CN104116021B - The method of the nuclei of crystallization in removing honey - Google Patents
The method of the nuclei of crystallization in removing honey Download PDFInfo
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- CN104116021B CN104116021B CN201410232881.XA CN201410232881A CN104116021B CN 104116021 B CN104116021 B CN 104116021B CN 201410232881 A CN201410232881 A CN 201410232881A CN 104116021 B CN104116021 B CN 104116021B
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- honey
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- green molasses
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L21/00—Marmalades, jams, jellies or the like; Products from apiculture; Preparation or treatment thereof
- A23L21/20—Products from apiculture, e.g. royal jelly or pollen; Substitutes therefor
- A23L21/25—Honey; Honey substitutes
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/30—Physical treatment, e.g. electrical or magnetic means, wave energy or irradiation
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- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Jellies, Jams, And Syrups (AREA)
Abstract
The invention discloses a kind of method removing the nuclei of crystallization in honey, first green molasses is diluted to water content 50 ~ 65% by the method, is placed in 200 order filters and filters, the dead honeybee of honey contained in removing dilution green molasses, the large molecular impurity of beeswax; Then green molasses heating hydrolysis process under 30 ~ 50 DEG C of conditions will be diluted after removal of impurities; Again the dilution green molasses wash-out after heating is obtained secondary eluent, be concentrated at 30 ~ 50 DEG C of filter vacuum the filtrate that water content is 10 ~ 20%; By water content be 10 ~ 20% filtrate be placed in resin column and cross post process, obtain non crystallized honey.The present invention eliminates the minute impurities and Bee Pollen that are invisible to the naked eye in honey, and the nutrition of honey, active material are retained, eliminate the minute impurities causing honey crystallization in honey, the Bee Pollen nuclei of crystallization, and the content not needing the condition of adding any material to reduce glucose in honey, obtains non crystallized honey.
Description
Technical field
The present invention relates to a kind of honey processing method, refer to a kind of method removing the nuclei of crystallization in honey particularly.
Background technology
Honey is a kind of product that often can contact and eat in people's daily life, the problem that in the prior art of honey processing, existence one is serious: the easy crystallization of honey.The crystallization of honey is in fact that glucose separates out separated a kind of phenomenon and process from honey.From the viewpoint of molecular theory, in honey, glucose molecule was with having no order moving originally, but glucose exceedes its solubility in honey, when becoming supersaturated solution, start to move regularly, line up in honey with regard to some glucose molecule, form small nuclei of crystallization, become the center of a crystallization, more glucose molecule is arranged in its each regularly, forms larger crystal gradually, separate from honey, Here it is honey crystallization.Honey crystallization is mainly due to two reasons:
1, honey is the supersaturated solution of glucose and fructose, and the content of its glucose and fructose is greater than 60%, and glucose content is higher, the easier crystallization of honey, and e.g., in acacia honey and Mel Jujubae, fructose content is higher, and crystallization time is slower.
2, a large amount of pollen is contained in honey, tiny Bee Pollen is wherein a kind of nuclei of crystallization, filter although secondly pass through in honey processing, but adopt 200 mesh filter screens to filter because general, can only the larger impurity of filtering, can not filter invisible fine impurities and Bee Pollen, trickle impurity and Bee Pollen become the nuclei of crystallization, are also to cause one of easy crystallization reason of honey.
Current honey processing factory mainly destroys the nuclei of crystallization by the method heated honey, to postpone its crystallization, because heating can only dissolve glucose crystallization core, do not reduce the nuclei of crystallization quantity existed in honey, so the effect of postponing honey crystallization is poor, and because heating-up temperature is too high, destroy nutrition and the mouthfeel of honey.Because honey crystallization affects its perception, edible inconvenient, so a part of consumer does not approve, a difficult problem for honey crystallization Shi Kunlong honey enterprise, postpones the problem that honey crystallization is also the outer honey enterprise of Present Domestic.
Summary of the invention
Technical problem to be solved by this invention is just to provide a kind of method removing the nuclei of crystallization in honey.The method heats under cryogenic, and under need not adding the condition of any material, removes most of nuclei of crystallization in green molasses, obtains the honey that non-crystallizable and nutritional labeling does not run off.
For solving the problems of the technologies described above, a kind of method removing the nuclei of crystallization in honey provided by the invention, comprises the following steps:
1) green molasses is diluted to water content 50 ~ 65%, is placed in 200 order filters and filters, the dead honeybee of honey contained in removing dilution green molasses, the large molecular impurity of beeswax;
2) green molasses heating hydrolysis process under 30 ~ 50 DEG C of conditions will be diluted after removal of impurities;
3) by the dilution green molasses after heating through alkalescence anion-exchange resin process, obtain one-level eluent, then one-level eluent is de-in siliceous earth column washes, obtains secondary eluent;
4) under pressure is 0.5 ~ 2MPs condition, by the pressure filtration of secondary eluent, filtrate is obtained;
5) be concentrated at 30 ~ 50 DEG C of filter vacuum the filtrate that water content is 10 ~ 20%;
6) by water content be 10 ~ 20% filtrate be placed in resin column and cross post process, obtain non crystallized honey, wherein, crossing column flow rate is 0.3 ~ 0.5mL/min.
Further, described step 6) in, hydrochloric acid, mass fraction that eluent is 4% by mass fraction are 1% NaOH and the deionized water mixed liquor that mixes of 1 ︰ 1 ︰ 1 ~ 3 by volume.
Beneficial effect of the present invention is:
1, the present invention eliminates the minute impurities and Bee Pollen that are invisible to the naked eye in honey, and the nutrition of honey, active material are retained, eliminate the minute impurities causing honey crystallization in honey, the Bee Pollen nuclei of crystallization, and the content not needing the condition of adding any material to reduce glucose in honey, thus postpone the honey crystallization phase, obtain non crystallized honey.
2, the present invention processes green molasses at low temperatures, at utmost lower nutritional labeling and the active material ensureing honey.
Detailed description of the invention
In order to explain the present invention better, illustrate main contents of the present invention further below in conjunction with specific embodiment, but content of the present invention is not only confined to following examples.
Remove a method for the nuclei of crystallization in honey, comprise the following steps:
1) green molasses is diluted to water content 50 ~ 65%, is placed in 200 order filters and filters, the dead honeybee of honey contained in removing dilution green molasses, the large molecular impurity of beeswax;
2) green molasses heating hydrolysis process under 30 ~ 50 DEG C of conditions will be diluted after removal of impurities;
3) by the dilution green molasses after heating through alkalescence anion-exchange resin process, obtain one-level eluent, then one-level eluent is de-in siliceous earth column washes, obtains secondary eluent;
4) under pressure is 0.5 ~ 2MPs condition, by the pressure filtration of secondary eluent, filtrate is obtained;
5) be concentrated at 30 ~ 50 DEG C of filter vacuum the filtrate that water content is 10 ~ 20%;
6) by water content be 10 ~ 20% filtrate be placed in resin column and cross post process, obtain non crystallized honey, wherein, crossing column flow rate is 0.3 ~ 0.5mL/min, and hydrochloric acid, mass fraction that eluent is 4% by mass fraction are 1% NaOH and the deionized water mixed liquor that mixes of 1 ︰ 1 ︰ 1 ~ 3 by volume.
The honey of preparation is carried out test compare,
1, impurity affects shown in table 1 on honey crystallization:
With green molasses for blank group, honey prepared by conventional method is control group, and it is experimental group that this method obtains honey.
Table 1
| Impurity content (%) | There is the time (d) of crystallization | |
| Control group | 5～10％ | 7 |
| Blank group | 10～20％ | 3 |
| Experimental group | 0.05～0.2％ | ＞35 |
2, table 2 is the content of various nutriment in heat treatment under different temperatures
Table 2
Shown in table 2, the rising of temperature at any time, the content of reduced sugar increases, and fruit Portugal is than increasing, and the content of protein and vitamin reduces, and is optimum temperature when temperature is 35 DEG C.Reduce than prior art temperature like this, contribute to reducing nutriment and run off.
3, the present invention shown in table 3 prepares the contrast of glucose in honey and heat treated green molasses
The present invention prepares that honey is experimental group, green molasses is control group.
| Glucose content (%) | Fruit Portugal ratio | |
| Experimental group | 30.45 | 1.34 |
| Control group | 32.31 | 1.19 |
The present invention takes off by heat treatment and resin column that to wash honey that conbined usage prepares more a lot of than high than the fruit Portugal of only heat treated green molasses, is conducive to the non-crystallizable of honey.
Other unspecified part is prior art.Although above-described embodiment is to invention has been detailed description; but it is only the present invention's part embodiment; instead of whole embodiment, people can also obtain other embodiments according to the present embodiment under without creative prerequisite, and these embodiments all belong to scope.
Claims (2)
1. remove a method for the nuclei of crystallization in honey, it is characterized in that: comprise the following steps:
1) green molasses is diluted to water content 50 ~ 65%, is placed in 200 order filters and filters, the dead honeybee of honey contained in removing dilution green molasses, the large molecular impurity of beeswax;
2) green molasses heating hydrolysis process under 30 ~ 50 DEG C of conditions will be diluted after removal of impurities;
3) by the dilution green molasses after heating through alkalescence anion-exchange resin process, obtain one-level eluent, then one-level eluent is injected siliceous earth column carry out de-washing, obtain secondary eluent;
4) under pressure is 0.5 ~ 2Mpa condition, by the pressure filtration of secondary eluent, filtrate is obtained;
5) under temperature is 30 ~ 50 DEG C of conditions, filter vacuum is concentrated into the filtrate that water content is 10 ~ 20%;
6) by water content be 10 ~ 20% filtrate be placed in alkalescence anion-exchange resin and cross post process, obtain non crystallized honey, wherein, crossing column flow rate is 0.3 ~ 0.5mL/min.
2. remove the method for the nuclei of crystallization in honey according to claim 1, it is characterized in that: described step 6) in, hydrochloric acid, mass fraction that eluent is 4% by mass fraction are 1% NaOH and the deionized water mixed liquor that mixes of 1 ︰ 1 ︰ 1 ~ 3 by volume.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410232881.XA CN104116021B (en) | 2014-05-29 | 2014-05-29 | The method of the nuclei of crystallization in removing honey |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410232881.XA CN104116021B (en) | 2014-05-29 | 2014-05-29 | The method of the nuclei of crystallization in removing honey |
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| CN104116021B true CN104116021B (en) | 2016-04-13 |
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Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104522458A (en) * | 2015-02-03 | 2015-04-22 | 芜湖蜂联有限公司 | Processing method for removing pollen in honey |
| CN106259219A (en) * | 2016-08-17 | 2017-01-04 | 普洱宏阳农林苗木扩繁有限公司 | The collection of a kind of coffee nectar and processing method |
| CN111772024A (en) * | 2020-08-05 | 2020-10-16 | 安徽泓顺源生物科技有限公司 | Formula and preparation method of honey fructose |
| CN112189820A (en) * | 2020-10-14 | 2021-01-08 | 贵州嘉禾香农业发展有限责任公司 | Processing method for improving honey crystallization |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH03160963A (en) * | 1989-11-15 | 1991-07-10 | Gifu Youhou Kk | Noncrystalline honey and production thereof |
| CN1315140A (en) * | 2000-03-30 | 2001-10-03 | 上海大承生物制品有限公司 | Process for preparing high-purity honey not crystallized easily |
| CN101785539A (en) * | 2009-12-16 | 2010-07-28 | 中国农业科学院蜜蜂研究所 | Honey difficult to crystallize and preparation method thereof |
-
2014
- 2014-05-29 CN CN201410232881.XA patent/CN104116021B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH03160963A (en) * | 1989-11-15 | 1991-07-10 | Gifu Youhou Kk | Noncrystalline honey and production thereof |
| CN1315140A (en) * | 2000-03-30 | 2001-10-03 | 上海大承生物制品有限公司 | Process for preparing high-purity honey not crystallized easily |
| CN101785539A (en) * | 2009-12-16 | 2010-07-28 | 中国农业科学院蜜蜂研究所 | Honey difficult to crystallize and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 国内外蜂蜜加工工艺流程的新进展;潘建国等;《中国商办工业》;20010831(第8期);第43-45页 * |
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Address after: 430301 Hengdian Street Hengtian Road, Huangpi District, Wuhan City, Hubei Province Patentee after: Wuhan Sinter Food Co., Ltd. Address before: 430301 Hengdian Street Hengtian Road, Huangpi District, Wuhan City, Hubei Province Patentee before: WUHAN SIWEITE FOOD CO., LTD. |