有限公司 | Efficient silicone defoaming agent |
| CN102350097A (en) * | 2011-07-18 | 2012-02-15 | 南通恒尔特高分子材料科技有限公司 | Silicone-polyether antifoaming agent and preparation method thereof |
| WO2012174405A1 (en) * | 2011-06-17 | 2012-12-20 | Kemira Oyj | Powder defoaming compositions and methods of reducing gas entrainment in fluids |
| CN103041623A (en) * | 2012-12-28 | 2013-04-17 | 河南省科学院高新技术研究中心 | High-efficiency organic silicon defoaming agent |
| CN103572653A (en) * | 2013-10-31 | 2014-02-12 | 江苏赛欧信越消泡剂有限公司 | Emulsion type silicon resin defoaming agent for pulping in papermaking |
-
2014
- 2014-07-21 CN CN201410349091.XA patent/CN104162294A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2012174405A1 (en) * | 2011-06-17 | 2012-12-20 | Kemira Oyj | Powder defoaming compositions and methods of reducing gas entrainment in fluids |
| CN102350097A (en) * | 2011-07-18 | 2012-02-15 | 南通恒尔特高分子材料科技有限公司 | Silicone-polyether antifoaming agent and preparation method thereof |
| CN102343165A (en) * | 2011-10-20 | 2012-02-08 | 山东大易化工有限公司 | Efficient silicone defoaming agent |
| CN103041623A (en) * | 2012-12-28 | 2013-04-17 | 河南省科学院高新技术研究中心 | High-efficiency organic silicon defoaming agent |
| CN103572653A (en) * | 2013-10-31 | 2014-02-12 | 江苏赛欧信越消泡剂有限公司 | Emulsion type silicon resin defoaming agent for pulping in papermaking |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105983252A (en) * | 2015-01-29 | 2016-10-05 | 吕锡池 | Plant oil-based defoamer and preparation method of same |
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