CN104086082A - Beer bottle glass and preparation method thereof - Google Patents
Beer bottle glass and preparation method thereof Download PDFInfo
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- CN104086082A CN104086082A CN201410356397.8A CN201410356397A CN104086082A CN 104086082 A CN104086082 A CN 104086082A CN 201410356397 A CN201410356397 A CN 201410356397A CN 104086082 A CN104086082 A CN 104086082A
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- beer bottle
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Abstract
The invention discloses a beer bottle glass and a preparation method thereof. The method comprises the following steps: 1) mixing and melting quartz sand, sodium carbonate, calcite, wood charcoal, white arsenic, mirabilite, copper sulfate, aluminum oxide and potassium dichromate at 1400-1550 DEG C to prepare a melt; 2) casting the melt at 1200-1250 DEG C to obtain a primary finished product; and 3) annealing the primary finished product at 540-560 DEG C to obtain the beer bottle glass. The beer bottle glass disclosed by the invention has the advantages of thin wall, excellent internal pressure resistance and excellent shock resistance.
Description
Technical field
The present invention relates to glass art, particularly, relate to a kind of beer bottle glass and preparation method thereof.
Background technology
Beer bottle glass has directly affected the quality of Beer Bottle, and especially the thickness of beer bottle glass and intensity play key effect.Beer bottle glass too thick, has not only increased production cost, has increased the weight of Beer Bottle simultaneously so that has been not easy to carrying.Beer bottle glass too thin, is difficult to ensure that the intensity of Beer Bottle makes Beer Bottle easily broken.
Summary of the invention
The object of this invention is to provide a kind of beer bottle glass, this beer bottle glass thin thickness and intensity are high, and the step of simultaneously preparing this beer bottle glass is simple, and raw material is easy to get.
To achieve these goals, the invention provides a kind of preparation method of beer bottle glass, described method comprises:
1) quartz sand, soda ash, calcite, charcoal, white arsenic, saltcake, copper sulfate, aluminum oxide and potassium bichromate are carried out at 1400-1550 DEG C to mixed melting to make the operation of melts;
2) described melts is carried out at 1200-1250 DEG C to cast molding to make the just operation of finished product;
3) described just finished product is annealed to make at 540-560 DEG C the operation of beer bottle glass;
Wherein, with respect to the quartz sand of 100 weight parts, the consumption of described soda ash is that the consumption of 45-50 weight part, described calcite is 5-7 weight part, the consumption of described charcoal is 0.3-0.5 weight part, the consumption of described white arsenic is 0.03-0.06 weight part, the consumption of described saltcake is 5-6 weight part, and the consumption of described copper sulfate is 1.1-1.3 weight part, and the consumption of described potassium bichromate is 1.2-1.4 weight part.
The present invention also provides a kind of beer bottle glass, and described beer bottle glass obtains by above-mentioned method preparation.
According to technique scheme, it is in quartz sand, soda ash, calcite, charcoal and copper sulfate that white arsenic, potassium bichromate, aluminum oxide and saltcake are joined the raw material of preparing glass in prior art by the present invention, make the beer bottle glass making when wall is thin, there is excellent intensity by the synergy of white arsenic, potassium bichromate and saltcake, thereby greatly reduced the cost of producing Beer Bottle.The method steps of preparing in addition this beer bottle glass is simple, and raw material is easy to get.
Other features and advantages of the present invention are described in detail the embodiment part subsequently.
Embodiment
Below the specific embodiment of the present invention is elaborated.Should be understood that, embodiment described herein only, for description and interpretation the present invention, is not limited to the present invention.
The invention provides a kind of preparation method of beer bottle glass, described method comprises:
1) quartz sand, soda ash, calcite, charcoal, white arsenic, saltcake, copper sulfate, aluminum oxide and potassium bichromate are carried out at 1400-1550 DEG C to mixed melting to make the operation of melts;
2) described melts is carried out at 1200-1250 DEG C to cast molding to make the just operation of finished product;
3) described just finished product is annealed to make at 540-560 DEG C the operation of beer bottle glass.
In the present invention, the consumption of each raw material can be selected in wide scope, for the beer bottle glass that makes to make has more excellent physical strength, preferably, with respect to the quartz sand of 100 weight parts, the consumption of described soda ash is 45-50 weight part, the consumption of described calcite is 5-7 weight part, the consumption of described charcoal is 0.3-0.5 weight part, the consumption of described white arsenic is 0.03-0.06 weight part, the consumption of described saltcake is 5-6 weight part, the consumption of described copper sulfate is 1.1-1.3 weight part, the consumption of described aluminum oxide is 1-5 weight part, the consumption of described potassium bichromate is 1.2-1.4 weight part.
Carrying out mixed melting to make in the operation of melts, the temperature of described mixed melting can be selected in wide scope, and for the beer bottle glass that makes to make has more excellent physical strength, preferably, the temperature of described mixed melting is 1430-1450 DEG C.
Carrying out mixed melting to make in the operation of melts, in the scope that the time of described mixed melting can be wide, select, for the beer bottle glass that makes to make has more excellent physical strength and improves the productive rate of beer bottle glass, preferably, the time of described mixed melting is 2-3h.
Carrying out cast molding to make in the operation of first finished product, the temperature of described cast molding can be selected in wide scope, and for the beer bottle glass that makes to make has more excellent physical strength, preferably, the temperature of described cast molding is 1230-1240 DEG C.
Carrying out cast molding to make in the operation of first finished product, the time of described cast molding can be selected in wide scope, for the beer bottle glass that makes to make has more excellent physical strength and improves the productive rate of beer bottle glass, preferably, the time of described cast molding is 1-2h.
Annealing to make in the operation of beer bottle glass, the temperature of described annealing can be selected in wide scope, and for the beer bottle glass that makes to make has more excellent physical strength, preferably, the temperature of described annealing is 550-555 DEG C.
Annealing to make in the operation of beer bottle glass, the time of described annealing can be selected in this wide scope, for the beer bottle glass that makes to make has more excellent physical strength and improves the productive rate of beer bottle glass, preferably, the time of described annealing is 1.5-2.5h.
The present invention also provides a kind of beer bottle glass, and described beer bottle glass is prepared gained by above-mentioned method.The method step is simple, easy to operate, and raw material is easy to get simultaneously.
Below will describe the present invention by embodiment.In following examples, vial carrying capacity parameter records by the vial carrying capacity test machine of Zhaoqing Jia Yi Instrument Ltd., and vial shock resistance parameter records by the vial impact test machine of Beijing Cheng Jiaquan Science and Technology Ltd..
Quartz sand is the product of Tianjin Yan Dong mineral products company limited; soda ash is the product of Tianjin supply and marketing company of BoHai Chemical Engineering group; calcite is the product of Lingshou County Wo Kun mineral products processing factory; charcoal is the product of Ke Xing gac factory of Changge City; saltcake is the product of Dongying City Shuan Qiao Chemical Co., Ltd.; copper sulfate is the product of Chang Yuan Chemicals company limited of Zhengzhou City; aluminum oxide is the product of Guangzhou De Zunliang Chemical Industry Science Co., Ltd, and potassium bichromate is the product of Shijiazhuang Bai Na auxiliary chemicals company limited.
Embodiment 1
At 1440 DEG C by 100kg quartz sand, 48kg soda ash, 6kg calcite, 0.4kg charcoal, 0.05kg white arsenic, 5.5kg saltcake, 1.2kg copper sulfate, 3kg aluminum oxide and 1.3kg potassium bichromate mixed melting 2.5h, then at 1235 DEG C, carry out cast molding and keep constant temperature 1.5h, at last 553 DEG C, anneal and keep the thick beer bottle glass A1 of the cooling 5mm of making after constant temperature 2h, the burst strength of this beer bottle glass is 2.4MPa, and impact energy values is 2.9Nm.
Embodiment 2
At 1430 DEG C by 100kg quartz sand, 45kg soda ash, 5kg calcite, 0.3kg charcoal, 0.03kg white arsenic, 5kg saltcake, 1.1kg copper sulfate, 1kg aluminum oxide and 1.2kg potassium bichromate mixed melting 2h, then at 1230 DEG C, carry out cast molding and keep constant temperature 1h, at last 550 DEG C, anneal and keep the thick beer bottle glass A2 of the cooling 5mm of making after constant temperature 1.5h, the burst strength of this beer bottle glass is 2.3MPa, and impact energy values is 2.9Nm.
Embodiment 3
At 1450 DEG C by 100kg quartz sand, 50kg soda ash, 7kg calcite, 0.5kg charcoal, 0.06kg white arsenic, 6kg saltcake, 1.3kg copper sulfate, 5kg aluminum oxide and 1.4kg potassium bichromate mixed melting 3h, then at 1240 DEG C, carry out cast molding and keep constant temperature 2h, at last 555 DEG C, anneal and keep the thick beer bottle glass A3 of the cooling 5mm of making after constant temperature 2.5h, the burst strength of this beer bottle glass is 2.4MPa, and impact energy values is 2.8Nm.
Embodiment 4
Make beer bottle glass A4 according to the method for embodiment 1, difference is that the temperature of mixed melting is 1400 DEG C, and the burst strength of this beer bottle glass is 2.3MPa, and impact energy values is 2.7Nm.
Embodiment 5
Make beer bottle glass A5 according to the method for embodiment 1, difference is that the temperature of mixed melting is 1550 DEG C, and the burst strength of this beer bottle glass is 2.2MPa, and impact energy values is 2.7Nm.
Embodiment 6
Make beer bottle glass A6 according to the method for embodiment 1, difference is that the temperature of cast molding is 1200 DEG C, and the burst strength of this beer bottle glass is 2.3MPa, and impact energy values is 2.4Nm.
Embodiment 7
Make beer bottle glass A7 according to the method for embodiment 1, difference is that the temperature of cast molding is 1250 DEG C, and the burst strength of this beer bottle glass is 2.4MPa, and impact energy values is 2.6Nm.
Embodiment 8
Make beer bottle glass A8 according to the method for embodiment 1, difference is that the temperature of annealing is 540 DEG C, and the burst strength of this beer bottle glass is 2.3MPa, and impact energy values is 2.8Nm.
Embodiment 9
Make beer bottle glass A9 according to the method for embodiment 1, difference is that the temperature of annealing is 560 DEG C, and the burst strength of this beer bottle glass is 2.3MPa, and impact energy values is 2.7Nm.
Comparative example 1
Make beer bottle glass B1 according to the method for embodiment 1, difference is that the temperature of mixed melting is 1300 DEG C, and the burst strength of this beer bottle glass is 2.0MPa, and impact energy values is 2.0Nm.
Comparative example 2
Make beer bottle glass B2 according to the method for embodiment 1, difference is that the temperature of mixed melting is 1650 DEG C, and the burst strength of this beer bottle glass is 2.0MPa, and impact energy values is 1.9Nm.
Comparative example 3
Make beer bottle glass B3 according to the method for embodiment 1, difference is that the temperature of cast molding is 1100 DEG C, and the burst strength of this beer bottle glass is 1.8MPa, and impact energy values is 2.1Nm.
Comparative example 4
Make beer bottle glass B4 according to the method for embodiment 1, difference is that the temperature of cast molding is 1350 DEG C, and the burst strength of this beer bottle glass is 2.0MPa, and impact energy values is 1.8Nm.
Comparative example 5
Make beer bottle glass B5 according to the method for embodiment 1, difference is that the temperature of annealing is 530 DEG C, and the burst strength of this beer bottle glass is 2.0MPa, and impact energy values is 2.1Nm.
Comparative example 6
Make beer bottle glass B6 according to the method for embodiment 1, difference is that the temperature of annealing is 580 DEG C, and the burst strength of this beer bottle glass is 1.9MPa, and impact energy values is 2.1Nm.
From above-described embodiment and comparative example, beer bottle glass wall provided by the invention is thin has excellent internal pressure-resistant performance and shock resistance simultaneously.
More than describe the preferred embodiment of the present invention in detail; but the present invention is not limited to the detail in above-mentioned embodiment, within the scope of technical conceive of the present invention; can carry out multiple simple variant to technical scheme of the present invention, these simple variant all belong to protection scope of the present invention.
It should be noted that in addition, each concrete technical characterictic described in above-mentioned embodiment, in reconcilable situation, can combine by any suitable mode, for fear of unnecessary repetition, the present invention is to the explanation no longer separately of various possible array modes.
In addition, also can carry out arbitrary combination between various embodiment of the present invention, as long as it is without prejudice to thought of the present invention, it should be considered as content disclosed in this invention equally.
Claims (9)
1. a preparation method for beer bottle glass, is characterized in that, described method comprises:
1) quartz sand, soda ash, calcite, charcoal, white arsenic, saltcake, copper sulfate, aluminum oxide and potassium bichromate are carried out at 1400-1550 DEG C to mixed melting to make the operation of melts;
2) described melts is carried out at 1200-1250 DEG C to cast molding to make the just operation of finished product;
3) described just finished product is annealed to make at 540-560 DEG C the operation of beer bottle glass.
2. preparation method according to claim 1, wherein, with respect to the quartz sand of 100 weight parts, the consumption of described soda ash is that the consumption of 45-50 weight part, described calcite is 5-7 weight part, and the consumption of described charcoal is 0.3-0.5 weight part, and the consumption of described white arsenic is 0.03-0.06 weight part, the consumption of described saltcake is 5-6 weight part, the consumption of described copper sulfate is 1.1-1.3 weight part, and the consumption of described aluminum oxide is 1-5 weight part, and the consumption of described potassium bichromate is 1.2-1.4 weight part.
3. according to the preparation method described in any one in claim 1 or 2, wherein, carrying out mixed melting to make in the operation of melts, the temperature of described mixed melting is 1430-1450 DEG C.
4. preparation method according to claim 3, wherein, carrying out mixed melting to make in the operation of melts, the time of described mixed melting is 2-3h.
5. according to the preparation method described in any one in claim 1 or 2, wherein, carrying out cast molding to make in the operation of first finished product, the temperature of described cast molding is 1230-1240 DEG C.
6. preparation method according to claim 5, wherein, carrying out cast molding to make in the operation of first finished product, the time of described cast molding is 1-2h.
7. according to the preparation method described in any one in claim 1 or 2, wherein, annealing to make in the operation of beer bottle glass, the temperature of described annealing is 550-555 DEG C.
8. preparation method according to claim 7, wherein, annealing to make in the operation of beer bottle glass, the time of described annealing is 1.5-2.5h.
9. a beer bottle glass, is characterized in that, described beer bottle glass obtains by the method preparation described in any one in claim 1-8.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410356397.8A CN104086082B (en) | 2014-07-24 | 2014-07-24 | Beer bottle glass and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410356397.8A CN104086082B (en) | 2014-07-24 | 2014-07-24 | Beer bottle glass and preparation method thereof |
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| CN104086082A true CN104086082A (en) | 2014-10-08 |
| CN104086082B CN104086082B (en) | 2016-05-11 |
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| CN201410356397.8A Expired - Fee Related CN104086082B (en) | 2014-07-24 | 2014-07-24 | Beer bottle glass and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106116145A (en) * | 2016-06-30 | 2016-11-16 | 芜湖滕波电子商务有限公司 | High-intensity inorganic salt fat and preparation method thereof |
| CN107082564A (en) * | 2017-06-29 | 2017-08-22 | 合肥利裕泰玻璃制品有限公司 | A kind of white wine bottle glass and preparation method thereof |
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| EP2319811A1 (en) * | 2009-11-04 | 2011-05-11 | Orange Bottle Company B.V. | Protective beer bottle with high luminous transmittance |
| CN102557443A (en) * | 2012-01-16 | 2012-07-11 | 芜湖市天地电子科技有限公司 | Bear bottle and preparation method thereof |
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Patent Citations (6)
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| EP2319811A1 (en) * | 2009-11-04 | 2011-05-11 | Orange Bottle Company B.V. | Protective beer bottle with high luminous transmittance |
| CN102584017A (en) * | 2011-01-18 | 2012-07-18 | 武汉华夏玻璃制品有限公司 | Method for manufacturing beer bottles through broken glass |
| CN102557443A (en) * | 2012-01-16 | 2012-07-11 | 芜湖市天地电子科技有限公司 | Bear bottle and preparation method thereof |
| CN103241954A (en) * | 2012-02-08 | 2013-08-14 | 訾然 | Method for producing a green glass beer bottle |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106116145A (en) * | 2016-06-30 | 2016-11-16 | 芜湖滕波电子商务有限公司 | High-intensity inorganic salt fat and preparation method thereof |
| CN107082564A (en) * | 2017-06-29 | 2017-08-22 | 合肥利裕泰玻璃制品有限公司 | A kind of white wine bottle glass and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN104086082B (en) | 2016-05-11 |
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