CN104155272B - A kind of method of squaric amide derivant detection TNT explosive - Google Patents
A kind of method of squaric amide derivant detection TNT explosive Download PDFInfo
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- CN104155272B CN104155272B CN201410354335.3A CN201410354335A CN104155272B CN 104155272 B CN104155272 B CN 104155272B CN 201410354335 A CN201410354335 A CN 201410354335A CN 104155272 B CN104155272 B CN 104155272B
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- tnt
- squaric amide
- amide derivant
- detection
- squaric
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Abstract
Description
Sample | 1 | 2 | 3 | 4 | 5 |
Theoretical content | 10-5 | 1.5×10-5 | 5×10-5 | 10-4 | 3×10-4 |
Detection level | 0.98×10-5 | 1.47×10-5 | 4.97×10-5 | 1.03×10-4 | 3.02×10-4 |
Sample | 1 | 2 | 3 | 4 | 5 |
Theoretical content | 10-5 | 1.5×10-5 | 5×10-5 | 10-4 | 3×10-4 |
Detection level | 0.98×10-5 | 1.48×10-5 | 5.02×10-5 | 1.02×10-4 | 2.97×10-4 |
Sample | 1 | 2 | 3 | 4 | 5 |
Theoretical content | 10-5 | 1.5×10-5 | 5×10-5 | 10-4 | 3×10-4 |
Detection level | 0.96×10-5 | 1.49×10-5 | 4.98×10-5 | 1.01×10-4 | 3.02×10-4 |
Claims (4)
Priority Applications (1)
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CN201410354335.3A CN104155272B (en) | 2014-07-23 | 2014-07-23 | A kind of method of squaric amide derivant detection TNT explosive |
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CN201410354335.3A CN104155272B (en) | 2014-07-23 | 2014-07-23 | A kind of method of squaric amide derivant detection TNT explosive |
Publications (2)
Publication Number | Publication Date |
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CN104155272A CN104155272A (en) | 2014-11-19 |
CN104155272B true CN104155272B (en) | 2016-07-06 |
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CN201410354335.3A Expired - Fee Related CN104155272B (en) | 2014-07-23 | 2014-07-23 | A kind of method of squaric amide derivant detection TNT explosive |
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CN (1) | CN104155272B (en) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN104865204B (en) * | 2015-01-16 | 2018-03-30 | 北京理工大学 | A kind of method for F colorimetric detections |
CN104897595A (en) * | 2015-05-21 | 2015-09-09 | 四川大学 | Method for simultaneously measuring contents of HMX, RDX and TNT in PBX explosive by ultraviolet spectrometry |
CN106167500B (en) * | 2016-06-08 | 2018-07-31 | 华中科技大学 | A kind of compound and preparation method thereof for explosive TNT detection and analysis |
Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2005047225A1 (en) * | 2003-11-17 | 2005-05-26 | Universidad Politecnica De Valencia | Method for the detection of thiols in aqueous solution |
CN101666748A (en) * | 2009-10-15 | 2010-03-10 | 青岛大学 | New method for detecting TNT in water phase by fluorescence |
CN101692023B (en) * | 2009-09-16 | 2011-04-20 | 合肥学院 | Chemical preparing method of molecular recognition of ultratrace explosive TNT based on fluorescence resonance energy transfer |
CN102795995A (en) * | 2012-08-16 | 2012-11-28 | 常州大学 | Squarylium cyanine chemical sensor used for Fe<3+> detection and preparation method thereof |
CN103173213A (en) * | 2013-03-11 | 2013-06-26 | 中南大学 | Hypochlorite ion fluorescence probe, and synthetic method and application thereof |
CN103389302A (en) * | 2013-04-07 | 2013-11-13 | 中国科学院化学研究所 | Detection method for trinitrotoluene (TNT) existing in different states by using colorimetry |
KR20130126400A (en) * | 2012-05-11 | 2013-11-20 | 경북대학교 산학협력단 | Squarylium dye and method for detecting anion |
CN103923481A (en) * | 2014-04-14 | 2014-07-16 | 福州大学 | Adamantyl-modified near-infrared squaraine dye as well as preparation method and application thereof |
-
2014
- 2014-07-23 CN CN201410354335.3A patent/CN104155272B/en not_active Expired - Fee Related
Patent Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2005047225A1 (en) * | 2003-11-17 | 2005-05-26 | Universidad Politecnica De Valencia | Method for the detection of thiols in aqueous solution |
CN101692023B (en) * | 2009-09-16 | 2011-04-20 | 合肥学院 | Chemical preparing method of molecular recognition of ultratrace explosive TNT based on fluorescence resonance energy transfer |
CN101666748A (en) * | 2009-10-15 | 2010-03-10 | 青岛大学 | New method for detecting TNT in water phase by fluorescence |
KR20130126400A (en) * | 2012-05-11 | 2013-11-20 | 경북대학교 산학협력단 | Squarylium dye and method for detecting anion |
CN102795995A (en) * | 2012-08-16 | 2012-11-28 | 常州大学 | Squarylium cyanine chemical sensor used for Fe<3+> detection and preparation method thereof |
CN103173213A (en) * | 2013-03-11 | 2013-06-26 | 中南大学 | Hypochlorite ion fluorescence probe, and synthetic method and application thereof |
CN103389302A (en) * | 2013-04-07 | 2013-11-13 | 中国科学院化学研究所 | Detection method for trinitrotoluene (TNT) existing in different states by using colorimetry |
CN103923481A (en) * | 2014-04-14 | 2014-07-16 | 福州大学 | Adamantyl-modified near-infrared squaraine dye as well as preparation method and application thereof |
Non-Patent Citations (3)
Title |
---|
N,N-diarylsquaramides: general, high-yield –ing synthesis and applications in colori -metric anion sensing;Rostami A, et al.;<J. Org. Chem.>;20101231;第75卷(第12期);第3983-3992页 * |
The squaramide versus urea contest for anion recognition;Amendola V, et al.;<Chem. Eur. J.>;20100412;第16卷(第14期);第4368-4380页 * |
杯[4]芳烃硝基衍生物的合成及其与TNT、RDX配合研究;陈鑫;<中国优秀硕士学位论文全文数据库>;20071015;第35-42页 * |
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Inventor after: Dan Bo Inventor after: Shu Qinghai Inventor after: Li Lijie Inventor after: Liu Yunfei Inventor after: Su Qiang Inventor before: Shu Qinghai Inventor before: Li Lijie Inventor before: Liu Yunfei Inventor before: Dan Bo Inventor before: Su Qiang |
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Free format text: CORRECT: INVENTOR; FROM: SHU QINGHAI LI LIJIE LIU YUNFEI DAN BO SU QIANG TO: DAN BO SHU QINGHAI LI LIJIE LIU YUNFEI SU QIANG |
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Inventor after: Shu Qinghai Inventor after: Wu Xiaoxue Inventor after: Li Lijie Inventor after: Liu Yunfei Inventor after: Dan Bo Inventor after: Su Qiang Inventor before: Dan Bo Inventor before: Shu Qinghai Inventor before: Li Lijie Inventor before: Liu Yunfei Inventor before: Su Qiang |
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