CN104030888B - A kind of high purity L-Borneol extraction element - Google Patents
A kind of high purity L-Borneol extraction element Download PDFInfo
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- CN104030888B CN104030888B CN201410241741.9A CN201410241741A CN104030888B CN 104030888 B CN104030888 B CN 104030888B CN 201410241741 A CN201410241741 A CN 201410241741A CN 104030888 B CN104030888 B CN 104030888B
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- time controling
- cooling tank
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
- C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2602/00—Systems containing two condensed rings
- C07C2602/36—Systems containing two condensed rings the rings having more than two atoms in common
- C07C2602/42—Systems containing two condensed rings the rings having more than two atoms in common the bicyclo ring system containing seven carbon atoms
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- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
A kind of high purity L-Borneol extraction element provided by the invention, comprises distiller, first cold bucket, whizzer, storage vat, rectifier, front cooling tank, distillation pot, rear cooling tank, strainer; Described distiller, first cold bucket, whizzer, storage vat, rectifier, front cooling tank, distillation pot, rear cooling tank, strainer successively pipeline connect, and are controlled by DCS system.The present invention: 1. whole plant integration runs, and avoids the pollution that pilot process brings, also avoids the loss of raw material in operation process greatly; 2. single Controlling System carries out entirety control, avoids the conflict in each side such as time, energy consumption, manpower consumptions between multiple Controlling System, has saved the energy greatly, reduced enterprise cost; 3. operation simplifies greatly, and 1 ~ 3 people can ensure the normal operation of whole plant, reduces the input of enterprise in manpower.
Description
Technical field
The present invention relates to a kind of high purity L-Borneol extraction element.
Background technology
For the extraction of L-Borneol in prior art, also do not have the device of a whole set of automatic operating, although patent " a kind of preparation method of L-Borneol and preparation apparatus (CN102423331B that my company applied in 2011, 2014.01.15) " provide a kind of preparation apparatus of L-Borneol, but this preparation apparatus does not provide the scheme of integrated a whole set of automatic operating, even the most basic integration does not also realize, to such an extent as in practice process, transient process between each equipment can cause great waste to raw material, and have great Pollution risk, and each equipment is independently arranged, then each equipment respectively has control device, and these control device all need independent energy consumption, the significant wastage of the energy can be caused thus.
Summary of the invention
For solving the problems of the technologies described above, the invention provides a kind of high purity L-Borneol extraction element, this high purity L-Borneol extraction element is controlled by integral structure, DCS system entirety, achieve a whole set of operation automatically of the integration of extracting for L-Borneol, seamless link between each equipment, avoids Pollution risk greatly, each equipment structure is in aggregates to be controlled, avoid the independent energy consumption of Controlling System, saved the energy greatly, and also greatly reduce the human cost of enterprise's needs input.
The present invention is achieved by the following technical programs.
A kind of high purity L-Borneol extraction element provided by the invention, comprises distiller, first cold bucket, whizzer, storage vat, rectifier, front cooling tank, distillation pot, rear cooling tank, strainer; Described distiller, first cold bucket, whizzer, storage vat, rectifier, front cooling tank, distillation pot, rear cooling tank, strainer successively pipeline connect, wherein distiller, rectifier, distillation pot are positioned at extreme lower position, and distiller, rectifier, distillation pot bottom are provided with heating unit; Described just cold bucket is arranged on whizzer top, and the outlet of first cold bucket and whizzer lead directly to; Described storage vat is also provided with feeding pump in being connected with the pipeline of rectifier; Described metre filter is realized by production board, and production board can take out from the side exit of strainer; Described filter bottom pipeline is connected to distillation pot side lower, and strainer is provided with reflux pump in being connected with the pipeline of distillation pot; Described front cooling tank is connected for one-way channel with the pipeline of distillation pot; Described front cooling tank and rear cooling tank share cooling water pipeline.
Described rectifier inside is provided with grid agitator.
Described distiller, first cold bucket, whizzer, storage vat, rectifier, front cooling tank, distillation pot, rear cooling tank, strainer are controlled by DCS system.
Described DCS system controls to connect in the following manner: initiating signal reception exports to walk abreast and accesses to time controling one, time controling two, time controling six; Time controling two exports and accesses to and door one; Export with door one and access to time controling three, time controling four simultaneously; Time controling three, time controling four export and access to that just cold bucket initiating signal controls, whizzer initiating signal controls respectively, and time controling three, time controling four export and also access to and door two; Export with door two and accessed to and door one by not gate, time controling five successively; Time controling six exports and accesses to the control of rectifier initiating signal, time controling seven simultaneously, and time controling seven exports and accesses to the control of distillation pot initiating signal, time controling eight simultaneously, and time controling eight exports and accesses to the control of strainer initiating signal.
Described initiating signal reception sends signal by operator and controls; Described distiller initiating signal controls the heating unit of distiller, described just cold bucket initiating signal controls the bottom valve of just cold bucket, described whizzer initiating signal controls the start and stop of whizzer, rectifier initiating signal controls the start and stop of feeding pump and rectifier, the start and stop of cooling tank, distillation pot before described distillation pot initiating signal controls, the overall start and stop of cooling tank, strainer, production board, reflux pump after described strainer initiating signal controls.
Beneficial effect of the present invention is: 1. whole plant integration runs, and avoids the pollution that pilot process brings, also avoids the loss of raw material in operation process greatly; 2. single Controlling System carries out entirety control, avoids the conflict in each side such as time, energy consumption, manpower consumptions between multiple Controlling System, has saved the energy greatly, reduced enterprise cost; 3. operation simplifies greatly, and 1 ~ 3 people can ensure the normal operation of whole plant, reduces the input of enterprise in manpower.
Accompanying drawing explanation
Fig. 1 is structural representation of the present invention;
Fig. 2 is the front view of Fig. 1;
Fig. 3 is the vertical view of Fig. 1;
Fig. 4 is the side-view of Fig. 1;
Fig. 5 is the connection diagram of Controlling System in the present invention;
In figure: 11-distiller, 12-is cold bucket just, 13-whizzer, 14-storage vat, 21-feeding pump, 22-rectifier, cooling tank before 23-, 24-distils pot, cooling tank after 31-, 32-strainer, 33-production board, 34-reflux pump, 100-initiating signal receives, 101-distiller initiating signal controls, 102-just cold bucket initiating signal controls, 103-whizzer initiating signal controls, 104-rectifier initiating signal controls, 105-distillation pot initiating signal controls, 106-strainer initiating signal controls, 201-time controling one, 202-time controling two, 203-time controling three, 204-time controling four, 205-time controling five, 206-time controling six, 207-time controling seven, 208-time controling eight, 301-and door one, 302-and door two, 303-not gate.
Embodiment
Further describe technical scheme of the present invention below, but described in claimed scope is not limited to.
A kind of high purity L-Borneol extraction element as shown in Figures 1 to 4, comprises distiller 11, first cold bucket 12, whizzer 13, storage vat 14, rectifier 22, front cooling tank 23, distillation pot 24, rear cooling tank 31, strainer 32; Described distiller 11, first cold bucket 12, whizzer 13, storage vat 14, rectifier 22, front cooling tank 23, distillation pot 24, rear cooling tank 31, strainer 32 successively pipeline connect, wherein distiller 11, rectifier 22, distillation pot 24 be positioned at extreme lower position, and distiller 11, rectifier 22, distillation pot 24 bottom be provided with heating unit; Described just cold bucket 12 is arranged on whizzer 13 top, and outlet and the whizzer 13 of first cold bucket 12 lead directly to; Feeding pump 21 is also provided with during described storage vat 14 is connected with the pipeline of rectifier 22; Described strainer 32 is filtered through production board 33 and realizes, and production board 33 can take out from the side exit of strainer 32; Described strainer 32 bottom pipe is connected to distillation pot 24 side lower, and strainer 32 is provided with reflux pump 34 in being connected with the pipeline of distillation pot 24; Described front cooling tank 23 is connected for one-way channel with the pipeline of distillation pot 24; Described front cooling tank 23 and rear cooling tank 31 share cooling water pipeline.
Described rectifier 22 inside is provided with grid agitator.
Described distiller 11, first cold bucket 12, whizzer 13, storage vat 14, rectifier 22, front cooling tank 23, distillation pot 24, rear cooling tank 31, strainer 32 are controlled by DCS system.
As shown in Figure 5, described DCS system controls to connect in the following manner: initiating signal reception 100 exports to walk abreast and accesses to time controling 1, time controling 2 202, time controling 6 206; Time controling 2 202 exports and accesses to and door 1; Export with door 1 and access to time controling 3 203, time controling 4 204 simultaneously; Time controling 3 203, time controling 4 204 export and access to just cold bucket initiating signal control 102, whizzer initiating signal control 103 respectively, and the output of time controling 3 203, time controling 4 204 also accesses to and door 2 302; Export with door 2 302 and accessed to and door 1 by not gate 303, time controling 5 205 successively; Time controling 6 206 exports and accesses to rectifier initiating signal control 104, time controling 7 207 simultaneously, time controling 7 207 exports and accesses to distillation pot initiating signal control 105, time controling 8 208 simultaneously, and time controling 8 208 exports and accesses to strainer initiating signal control 106.
Described initiating signal reception 100 sends signal by operator and controls; Described distiller initiating signal controls the heating unit that 101 control distiller 11, described just cold bucket initiating signal controls the bottom valve that 102 control just cold bucket 12, described whizzer initiating signal controls the start and stop that 103 control whizzer 13, rectifier initiating signal controls the start and stop that 104 control feeding pump 21 and rectifier 22, described distillation pot initiating signal controls the start and stop that 105 control front cooling tank 23, distillation pot 24, the overall start and stop of cooling tank 31, strainer 32, production board 33, reflux pump 34 after described strainer initiating signal control 106 controls.
Because whizzer 13 cannot run continuously, therefore just cold bucket 12 and whizzer 13 need intermitten service, mainly be just to store in cold bucket 12 and a certain amount ofly just cool finished product, then making it to enter into whizzer 13 carries out centrifugal, and whizzer 13 centrifugal after product introduction to storage vat 14, its follow-up feeding pump 21, rectifier 22, front cooling tank 23, distillation pot 24, rear cooling tank 31, the treating processes of strainer 32 can be carried out continuously, just only to need when startup on the guarantee time, and for the time controling that each major parts starts, then can pass through time controling 1 completely, time controling 2 202, time controling 3 203, time controling 4 204, time controling 5 205, time controling 6 206, time controling 7 207, time controling 8 208 these eight completes.
Therefore, the present invention in use, as long as set each parameter, initiating signal sends rear each parts and can extract according to setting-up time startup successively, with door 1, then can ensure that just cold bucket 12 and whizzer 13 are interrupted start and stop with door 2 302 and not gate 303, corresponding, when equipment need out of service to safeguard time, Controlling System also can ensure that each parts stop successively, thus ensures that raw material is not in a device wasted as far as possible.
Claims (3)
1. a high purity L-Borneol extraction element, comprise distiller (11), first cold bucket (12), whizzer (13), storage vat (14), rectifier (22), front cooling tank (23), distillation pot (24), rear cooling tank (31), strainer (32), it is characterized in that: described distiller (11), first cold bucket (12), whizzer (13), storage vat (14), rectifier (22), front cooling tank (23), distillation pot (24), rear cooling tank (31), strainer (32) successively pipeline connects, wherein distiller (11), rectifier (22), distillation pot (24) is positioned at extreme lower position, and distiller (11), rectifier (22), distillation pot (24) bottom is provided with heating unit, described just cold bucket (12) is arranged on whizzer (13) top, and the outlet of first cold bucket (12) and whizzer (13) lead directly to, described storage vat (14) is also provided with feeding pump (21) in being connected with the pipeline of rectifier (22), described strainer (32) is filtered through production board (33) and realizes, and production board (33) can take out from the side exit of strainer (32), described strainer (32) bottom pipe is connected to distillation pot (24) side lower, and strainer (32) is provided with reflux pump (34) in being connected with the pipeline of distillation pot (24), described front cooling tank (23) is connected with the pipeline of distillation pot (24) for one-way channel, described front cooling tank (23) and rear cooling tank (31) share cooling water pipeline,
Described distiller (11), first cold bucket (12), whizzer (13), storage vat (14), rectifier (22), front cooling tank (23), distillation pot (24), rear cooling tank (31), strainer (32) are controlled by DCS system;
Described DCS system controls to connect in the following manner: initiating signal reception (100) exports to walk abreast and accesses to time controling one (201), time controling two (202), time controling six (206); Time controling two (202) exports and accesses to and door one (301); Export with door one (301) and access to time controling three (203), time controling four (204) simultaneously; Time controling three (203), time controling four (204) export and access to just cold bucket initiating signal control (102), whizzer initiating signal control (103) respectively, and the output of time controling three (203), time controling four (204) also accesses to and door two (302); Export with door two (302) and accessed to and door one (301) by not gate (303), time controling five (205) successively; Time controling six (206) exports and accesses to the control of rectifier initiating signal (104), time controling seven (207) simultaneously, time controling seven (207) exports and accesses to the control of distillation pot initiating signal (105), time controling eight (208) simultaneously, and time controling eight (208) exports and accesses to strainer initiating signal control (106).
2. high purity L-Borneol extraction element as claimed in claim 1, is characterized in that: described rectifier (22) inside is provided with grid agitator.
3. high purity L-Borneol extraction element as claimed in claim 1 or 2, is characterized in that: described initiating signal reception (100) sends signal by operator and controls, described distiller initiating signal controls the heating unit that (101) control distiller (11), described just cold bucket initiating signal controls the bottom valve that (102) control just cold bucket (12), described whizzer initiating signal controls the start and stop that (103) control whizzer (13), rectifier initiating signal controls the start and stop that (104) control feeding pump (21) and rectifier (22), described distillation pot initiating signal controls (105) and controls front cooling tank (23), the start and stop of distillation pot (24), described strainer initiating signal controls (106) and controls rear cooling tank (31), strainer (32), production board (33), the overall start and stop of reflux pump (34).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410241741.9A CN104030888B (en) | 2014-06-03 | 2014-06-03 | A kind of high purity L-Borneol extraction element |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410241741.9A CN104030888B (en) | 2014-06-03 | 2014-06-03 | A kind of high purity L-Borneol extraction element |
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| Publication Number | Publication Date |
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| CN104030888A CN104030888A (en) | 2014-09-10 |
| CN104030888B true CN104030888B (en) | 2015-12-09 |
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| CN201410241741.9A Active CN104030888B (en) | 2014-06-03 | 2014-06-03 | A kind of high purity L-Borneol extraction element |
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN201334471Y (en) * | 2009-01-21 | 2009-10-28 | 中国热带农业科学院热带作物品种资源研究所 | Blumea balsamifera powder extracting device |
| CN201485438U (en) * | 2009-09-14 | 2010-05-26 | 中国热带农业科学院热带作物品种资源研究所 | Blumea balsamifera processing and extracting equipment |
| CN102423331A (en) * | 2011-12-06 | 2012-04-25 | 江口县苗药生物科技有限公司 | Method and equipment for preparing borneol flakes |
| CN102557881A (en) * | 2010-12-09 | 2012-07-11 | 江南大学 | Method for extraction and separation purification of blumea balsamifera (L.)DC. sheets |
| CN203513533U (en) * | 2013-11-01 | 2014-04-02 | 宜昌万森生态科技发展有限公司 | Natural borneol extraction device |
| CN203960089U (en) * | 2014-06-03 | 2014-11-26 | 江口县苗药生物科技有限公司 | A kind of high purity L-Borneol extraction element |
-
2014
- 2014-06-03 CN CN201410241741.9A patent/CN104030888B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN201334471Y (en) * | 2009-01-21 | 2009-10-28 | 中国热带农业科学院热带作物品种资源研究所 | Blumea balsamifera powder extracting device |
| CN201485438U (en) * | 2009-09-14 | 2010-05-26 | 中国热带农业科学院热带作物品种资源研究所 | Blumea balsamifera processing and extracting equipment |
| CN102557881A (en) * | 2010-12-09 | 2012-07-11 | 江南大学 | Method for extraction and separation purification of blumea balsamifera (L.)DC. sheets |
| CN102423331A (en) * | 2011-12-06 | 2012-04-25 | 江口县苗药生物科技有限公司 | Method and equipment for preparing borneol flakes |
| CN203513533U (en) * | 2013-11-01 | 2014-04-02 | 宜昌万森生态科技发展有限公司 | Natural borneol extraction device |
| CN203960089U (en) * | 2014-06-03 | 2014-11-26 | 江口县苗药生物科技有限公司 | A kind of high purity L-Borneol extraction element |
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| CN104030888A (en) | 2014-09-10 |
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