CN104126878B - Electronic cigarette with microcapsule releasing device and microcapsule - Google Patents

Electronic cigarette with microcapsule releasing device and microcapsule Download PDF

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Publication number
CN104126878B
CN104126878B CN201410402384.XA CN201410402384A CN104126878B CN 104126878 B CN104126878 B CN 104126878B CN 201410402384 A CN201410402384 A CN 201410402384A CN 104126878 B CN104126878 B CN 104126878B
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microcapsule
cigarette
cavity
adsorbing material
electronic cigarette
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CN201410402384.XA
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CN104126878A (en
Inventor
赵伟
孙志勇
杨柳
段沅杏
杨继
尚善斋
汤建国
朱东来
陈永宽
缪明明
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China Tobacco Yunnan Industrial Co Ltd
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China Tobacco Yunnan Industrial Co Ltd
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Abstract

The invention relates to an electronic cigarette with a microcapsule releasing device and a microcapsule. The electronic cigarette with the microcapsule releasing device comprises a cigarette-shaped cavity shell, a battery, an indicating lamp, a cigarette holder and an adsorbing material, an atomizer is arranged in the adsorbing material and is connected with the battery and a starting switch, the indicating lamp is located on one end face of the cigarette-shaped cavity shell, the battery and the adsorbing material are arranged at the end, close to the indicating lamp, in the cigarette-shaped cavity shell, a microcapsule cavity is formed in the other end of the adsorbing material and is internally provided with a microcapsule, the cigarette holder is arranged at the other end of the microcapsule cavity, and a piercing needle is arranged in the middle of the cigarette holder. The electronic cigarette with the microcapsule releasing device and the microcapsule have the advantages that releasing can be controlled, the stability of tobacco tar can be controlled, the microcapsule can be replaced, taste and smell can be shielded, other smells in the environment cannot enter the tobacco tar easily, and the ingredients of the tobacco tar are protected against contamination.

Description

A kind of electronic cigarette containing Microencapsulated Slow device and microcapsule
Technical field
The present invention relates to a kind of electronic cigarette containing Microencapsulated Slow device and microcapsule, belong to electronic cigarette production technical field.
Background technology
Electronic cigarette, also known as electronics nicotine transmission system, official of the World Health Organization (WHO) to electronics nicotine transmission system It is defined as:Electronics nicotine transmission system(ENDS)It is a kind of consumer products, nicotine can be transmitted to lung.Luxuriant and rich with fragrance not Nicotiana tabacum L. is public The research such as department, Reynolds Tobacco Company shows that TPM and bio-toxicity of electronic cigarette etc. are significantly reduced.Further, since Its in physiology impression, psychological response, suck the aspects such as mode relatively traditional cigarette, therefore suffered from the green grass or young crops of consumers in general Look at.
Country's Zhao Yu loyalties have applied for first electronic cigarette utility model patent " electronic cigarette " within 1989 (CN89207339.X), the research of subsequent electronic cigarette is constantly in dormancy state;Just enter electronic cigarette at the beginning of 2000 to grind The developmental stage sent out, domestic Han Li has applied for a series of utility model patents(CN200580011022.7、 CN200200710123347.5、CN201080016105.6、CN03111582.9、CN200720148285.9), started generation The tide of electronic cigarette development, has established conditional electronic cigarette apparatus structure in the range of boundary.Electronic cigarette device has generally comprised tobacco rod(Bag Include the components and parts such as light emitting diode, battery, control circuit, pneumatic switch, nebulizer)With cigarette bullet(Including reservoir compartment and suction nozzle). There is a gas channel in the inside center line position of tobacco rod, when electronic cigarette is aspirated, negative pressure of the pneumatic inductive switch in suction The lower triggering of effect, integral control circuit is connected, and display lamp is lighted, and the ree-oil atomization in reservoir compartment, atomization ree-oil enters with air-flow Enter human oral cavity, so as to reach the effect that simulation is smoked.
In traditional electronic cigarette device structure, ree-oil is infiltrated on the first-class adsorbing material of glass cotton, but in storage and is transported During unavoidably bring the volatilization loss of ree-oil composition;And more importantly infiltrate ree-oil adsorbing material, Jing batteries The smoke components that heating is discharged are uneven, and presentation first rises and declines afterwards, and the persistence of smoke perfume substance release is poor, therefore Smoker's normal physiological demand can not be met.
The content of the invention
It is an object of the invention to provide a kind of electronic cigarette containing Microencapsulated Slow device and slight capsule, can be according to individual Taste loads the microcapsule of different taste, can carry out combination in any, can shield taste and abnormal smells from the patient.By ree-oil micro encapsulation, every Contact with environment absolutely so that other abnormal smells from the patients are not easily accessible in ree-oil in environment, it is ensured that ree-oil composition is not contaminated.
Microcapsule technology is using naturally occurring or synthetic macromolecular material(Utricule)By solid, liquid or gas(Capsule is tolerant) A kind of miniature microcapsule technology with semipermeable membrane or sealing cyst membrane that Jing encapsulations are formed.The present invention utilizes microcapsule technology, The delayed release device and microcapsule of a kind of electronic cigarette microcapsule are devised, is mainly used in improving the release of electronic cigarette flue gas fragrance matter Persistence.
The technical scheme is that:
A kind of electronic cigarette containing Microencapsulated Slow device, including cigarette cavity shell, battery, display lamp, cigarette holder, absorption Material, there is nebulizer in adsorbing material, and is connected with battery and activate switch, and display lamp is in one end of cigarette cavity shell Face, battery, adsorbing material be mounted in successively in cigarette cavity shell by display lamp one end, it is characterised in that in adsorbing material The other end has microcapsule cavity, the built-in microcapsule of the cavity, and the other end of microcapsule cavity is cigarette holder, the middle spinosity of cigarette holder Pin.
There is a space between described microcapsule cavity and cigarette holder.
Described cigarette holder is tube-in-tube structure, is provided with an internal layer, and internal layer is connected or is slidably connected with cigarette holder outer layer screw thread, cigarette Mouth aspiration end is provided with suction socket.
Described pricker is arranged on cigarette holder outer layer inner hub location, to puncture microcapsule,
Described microcapsule cavity is poroid infiltration sieve plate near adsorbing material end, and is contacted with adsorbing material.
Described microcapsule can load one or more than one, and microcapsule is replaceable.When microcapsule is 2 or more, such as First microcapsule core contains nicotine, glycerol or Propylene Glycol, menthol;Second microcapsule contains dorinone;Two Microcapsule position can combination in any.
Above-described microcapsule is prepared as follows:
Microcapsule core formula includes nicotine, Propylene Glycol or glycerol, menthol, Propylene Glycol or glycerol quality percentage Than for 85-90%, nicotine mass percent is 5-7%, menthol or dorinone mass percent are 2-8%.
The aqueous gelatin solution for taking appropriate 10% stirs, and in being placed on 45~55 DEG C of water-bath, with 5% acetic acid pH is adjusted It is worth to 5-6, is cooled to 40-50 DEG C or so, add any of the above composition and stir 24 h, adds dehydrated alcohol and in l000 Stir under the conditions of r/min, stand and filter, dry the microcapsule under the conditions of 5-6 DEG C(Can by aqueous gelatin solution and nicotine, third Glycol or glycerol, menthol weight ratio are:1-10:0.5-5:1-10:0.5-5 is configured).Or prepare by the method for prior art Microcapsule.
It is an advantage of the current invention that:1. control release.By the way that ree-oil composition is slightly encapsulated, can reach ree-oil composition by Discharge according to certain rate uniform, obtain the suction sensation that fragrance uniformly discharges;2. the stability of ree-oil is improved.Due to microcapsule Core can be separated with surrounding, it is to avoid the impact of air, temperature etc., while it also avoid in storage and transportation The volatilization loss of fragrance matter;3. microcapsule is realized replaceable.Microcapsule can load one or more than one, while according to individual Taste can also load the microcapsule of different taste, carry out combination in any;4. taste and abnormal smells from the patient are shielded.By ree-oil microcapsule Change, completely cut off and contacted with environment so that other abnormal smells from the patients are not easily accessible in ree-oil in environment, it is ensured that ree-oil composition is not contaminated.
Description of the drawings
Fig. 1 is the electronic cigarette structure schematic diagram containing Microencapsulated Slow device of the present invention.
1- display lamps, 2- cigarette cavity shells, 3- batteries, 4- adsorbing materials, the poroid infiltration sieve plates of 5-, 6- is micro- Capsule, 7- microcapsule cavitys, 8- spaces, 9- internal layers, 10- cigarette holder outer layers, 11- prickers.
Specific embodiment
Embodiment 1:
As shown in figure 1, a kind of electronic cigarette containing Microencapsulated Slow device, including cigarette cavity shell 2, battery 3, instruction Lamp 1, cigarette holder(Including cigarette holder outer layer 10 and internal layer 9), adsorbing material 4, have nebulizer in adsorbing material, and open with battery and startup Pass is connected, and in the end face of cigarette cavity shell, battery, adsorbing material are mounted in successively in cigarette cavity shell display lamp By display lamp one end(Below prior art can be adopted.There is microcapsule cavity in the other end of adsorbing material, the cavity is built-in Microcapsule 6, the other end of microcapsule cavity 7 is cigarette holder, and there is pricker 11 centre of cigarette holder.
There is a space 8 between described microcapsule cavity 7 and cigarette holder.
Described cigarette holder is tube-in-tube structure, is provided with an internal layer 9, and internal layer 9 is connected or adopts with the screw thread of cigarette holder outer layer 10 It is slidably connected, cigarette holder aspiration end is provided with suction socket.
Described pricker 11 is arranged on the inner hub location of cigarette holder outer layer 10, to puncture microcapsule.
Described microcapsule cavity is the infiltration sieve plate 5 of cavernous structure near adsorbing material end, and is contacted with adsorbing material, Liquid is penetrated in adsorbing material by it in make microcapsule.
Described microcapsule cavity 7 is poroid infiltration sieve plate 5 near adsorbing material end.
Described microcapsule can load one or more than one, and microcapsule is replaceable.
When rotating or pressing cigarette holder outer layer 10, pricker 11 can puncture microcapsule 6, and by suction microcapsule cavity is formed Middle negative pressure so that liquid flows to adsorbing material by permeability apparatus in the microcapsule for puncturing.Microcapsule content can pass through poroid The hole of infiltration sieve plate 5 is flowed in adsorbing material 4.
Embodiment 2:
The above microcapsule core formula includes nicotine, Propylene Glycol, menthol, and Propylene Glycol mass percent is 85%, Nicotine mass percent is 7%, and menthol mass percent is 8%.
Preparation method:Will be appropriate(Also can be by aqueous gelatin solution and nicotine, Propylene Glycol or glycerol, menthol weight ratio For:1-10:0.5-5:1-10:0.5-5)10% aqueous gelatin solution stirs, and in being placed on 45~55 DEG C of water-bath, uses 5% acetic acid adjusts pH value to 5.0 or so, is cooled to 40 DEG C or so, adds any of the above composition and stirs 24 h, adds anhydrous second Alcohol is simultaneously stirred under the conditions of l000 r/min, is stood and is filtered, dry the microcapsule under the conditions of 5 DEG C.Or by existing technology its Its method prepares microcapsule.
Embodiment 3:
The above microcapsule core formula composition see the table below;
The microcapsule for preparing is inserted in electronic cigarette, and sense organ has been carried out with the electronic cigarette of no added microcapsule and commented Inhale, as a result see the table below.Electronic cigarette is far from each other with traditional cigarette due to the principle that flue gas discharges, it is necessary to which electronic cigarette sense organ is commented Inhale index and score value is necessarily adjusted:Sweet sense, amount of smoke are that electronic cigarette is smoked panel test important indicator, therefore spy is added to sensory evolution In index;The device is mainly used in increasing the persistence of smoke perfume release, while reducing ree-oil due to exposing band in the environment The miscellaneous QI for coming, therefore add persistence, miscellaneous QI index.
From sensory evolution as can be seen that Microencapsulated Slow technique device is applied in electronic cigarette, compared with the control, items sense See index to make moderate progress.By the application of the slow release method device of microcapsule so that flue gas release is more uniform, zest and Persistence is significantly improved.Further, since ree-oil is wrapped in microcapsule, it is to avoid ree-oil exposure introduces in atmosphere other Fragrance, miscellaneous QI has also obtained to a certain degree reducing.

Claims (4)

1. a kind of electronic cigarette containing Microencapsulated Slow device, including cigarette cavity shell(2), battery(3), display lamp(1), cigarette Mouth, adsorbing material(4), there is nebulizer in adsorbing material, and be connected with battery and activate switch, display lamp is in cigarette cavity The end face of shell, battery, adsorbing material be mounted in successively in cigarette cavity shell by display lamp one end, it is characterised in that: There is microcapsule cavity in the other end of adsorbing material(7), the built-in microcapsule of the cavity(6), microcapsule cavity(7)The other end be There is pricker cigarette holder, the centre of cigarette holder(11);Described microcapsule cavity is near the infiltration sieve plate that adsorbing material end is cavernous structure (5);Described cigarette holder is tube-in-tube structure, is provided with an internal layer, and internal layer is connected or is slidably connected with cigarette holder outer layer screw thread, and cigarette holder is taken out Inhale end and be provided with suction socket, described pricker is arranged on cigarette holder outer layer(10)Inner hub location, to puncture microcapsule.
2. the electronic cigarette containing Microencapsulated Slow device according to claim 1, it is characterised in that described microcapsule cavity with There is a space between cigarette holder(8).
3. the electronic cigarette of Microencapsulated Slow device is contained according to claim 1, it is characterised in that described microcapsule filling one Or more than one.
4. a kind of microcapsule of the as claimed in claim 1 electronic cigarette containing Microencapsulated Slow device, it is characterised in that microcapsule is matched somebody with somebody Side includes nicotine, Propylene Glycol or glycerol and menthol or dorinone;Propylene Glycol or glycerol mass percent are 85- 90%, nicotine mass percent is 5-7%, and menthol or dorinone mass percent are 2-8%.
CN201410402384.XA 2014-08-15 2014-08-15 Electronic cigarette with microcapsule releasing device and microcapsule Active CN104126878B (en)

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CN104824850B (en) * 2015-04-01 2017-07-21 湖北中烟工业有限责任公司 It is a kind of containing nicotine-containing sustained release pellet without hot smokeless cigarette
PL3127441T3 (en) 2015-08-06 2019-06-28 Fontem Holdings 1 B.V. Electronic smoking device with a glass capillary tube
CN106543138A (en) * 2015-09-16 2017-03-29 黄志萍 It is a kind of to keep the non-discoloring method of nicotine and its application
CN105212273A (en) * 2015-09-18 2016-01-06 云南中烟工业有限责任公司 A kind of electronic cigarette fat capsule
CN205358218U (en) * 2015-11-30 2016-07-06 深圳麦克韦尔股份有限公司 Electronic cigarette and atomization device thereof
AU2016379094A1 (en) * 2015-12-24 2018-06-21 Philip Morris Products S.A. Nicotine powder delivery system
CN105411005B (en) * 2015-12-28 2018-12-07 湖南中烟工业有限责任公司 A kind of non-burning cigarette cigarette core of electric heating type and preparation method thereof
US11096415B2 (en) * 2016-05-31 2021-08-24 Philip Morris Products S.A. Heated aerosol-generating article with liquid aerosol-forming substrate and combustible heat generating element
GB201615602D0 (en) * 2016-09-14 2016-10-26 British American Tobacco Investments Ltd Receptacle Section
CN108420110B (en) * 2017-02-14 2024-02-27 湖南中烟工业有限责任公司 Cigarette, capsule type electronic cigarette atomizer and electronic cigarette thereof
CN110150744B (en) * 2018-02-13 2021-09-14 湖南中烟工业有限责任公司 Heating non-combustion cigarette and preparation method thereof
CN108968146A (en) * 2018-06-08 2018-12-11 云南中烟工业有限责任公司 A kind of liquid storage capsule and its preparation method and application
CN108741223B (en) * 2018-06-29 2024-05-07 中国烟草总公司郑州烟草研究院 Gaseous explosive bead cigarette
CN108652090B (en) * 2018-08-06 2024-02-27 深圳市华玉科技发展有限公司 Explosion bead type oil storage electronic cigarette
CN110367590A (en) * 2019-07-08 2019-10-25 龚忠盘 One kind crushing formula water core cigarette holder
WO2022236830A1 (en) * 2021-05-14 2022-11-17 深圳麦克韦尔科技有限公司 Atomizer, electronic atomization apparatus, and method for generating aerosol
CN113229521A (en) * 2021-06-23 2021-08-10 张家港外星人新材料科技有限公司 Electronic atomized liquid composition and packaging container thereof
CN114680362B (en) * 2021-12-28 2023-03-21 四川三联新材料有限公司 Electronic cigarette liquid with refreshing function

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