CN104031725B - A kind of anti-bacterial lubricant and preparation method thereof - Google Patents

A kind of anti-bacterial lubricant and preparation method thereof Download PDF

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Publication number
CN104031725B
CN104031725B CN201410293265.5A CN201410293265A CN104031725B CN 104031725 B CN104031725 B CN 104031725B CN 201410293265 A CN201410293265 A CN 201410293265A CN 104031725 B CN104031725 B CN 104031725B
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parts
polyoxyethylene glycol
lubricant
polydimethylsiloxane
polyacrylamide
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CN104031725A (en
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丁演
顾肖红
潘琳
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Zhuhai Meihe Technology Co., Ltd.
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Wuxi Chongan District Technology Innovation Service Center
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Abstract

A kind of anti-bacterial lubricant and preparation method thereof, this anti-bacterial lubricant comprises the following raw material according to mass fraction meter: tea oil 36-40 part, polydimethylsiloxane 12-14 part, ether of cellulose 24-30 part, graphite 12-15 part, single stearic acid glycerine lipoprotein 20-30 part, dilinoleic acid palmitin 5-8 part, polyacrylamide 15-26 part, polyoxyethylene glycol 20-24 part, glycerol 30-34 part.The present invention utilizes the common rationally composite of tea oil and other additives, effectively improves the lubricity of lubricant; Meanwhile, to other additives, there is good dissolution dispersity after utilizing single stearic acid glycerine lipoprotein and polyoxyethylene glycol mixing, thus effectively improve the lubricity of lubricant.

Description

A kind of anti-bacterial lubricant and preparation method thereof
Technical field
The invention belongs to technical field of lubricating oil, be specifically related to a kind of anti-bacterial lubricant and preparation method thereof.
Background technology
In recent years, along with developing rapidly of industry, lubricant use in the industry also tends to future development that is efficient, environmental protection gradually, and some lubrications with excellent lubricating function have extensively popular to people.Nowadays people not only require that lubricating oil has excellent lubricity, also will have excellent dispersiveness, good perviousness and environment amenable performance.Especially in recent years along with the enhancing gradually of people's environmental consciousness, the environment protective lubricant of people to multifunctional type was more favored.
Lubricating oil can reduce the friction between thing and thing, thus effectively reduces the abrasion of object.Along with the development of mechanical industry, the application of lubricating oil in mechanical devices, pipeline pump valve is also very extensive.Traditional lubricant had by some gradually the compounded lubricating oil of excellent lubricity replace, these lubricants not only have good oilness, also have the unexistent property of some conventional lubrication oil.And the composite problem in lubricant between base oil and additive is the technical barrier that field of lubricant is comparatively difficult always.
Although lubricant commercially available is at present the perfect further difference in functionality of lubricating oil, composite not ideal enough due between additive, still causes the effect of lubricant undesirable.
Summary of the invention
The object of this invention is to provide a kind of anti-bacterial lubricant and preparation method thereof, solve the conventional lubricant deficiency that lubricant effect is not good between friction means.
Present invention employs following technical scheme:
A kind of anti-bacterial lubricant, comprises the following raw material according to mass fraction meter: tea oil 36-40 part, polydimethylsiloxane 12-14 part, ether of cellulose 24-30 part, graphite 12-15 part, single stearic acid glycerine lipoprotein 20-30 part, dilinoleic acid palmitin 5-8 part, polyacrylamide 15-26 part, polyoxyethylene glycol 20-24 part, glycerol 30-34 part.
Described anti-bacterial lubricant, comprises the following raw material according to mass fraction meter: tea oil 36-38 part, polydimethylsiloxane 12-13 part, ether of cellulose 24-26 part, graphite 12-14 part, single stearic acid glycerine lipoprotein 20-25 part, dilinoleic acid palmitin 5-6 part, polyacrylamide 15-20 part, polyoxyethylene glycol 20-22 part, glycerol 30-33 part.
Described anti-bacterial lubricant, comprises the following raw material according to mass fraction meter: tea oil 38 parts, polydimethylsiloxane 13 parts, ether of cellulose 26 parts, 14 parts, graphite, single stearic acid glycerine lipoprotein 25 parts, dilinoleic acid palmitin 6 parts, polyacrylamide 20 parts, polyoxyethylene glycol 22 parts, glycerol 33 parts.
The preparation method of anti-bacterial lubricant, comprises the following steps:
The first step: according to quality proportioning, tea oil 36-40 part, polydimethylsiloxane 12-14 part, ether of cellulose 24-30 part, graphite 12-15 part, single stearic acid glycerine lipoprotein 20-30 part, dilinoleic acid palmitin 5-8 part are mixed, 20-30min is stirred at 45-50 DEG C, leave standstill, cool, obtain mixture A;
Second step: by step one gained mixture A and polyacrylamide 15-26 part, polyoxyethylene glycol 20-24 part, glycerol 30-34 part mixing and stirring, stirring velocity 200-250r/min, to obtain final product.
At 50 DEG C, 25min is stirred in step one.
beneficial effect
The present invention utilizes the common rationally composite of tea oil and other additives, effectively improves the lubricity of lubricant; Meanwhile, to other additives, there is good dissolution dispersity after utilizing single stearic acid glycerine lipoprotein and polyoxyethylene glycol mixing, thus effectively improve the lubricity of lubricant.
Embodiment
embodiment 1
A kind of anti-bacterial lubricant, comprises the following raw material according to mass fraction meter: tea oil 36kg, polydimethylsiloxane 12kg, ether of cellulose 24kg, graphite 12kg, single stearic acid glycerine lipoprotein 20kg, dilinoleic acid palmitin 5kg, polyacrylamide 15kg, polyoxyethylene glycol 20kg, glycerol 30kg.
The preparation method of the present embodiment, comprises the following steps:
The first step: according to quality proportioning, tea oil 36kg, polydimethylsiloxane 12kg, ether of cellulose 24kg, graphite 12kg, single stearic acid glycerine lipoprotein 20kg, dilinoleic acid palmitin 5kg are mixed, at 45 DEG C, stir 20min, leave standstill, cool, obtain mixture A;
Second step: by step one gained mixture A and polyacrylamide 15kg, polyoxyethylene glycol 20kg, glycerol 30kg mixing and stirring, stirring velocity 200r/min, to obtain final product.
embodiment 2
A kind of anti-bacterial lubricant, comprises the following raw material according to mass fraction meter: tea oil 40kg, polydimethylsiloxane 14kg, ether of cellulose 30kg, graphite 15kg, single stearic acid glycerine lipoprotein 30kg, dilinoleic acid palmitin 8kg, polyacrylamide 26kg, polyoxyethylene glycol 24kg, glycerol 34kg.
The preparation method of the present embodiment, comprises the following steps:
The first step: according to quality proportioning, tea oil 40kg, polydimethylsiloxane 14kg, ether of cellulose 30kg, graphite 15kg, single stearic acid glycerine lipoprotein 30kg, dilinoleic acid palmitin 8kg are mixed, at 50 DEG C, stir 30min, leave standstill, cool, obtain mixture A;
Second step: by step one gained mixture A and polyacrylamide 26kg, polyoxyethylene glycol 24kg, glycerol 34kg mixing and stirring, stirring velocity 250r/min, to obtain final product.
embodiment 3
Anti-bacterial lubricant, comprises the following raw material according to mass fraction meter: tea oil 38kg, polydimethylsiloxane 13kg, ether of cellulose 26kg, graphite 14kg, single stearic acid glycerine lipoprotein 25kg, dilinoleic acid palmitin 6kg, polyacrylamide 20kg, polyoxyethylene glycol 22kg, glycerol 33kg.
The preparation method of the present embodiment, comprises the following steps:
The first step: according to quality proportioning, tea oil 38kg, polydimethylsiloxane 13kg, ether of cellulose 26kg, graphite 14kg, single stearic acid glycerine lipoprotein 25kg, dilinoleic acid palmitin 6kg are mixed, at 45 DEG C, stir 30min, leave standstill, cool, obtain mixture A;
Second step: by step one gained mixture A and polyacrylamide 20kg, polyoxyethylene glycol 22kg, glycerol 33kg mixing and stirring, stirring velocity 250r/min, to obtain final product.
embodiment 4
A kind of anti-bacterial lubricant, comprises the following raw material according to mass fraction meter: tea oil 37kg, polydimethylsiloxane 12kg, ether of cellulose 24kg, graphite 13kg, single stearic acid glycerine lipoprotein 20kg, dilinoleic acid palmitin 6kg, polyacrylamide 15kg, polyoxyethylene glycol 22kg, glycerol 30kg.
The preparation method of the present embodiment, comprises the following steps:
The first step: according to quality proportioning, tea oil 37kg, polydimethylsiloxane 12kg, ether of cellulose 24kg, graphite 13kg, single stearic acid glycerine lipoprotein 20kg, dilinoleic acid palmitin 6kg are mixed, at 45 DEG C, stir 20min, leave standstill, cool, obtain mixture A;
Second step: by step one gained mixture A and polyacrylamide 15kg, polyoxyethylene glycol 22kg, glycerol 30kg mixing and stirring, stirring velocity 200r/min, to obtain final product.
embodiment 5
A kind of anti-bacterial lubricant, comprises the following raw material according to mass fraction meter: tea oil 38kg, polydimethylsiloxane 14kg, ether of cellulose 30kg, graphite 15kg, single stearic acid glycerine lipoprotein 24kg, dilinoleic acid palmitin 5kg, polyacrylamide 15kg, polyoxyethylene glycol 20kg, glycerol 34kg.
The preparation method of the present embodiment, comprises the following steps:
The first step: according to quality proportioning, tea oil 38kg, polydimethylsiloxane 14kg, ether of cellulose 30kg, graphite 15kg, single stearic acid glycerine lipoprotein 24kg, dilinoleic acid palmitin 5kg are mixed, at 45 DEG C, stir 20min, leave standstill, cool, obtain mixture A;
Second step: by step one gained mixture A and polyacrylamide 15kg, polyoxyethylene glycol 20kg, glycerol 34kg mixing and stirring, stirring velocity 200r/min, to obtain final product.
embodiment 6
A kind of anti-bacterial lubricant, comprises the following raw material according to mass fraction meter: tea oil 36kg, polydimethylsiloxane 12kg, ether of cellulose 28kg, graphite 13kg, single stearic acid glycerine lipoprotein 25kg, dilinoleic acid palmitin 7kg, polyacrylamide 15kg, polyoxyethylene glycol 22kg, glycerol 31kg.
The preparation method of the present embodiment, comprises the following steps:
The first step: according to quality proportioning, tea oil 36kg, polydimethylsiloxane 12kg, ether of cellulose 28kg, graphite 13kg, single stearic acid glycerine lipoprotein 25kg, dilinoleic acid palmitin 7kg are mixed, at 45 DEG C, stir 20min, leave standstill, cool, obtain mixture A;
Second step: by step one gained mixture A and polyacrylamide 15kg, polyoxyethylene glycol 22kg, glycerol 31kg mixing and stirring, stirring velocity 200r/min, to obtain final product.
reference examples 1
Be with the difference of embodiment 3: do not add single stearic acid glycerine lipoprotein in the 1st step, in second step, do not add polyoxyethylene glycol.Specifically refer to:
The preparation method of the present embodiment, comprises the steps:
The first step: according to quality proportioning, mixes tea oil 38kg, polydimethylsiloxane 13kg, ether of cellulose 26kg, graphite 14kg, dilinoleic acid palmitin 6kg, at 45 DEG C, stirs 30min, leaves standstill, cools, obtain mixture A;
Second step: by step one gained mixture A and polyacrylamide 20kg, glycerol 33kg mixing and stirring, stirring velocity 250r/min, to obtain final product.
reference examples 2
Be with the difference of embodiment 3: in second step, do not add polyoxyethylene glycol, specifically refer to:
The preparation method of the present embodiment, comprises the following steps:
The first step: according to quality proportioning, tea oil 38kg, polydimethylsiloxane 13kg, ether of cellulose 26kg, graphite 14kg, single stearic acid glycerine lipoprotein 25kg, dilinoleic acid palmitin 6kg are mixed, at 45 DEG C, stir 30min, leave standstill, cool, obtain mixture A;
Second step: by step one gained mixture A and polyacrylamide 20kg, glycerol 33kg mixing and stirring, stirring velocity 250r/min, to obtain final product.
performance test
Embodiment 1 to 6, reference examples 1 and 2 gained finished product are carried out performance test, test-results as in the table below:
Test-results is as shown in the table:
Embodiment 1 Embodiment 2 Embodiment 3 Embodiment 4 Embodiment 5 Embodiment 6 Reference examples 1 Reference examples 2
Frictional coefficient 0.120 0.119 0.120 0.118 0.117 0.118 0.148 0.157
Bacteriostasis rate/% 99.8 99.9 99.9 99.8 99.9 99.8 40 36
Antirust time/d 30 31 31 30 30 31 26 28
As can be seen from the table, compare by embodiment 3 can find out with reference examples 1, by the acting in conjunction of single stearic acid glycerine lipoprotein, polyoxyethylene glycol and other components, make finished product of the present invention have excellent oilness, biocidal property and rust-preventing characteristic; Embodiment 3 and reference examples 2 contrasts and can find out, polyoxyethylene glycol add the dispersiveness that effectively can improve lubricant, thus raising oilness, and effectively can also improve bacteriostasis property.

Claims (5)

1. an anti-bacterial lubricant, it is characterized in that, comprise the following raw material according to mass fraction meter: tea oil 36-40 part, polydimethylsiloxane 12-14 part, ether of cellulose 24-30 part, graphite 12-15 part, glyceryl monostearate 20-30 part, dilinoleic acid palmitin 5-8 part, polyacrylamide 15-26 part, polyoxyethylene glycol 20-24 part, glycerol 30-34 part.
2. anti-bacterial lubricant according to claim 1, it is characterized in that, comprise the following raw material according to mass fraction meter: tea oil 36-38 part, polydimethylsiloxane 12-13 part, ether of cellulose 24-26 part, graphite 12-14 part, glyceryl monostearate 20-25 part, dilinoleic acid palmitin 5-6 part, polyacrylamide 15-20 part, polyoxyethylene glycol 20-22 part, glycerol 30-33 part.
3. anti-bacterial lubricant according to claim 1, it is characterized in that, comprise the following raw material according to mass fraction meter: tea oil 38 parts, polydimethylsiloxane 13 parts, ether of cellulose 26 parts, 14 parts, graphite, glyceryl monostearate 25 parts, dilinoleic acid palmitin 6 parts, polyacrylamide 20 parts, polyoxyethylene glycol 22 parts, glycerol 33 parts.
4. the preparation method of anti-bacterial lubricant according to claim 1, is characterized in that, comprises the following steps:
The first step: according to quality proportioning, tea oil 36-40 part, polydimethylsiloxane 12-14 part, ether of cellulose 24-30 part, graphite 12-15 part, glyceryl monostearate 20-30 part, dilinoleic acid palmitin 5-8 part are mixed, 20-30min is stirred at 45-50 DEG C, leave standstill, cool, obtain mixture A;
Second step: by step one gained mixture A and polyacrylamide 15-26 part, polyoxyethylene glycol 20-24 part, glycerol 30-34 part mixing and stirring, stirring velocity 200-250r/min, to obtain final product.
5. the preparation method of anti-bacterial lubricant according to claim 4, is characterized in that, stirs 25min in step one at 50 DEG C.
CN201410293265.5A 2014-06-27 2014-06-27 A kind of anti-bacterial lubricant and preparation method thereof Active CN104031725B (en)

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CN106084634A (en) * 2016-06-30 2016-11-09 嘉兴市哈妮鞋业有限公司 Preparation rubber soles is with lubricator
CN106084635A (en) * 2016-06-30 2016-11-09 嘉兴市哈妮鞋业有限公司 Rubber soles preparation method with lubricator
CN106497646A (en) * 2016-09-13 2017-03-15 广西大学 A kind of antimicrobial antirust lubricant and preparation method thereof

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CN87102555A (en) * 1986-04-04 1987-10-14 隆察股份公司 The lubricant system of sheet material and bar and shape mill
CN103013630A (en) * 2012-12-06 2013-04-03 南通市华东润滑设备有限公司 Liquid lubricant
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CN103087811A (en) * 2011-11-07 2013-05-08 3M创新有限公司 Rustproof lubricating agent
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Inventor after: Hu Qingguang

Inventor before: Ding Yan

Inventor before: Gu Xiaohong

Inventor before: Pan Lin

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Effective date of registration: 20170517

Address after: 519050 Guangdong city in Zhuhai Province, South Bay Area town of Lejoin Road No. 8 (building)

Patentee after: Zhuhai Meihe Technology Co., Ltd.

Address before: 214000 Jiangsu province Wuxi chonganou Liberation Road No. 688

Patentee before: Wuxi City Chong'an District Technology Entrepreneurship Service Center