CN104074044B - Ultra-fine non-dust cloth of blending and preparation method thereof - Google Patents
Ultra-fine non-dust cloth of blending and preparation method thereof Download PDFInfo
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Abstract
The present invention provides the preparation method of the ultra-fine non-dust cloth of a kind of blending and prepared non-dust cloth thereof, and key step includes: dacron thread and polyester-nylon microfiber silk knitting machine that mass ratio is 1:2 is carried out mixed weaving and makes grey cloth；According to the bath raio of 1:5～7, grey cloth is put in dye vat；Penetrating agent, sodium hydroxide, EDTA 4Na and degreaser is added in dye vat；Cleaning in limit side washing row's mode, acetic acid soaks, and again cleans, is subsequently adding detergent, again cleans grey cloth etc. in limit side washing row's mode.The preparation method of the ultra-fine non-dust cloth of blending that the present invention provides, its non-dust cloth prepared not only has the characteristics such as good wearability, cleanliness factor and dirty removal capacities, and it effectively reduces cost, and technological process is simple.
Description
Technical field
The invention belongs to non-dust cloth field, it is a kind of by terylene with the non-dust cloth of polyester-nylon composite superfine fibre blending for particularly relating to, and uses
In replace the industry conventional wash brocade composite superfine non-dust cloth.
Background technology
Non-dust cloth is a kind of chemistry cloth being widely used in electron-optical medical treatment semiconductor equipment, cleanliness factor, the suction to itself
The property received, dust removal, wearability have the highest requirement, commonly use terylene non-dust cloth or wash compound ultra-fine of brocade in current row
Non-dust cloth.Terylene non-dust cloth competitively priced but dust removing effects is general, and rough surface easily abrades sophisticated product surface.And wash brocade
Composite ultrafine fiber non-dust cloth absorbability, dust removal performance are excellent, and surface exquisiteness is difficult to abrade sophisticated product surface, but expensive,
Make product cost be greatly increased, therefore be widely adopted not yet.
Additionally, the non-dust cloth that current non-dust cloth manufacture method prepares often there is also cleannes, dust adsorption ability, wearability
And the aspect such as dirty removal capacities is difficult to meet the defect of requirement, and production process is relatively complicated.
Summary of the invention
For making up the deficiencies in the prior art, the present invention provides the preparation method of the ultra-fine non-dust cloth of a kind of blending, the nothing that the method prepares
Dirt cloth not only has the characteristics such as good wearability, cleanliness factor and dirty removal capacities, and it effectively reduces cost, technique stream
Journey is simple.
The present invention is for reaching its purpose, and the technical scheme of employing is as follows:
The preparation method of the ultra-fine non-dust cloth of a kind of blending, comprises the steps:
1) dacron thread and polyester-nylon microfiber silk knitting machine that mass ratio is 1:2 are carried out mixed weaving, make grey cloth；
2) in dye vat, RO water is added, according to the bath raio of 1:5～7 by step 1) grey cloth for preparing puts in dye vat；
3) in dye vat, penetrating agent, sodium hydroxide, EDTA-4Na and degreaser are added；The temperature of solution in dye vat is risen to
105～110 DEG C, it is incubated 30～40 minutes；Penetrating agent, sodium hydroxide, EDTA-4Na and the degreaser concentration in dye vat is divided
It is not 1～1.5g/L, 6～10g/L, 1～1.5g/L, 2～4g/L.
4) grey cloth in dye vat, cooling are cleaned in limit side washing row's mode (that is, outwards discharging the solution in dye vat while cleaning)
To 50 DEG C, it is incubated 2～5 minutes；
5) in dye vat, add acetic acid to soak；
6) again grey cloth is cleaned in limit side washing row's mode, the water in the most drained dye vat；
7) in dye vat, add detergent, and in dye vat, inject RO water, be warming up to 120～125 DEG C, be incubated 55～65 minutes；
8) again grey cloth is cleaned in limit side washing row's mode；
9) in dye vat, inject RO water, be warming up to 60 DEG C, be incubated 8～15 minutes；
10) clean grey cloth in limit side washing row's mode, lower the temperature simultaneously, after being cooled to 40 DEG C, be incubated 8～15 minutes；
11) in dye vat, inject RO water, and again clean grey cloth in limit side washing row's mode, the water in the most drained dye vat, go out cloth.
Its specification of described dacron thread is 50D/72F, and described its specification of polyester-nylon microfiber silk is 75D/35F, uses this specification
Dacron thread and the collocation blending of polyester-nylon microfiber silk, prepare non-dust cloth best results, and not only cost is well controlled, and
Prepare non-dust cloth the aspects such as wearability, cleanliness factor and dirty removal capacities performance the most more preferably.
Further, step 5) in, the concentration of acetic acid is 0.3～0.5g/L.
Preferably, step 5) in, soak 4～7 minutes with acetic acid.
Preferably, step 7) in, the concentration of detergent is 1～2g/L.
Penetrating agent used by the present invention, degreaser, detergent all select the product that the art is conventional, such as, infiltration
Agent can use JFC, and degreaser can use the LZC301A etc. that degreaser ZJ-C301, connection village science and technology produce, and detergent can
With with liquid detergent, such as white cat board liquid detergent.
Second aspect present invention provides the ultra-fine non-dust cloth of blending that a kind of basis preparation method as described above prepares.
Polyester-nylon microfiber silk those skilled in the art described in literary composition are also called polyester-nylon composite superfine fibre or polyester-nylon superthin silk.
The water of RO (Reverses Osmosis) the i.e. reverse osmosis described in literary composition.Bath raio described in literary composition is the normal of the art
Rule technical term, it refers to the ratio (quality) of fabric and solution.
The technical scheme that the present invention provides, has the advantages that
Dacron thread and polyester-nylon superthin silk are passed through certain proportion blending by the present invention, then according to the washing process optimized, grey cloth is carried out water
Washing, its absorbent properties of non-dust cloth, wearability and the aspect such as cleanliness factor and dirty removal capacities prepared is attained by the requirement of superfine fibre
Standard, can substitute superfine fibre on a large scale.
Non-dust cloth prepared by the present invention, its raw materials used cost is low compared with superfine fibre dust-free cloth, but grey cloth cleanliness factor is higher, washing
Process simplification, can greatly limit reduce non-dust cloth cost.
The present invention is employed many times the mode of limit side washing row in the water-washing process of grey cloth can prevent contamination, can improve to greatest extent
Cleaning degree.
The named Pylon of non-dust cloth that the preparation method of the present invention is prepared by present inventor.
Detailed description of the invention
Below in conjunction with embodiment, technical scheme is described further:
Embodiment 1
Preparation embodiment for non-dust cloth.
A kind of ultra-fine non-dust cloth of blending, prepares in accordance with the following steps:
1) by dacron thread 50D/72F that mass ratio is 1:2 and the polyester-nylon microfiber silk 75D/35F circular knitting machine of 40 pins
Carry out mixed weaving, make grey cloth；Obtained its grammes per square metre of grey cloth is 105 ± 12g/m2, fabric width 2.24 ± 0.02m,
Thickness 0.44 ± 0.04mm；
2) in dye vat, RO water (about 2400L) is added, according to the bath raio of 1:6 by step 1) grey cloth for preparing puts into dye vat
In；
3) in dye vat, penetrating agent JFC 1.2g/L, sodium hydroxide 8g/L, EDTA-4Na 1.2g/L and degreaser LZC301A are added
3g/L；The temperature of solution in dye vat is risen to 110 DEG C, is incubated 35 minutes, time-consuming 40 minutes altogether；
4) cleaning the grey cloth in dye vat in limit side washing row's mode, be cooled to 50 DEG C, insulation runs 3 minutes, time-consuming 10 minutes altogether；
5) in dye vat, add acetic acid 0.4g/L, soak 5 minutes；
6) again grey cloth is cleaned 10 minutes in limit side washing row's mode, the water in drained dye vat after terminating；
7) in dye vat, add liquid detergent (the present embodiment uses white cat board to concentrate liquid detergent) 1.5g/L, and in dye vat, inject RO
Water (about 1400L), is warming up to 120 DEG C, and insulation runs 60 minutes；
8) in dye vat, inject RO water (about 1700L) again, again clean grey cloth 10 minutes in limit side washing row's mode；
9) injecting RO water (1080L) in dye vat, be warming up to 60 DEG C, insulation runs 10 minutes；
10) in dye vat, inject RO water (about 1700L) again, lower the temperature cleaning grey cloth, after being cooled to 40 DEG C in limit side washing row's mode
Insulation runs 10 minutes；
11) in dye vat, inject RO water (about 1700L), and again clean grey cloth in limit side washing row's mode, the most drained dye vat
Interior water, goes out cloth after draining.
12) open-width, sizing, rewinding, packaging；The non-dust cloth grammes per square metre 130 ± 12g/m2 of acquisition, fabric width 1.85 ± 0.02m, thickness
Degree 0.40 ± 0.04mm.
Embodiment 2
Preparation embodiment for non-dust cloth.
A kind of ultra-fine non-dust cloth of blending, prepares in accordance with the following steps:
1) by dacron thread 50D/72F that mass ratio is 1:2 and the polyester-nylon microfiber silk 75D/35F circular knitting machine of 40 pins
Carry out mixed weaving, make grey cloth；Obtained its grammes per square metre of grey cloth is 105 ± 12g/m2, fabric width 2.24 ± 0.02m,
Thickness 0.44 ± 0.04mm；
2) in dye vat, RO water (about 2400L) is added, according to the bath raio of 1:7 by step 1) grey cloth for preparing puts into dye vat
In；
3) in dye vat, add penetrating agent JFC 1.5g/L, sodium hydroxide 10g/L, EDTA-4Na 1.5g/L and degreaser (this
Embodiment degreaser is the LZC301A that connection village science and technology produces) 4g/L；The temperature of solution in dye vat is risen to 110 DEG C,
It is incubated 35 minutes, time-consuming 40 minutes altogether；
4) cleaning the grey cloth in dye vat in limit side washing row's mode, be cooled to 50 DEG C, insulation runs 3 minutes, time-consuming 10 minutes altogether；
5) in dye vat, add acetic acid 0.5g/L, soak 5 minutes；
6) again grey cloth is cleaned 10 minutes in limit side washing row's mode, the water in drained dye vat after terminating；
7) in dye vat, add liquid detergent (the present embodiment uses white cat board to concentrate liquid detergent) 2g/L, and in dye vat, inject RO
Water (about 1400L), is warming up to 125 DEG C, and insulation runs 60 minutes；
8) in dye vat, inject RO water (about 1700L) again, again clean grey cloth 10 minutes in limit side washing row's mode；
9) injecting RO water (1080L) in dye vat, be warming up to 60 DEG C, insulation runs 10 minutes；
10) in dye vat, inject RO water (about 1700L) again, lower the temperature cleaning grey cloth, after being cooled to 40 DEG C in limit side washing row's mode
Insulation runs 10 minutes；
11) in dye vat, inject RO water (about 1700L), and again clean grey cloth in limit side washing row's mode, the most drained dye vat
Interior water, goes out cloth after draining.
12) open-width, sizing, rewinding, packaging；The non-dust cloth grammes per square metre 130 ± 12g/m2 of acquisition, fabric width 1.85 ± 0.02m, thickness
Degree 0.40 ± 0.04mm.
Embodiment 3
Preparation embodiment for non-dust cloth.
A kind of ultra-fine non-dust cloth of blending, prepares in accordance with the following steps:
1) by dacron thread 50D/72F that mass ratio is 1:2 and the polyester-nylon microfiber silk 75D/35F circular knitting machine of 40 pins
Carry out mixed weaving, make grey cloth；Obtained its grammes per square metre of grey cloth is 105 ± 12g/m2, fabric width 2.24 ± 0.02m,
Thickness 0.44 ± 0.04mm；
2) in dye vat, RO water (about 2400L) is added, according to the bath raio of 1:5 by step 1) grey cloth for preparing puts into dye vat
In；
3) in dye vat, penetrating agent JFC 1g/L, sodium hydroxide 6g/L, EDTA-4Na 1g/L and degreaser (this enforcement are added
Example degreaser is the LZC301A that connection village science and technology produces) 2g/L；The temperature of solution in dye vat is risen to 105 DEG C, insulation
35 minutes, time-consuming 40 minutes altogether；
4) cleaning the grey cloth in dye vat in limit side washing row's mode, be cooled to 50 DEG C, insulation runs 3 minutes, time-consuming 10 minutes altogether；
5) in dye vat, add acetic acid 0.3g/L, soak 5 minutes；
6) again grey cloth is cleaned 10 minutes in limit side washing row's mode, the water in drained dye vat after terminating；
7) in dye vat, add liquid detergent (the present embodiment uses white cat board to concentrate liquid detergent) 1g/L, and in dye vat, inject RO
Water (about 1400L), is warming up to 120 DEG C, and insulation runs 60 minutes；
8) in dye vat, inject RO water (about 1700L) again, again clean grey cloth 10 minutes in limit side washing row's mode；
9) injecting RO water (1080L) in dye vat, be warming up to 60 DEG C, insulation runs 10 minutes；
10) in dye vat, inject RO water (about 1700L) again, lower the temperature cleaning grey cloth, after being cooled to 40 DEG C in limit side washing row's mode
Insulation runs 10 minutes；
11) in dye vat, inject RO water (about 1700L), and again clean grey cloth in limit side washing row's mode, the most drained dye vat
Interior water, goes out cloth after draining.
12) open-width, sizing, rewinding, packaging；The non-dust cloth grammes per square metre 130 ± 12g/m2 of acquisition, fabric width 1.85 ± 0.02m, thickness
Degree 0.40 ± 0.04mm.
Non-dust cloth prepared by the embodiment of the present invention 1 is detected, and existing WIP-5009 superfine fibre dust-free cloth
(WIP-5009DLE) under the conditions of same detection its testing result correction data as shown in table 1 below and table 2:
Table 1 non-dust cloth performance test results contrasts
Table 2 non-dust cloth IC (ion chromatography) testing result contrasts
Remarks: ND is not detected by
Non-dust cloth and the non-dust cloth testing result of embodiment 1 that the embodiment of the present invention 2,3 prepares are basically identical, repeat no more.By
Table 1,2 is visible, and the non-dust cloth that the present invention prepares is attained by ultra-fine fibre from absorbent properties, wearability and cleanliness factor and dirty removal capacities
The requirement standard of dimension, it can substitute superfine fibre on a large scale.
Penetrating agent used in specific embodiment, degreaser, detergent all can select the product that the art is conventional, such as,
Penetrating agent can use JFC, and degreaser can use the LZC301A etc. that degreaser ZJ-C301 or connection village science and technology produce, and washes
Washing agent can be with white cat board liquid detergent etc..Not specified part in literary composition, those skilled in the art all can pass through this skill grasped
Prior art or the common knowledge in art field are known, and repeat no more.
The above, be only presently preferred embodiments of the present invention, and the present invention not does any pro forma restriction, therefore all
Without departing from the content of technical solution of the present invention, according to the present invention technical spirit to any simple modification made for any of the above embodiments,
Equivalent variations and modification, all still fall within the range of technical solution of the present invention.
Claims (6)
1. the preparation method of the ultra-fine non-dust cloth of blending, it is characterised in that comprise the steps:
1) dacron thread and polyester-nylon microfiber silk knitting machine that mass ratio is 1:2 are carried out mixed weaving, make grey cloth, described
Knitting machine is the circular knitting machine of 40 pins；
2) in dye vat, RO water is added, according to the bath raio of 1:5～7 by step 1) grey cloth for preparing puts in dye vat；
3) in dye vat, penetrating agent 1～1.5g/L, sodium hydroxide 6～10g/L, EDTA-4Na 1～1.5g/L and degreaser are added
2～4g/L；The temperature of solution in dye vat is risen to 105～110 DEG C, is incubated 30～40 minutes；
4) clean the grey cloth in dye vat in limit side washing row's mode, be cooled to 50 DEG C, be incubated 2～5 minutes；
5) in dye vat, add acetic acid to soak；
6) again grey cloth is cleaned in limit side washing row's mode, the water in the most drained dye vat；
7) in dye vat, add detergent, and in dye vat, inject RO water, be warming up to 120～125 DEG C, be incubated 55～65 minutes；
8) again grey cloth is cleaned in limit side washing row's mode；
9) in dye vat, inject RO water, be warming up to 60 DEG C, be incubated 8～15 minutes；
10) clean grey cloth in limit side washing row's mode, lower the temperature simultaneously, after being cooled to 40 DEG C, be incubated 8～15 minutes；
11) in dye vat, inject RO water, and again clean grey cloth in limit side washing row's mode, the water in the most drained dye vat, go out cloth.
The preparation method of the ultra-fine non-dust cloth of blending the most according to claim 1, it is characterised in that its specification of described dacron thread is
50D/72F, described its specification of polyester-nylon microfiber silk is 75D/35F.
The preparation method of the ultra-fine non-dust cloth of blending the most according to claim 1, it is characterised in that step 5) in, acetic acid dense
Degree is 0.3～0.5g/L.
The preparation method of the ultra-fine non-dust cloth of blending the most according to claim 1, it is characterised in that step 5) in, soak with acetic acid
Steep 4～7 minutes.
The preparation method of the ultra-fine non-dust cloth of blending the most according to claim 1, it is characterised in that step 7) in, detergent
It is 1～2g/L that concentration controls.
6. the ultra-fine non-dust cloth of blending that the basis preparation method as described in any one of Claims 1 to 5 prepares.
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| CN106968106B (en) * | 2017-06-01 | 2019-06-18 | 龙钜超洁净科技（苏州）有限公司 | A kind of low soft flocks non-dust cloth procedure for producing of super abrasive |
| CN107523928A (en) * | 2017-09-25 | 2017-12-29 | 惠州市杰佰净化有限公司 | A kind of production method of high abrasion purification cleaning wiping cloth |
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| CN100441767C (en) * | 2006-07-18 | 2008-12-10 | 东华大学 | One-step process preprocessing technology of cotton fibric biological enzyme high-temp desizing refining and bleaching |
| CN102002846B (en) * | 2010-09-10 | 2012-04-18 | 东莞市中港净化用品科技有限公司 | Method for producing non-dust cloth |
| CN202081235U (en) * | 2011-05-16 | 2011-12-21 | 上海嘉麟杰纺织品股份有限公司 | Wiping cloth prepared by ultra-fine fibers and knitting terries |
| CN102535201A (en) * | 2011-12-06 | 2012-07-04 | 常熟市凯达印染有限公司 | Cold pad-batch dyeing process for pure cotton fabric |
| CN103361871A (en) * | 2012-03-19 | 2013-10-23 | 厦门市康保无尘科技有限公司 | Production method of antistatic non-dust cloth |
| CN103046383B (en) * | 2012-11-27 | 2016-05-04 | 江南大学 | A kind of enzyme oxygen one is bathed cotton type fabric low temperature pre-treating method |
| CN103147277A (en) * | 2013-03-27 | 2013-06-12 | 海安县锦荣化纤有限公司 | Method for preparing hollow polyester fiber textile fabric |
| CN103422338B (en) * | 2013-08-08 | 2015-04-22 | 东莞市无极净化用品科技有限公司 | Cleaning method for dust-free duster |
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