CN104004496B - Preparation method of reduced graphene oxide/nickel oxide composite wave-absorbing material - Google Patents
Preparation method of reduced graphene oxide/nickel oxide composite wave-absorbing material Download PDFInfo
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- CN104004496B CN104004496B CN201410173989.6A CN201410173989A CN104004496B CN 104004496 B CN104004496 B CN 104004496B CN 201410173989 A CN201410173989 A CN 201410173989A CN 104004496 B CN104004496 B CN 104004496B
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- Prior art keywords
- graphene
- absorbing material
- nickel oxide
- composite wave
- oxide composite
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- 229910021389 graphene Inorganic materials 0.000 title claims abstract description 65
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims abstract description 64
- 239000002131 composite material Substances 0.000 title claims abstract description 33
- 229910000480 nickel oxide Inorganic materials 0.000 title claims abstract description 27
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 239000011358 absorbing material Substances 0.000 title claims abstract description 16
- 239000012300 argon atmosphere Substances 0.000 claims abstract description 6
- 239000002105 nanoparticle Substances 0.000 claims abstract description 6
- 239000000463 material Substances 0.000 claims description 26
- 239000000243 solution Substances 0.000 claims description 16
- 238000000197 pyrolysis Methods 0.000 claims description 12
- 238000002156 mixing Methods 0.000 claims description 11
- AIYYMMQIMJOTBM-UHFFFAOYSA-L nickel(ii) acetate Chemical compound [Ni+2].CC([O-])=O.CC([O-])=O AIYYMMQIMJOTBM-UHFFFAOYSA-L 0.000 claims description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 239000007864 aqueous solution Substances 0.000 claims description 7
- 239000007795 chemical reaction product Substances 0.000 claims description 3
- 238000003760 magnetic stirring Methods 0.000 claims description 3
- 239000000047 product Substances 0.000 claims description 2
- 238000010521 absorption reaction Methods 0.000 abstract description 6
- GNRSAWUEBMWBQH-UHFFFAOYSA-N oxonickel Chemical compound [Ni]=O GNRSAWUEBMWBQH-UHFFFAOYSA-N 0.000 abstract description 4
- MQRWBMAEBQOWAF-UHFFFAOYSA-N acetic acid;nickel Chemical compound [Ni].CC(O)=O.CC(O)=O MQRWBMAEBQOWAF-UHFFFAOYSA-N 0.000 abstract 1
- 238000004108 freeze drying Methods 0.000 abstract 1
- 239000002135 nanosheet Substances 0.000 abstract 1
- 229940078494 nickel acetate Drugs 0.000 abstract 1
- 239000002245 particle Substances 0.000 abstract 1
- 239000000203 mixture Substances 0.000 description 6
- 239000011159 matrix material Substances 0.000 description 5
- 238000001035 drying Methods 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 238000013019 agitation Methods 0.000 description 3
- 230000008014 freezing Effects 0.000 description 3
- 238000007710 freezing Methods 0.000 description 3
- 229940078487 nickel acetate tetrahydrate Drugs 0.000 description 3
- OINIXPNQKAZCRL-UHFFFAOYSA-L nickel(2+);diacetate;tetrahydrate Chemical compound O.O.O.O.[Ni+2].CC([O-])=O.CC([O-])=O OINIXPNQKAZCRL-UHFFFAOYSA-L 0.000 description 3
- 229910052573 porcelain Inorganic materials 0.000 description 3
- 238000010792 warming Methods 0.000 description 3
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 2
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 description 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- UBEWDCMIDFGDOO-UHFFFAOYSA-N cobalt(2+);cobalt(3+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[O-2].[Co+2].[Co+3].[Co+3] UBEWDCMIDFGDOO-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 229910001416 lithium ion Inorganic materials 0.000 description 2
- VWDWKYIASSYTQR-UHFFFAOYSA-N sodium nitrate Chemical compound [Na+].[O-][N+]([O-])=O VWDWKYIASSYTQR-UHFFFAOYSA-N 0.000 description 2
- 239000002250 absorbent Substances 0.000 description 1
- 230000002745 absorbent Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008033 biological extinction Effects 0.000 description 1
- 239000003575 carbonaceous material Substances 0.000 description 1
- 238000001311 chemical methods and process Methods 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 230000005669 field effect Effects 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 238000001027 hydrothermal synthesis Methods 0.000 description 1
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N iron oxide Inorganic materials [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910044991 metal oxide Inorganic materials 0.000 description 1
- 150000004706 metal oxides Chemical class 0.000 description 1
- 239000002086 nanomaterial Substances 0.000 description 1
- 239000002073 nanorod Substances 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- NDLPOXTZKUMGOV-UHFFFAOYSA-N oxo(oxoferriooxy)iron hydrate Chemical compound O.O=[Fe]O[Fe]=O NDLPOXTZKUMGOV-UHFFFAOYSA-N 0.000 description 1
- 229920000767 polyaniline Polymers 0.000 description 1
- 239000012286 potassium permanganate Substances 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 229940001516 sodium nitrate Drugs 0.000 description 1
- 235000010344 sodium nitrate Nutrition 0.000 description 1
- 239000004317 sodium nitrate Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
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Abstract
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CN201410173989.6A CN104004496B (en) | 2014-04-26 | 2014-04-26 | Preparation method of reduced graphene oxide/nickel oxide composite wave-absorbing material |
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CN201410173989.6A CN104004496B (en) | 2014-04-26 | 2014-04-26 | Preparation method of reduced graphene oxide/nickel oxide composite wave-absorbing material |
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CN104004496A CN104004496A (en) | 2014-08-27 |
CN104004496B true CN104004496B (en) | 2015-11-18 |
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CN201410173989.6A Expired - Fee Related CN104004496B (en) | 2014-04-26 | 2014-04-26 | Preparation method of reduced graphene oxide/nickel oxide composite wave-absorbing material |
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Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104690289A (en) * | 2015-01-12 | 2015-06-10 | 冯丹 | Graphene-nano-nickel wave-absorbing material |
CN105023762B (en) * | 2015-08-10 | 2017-11-14 | 安徽建筑大学 | A kind of foliaceous CuO NiO composite construction nano materials and preparation method thereof |
CN109054710A (en) * | 2018-07-05 | 2018-12-21 | 广东石成科技有限公司 | A kind of graphene composite material and preparation method and its application as magnetic-conductive adhesive |
CN111218189B (en) * | 2018-11-26 | 2022-07-08 | 西安光启尖端技术研究院 | Resistive film and preparation method and application thereof |
CN112165848A (en) * | 2020-09-27 | 2021-01-01 | 晋中学院 | Composite wave-absorbing material with magnetic metal or oxide thereof loaded on graphene and preparation method thereof |
CN113823919B (en) * | 2021-09-24 | 2023-01-03 | 中南大学 | Light nickel/nickel oxide assembled graphene-based composite low-frequency wave-absorbing foam and preparation method thereof |
CN114784227B (en) * | 2022-04-12 | 2024-03-29 | 中国科学院电工研究所 | Graphene/metal oxide composite nano material, preparation method and application thereof, electrode plate and application thereof |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101733985A (en) * | 2009-12-23 | 2010-06-16 | 天津大学 | Graphene/nickel oxide laminated-structure composite film and preparation method thereof |
CN102184781A (en) * | 2011-03-03 | 2011-09-14 | 上海大学 | Nano-nickel oxide/graphene composite material and preparation method thereof |
CN102769124A (en) * | 2012-07-12 | 2012-11-07 | 上海大学 | Graphene-supported octahedral nickel oxide composite material and preparation method thereof |
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2014
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Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101733985A (en) * | 2009-12-23 | 2010-06-16 | 天津大学 | Graphene/nickel oxide laminated-structure composite film and preparation method thereof |
CN102184781A (en) * | 2011-03-03 | 2011-09-14 | 上海大学 | Nano-nickel oxide/graphene composite material and preparation method thereof |
CN102769124A (en) * | 2012-07-12 | 2012-11-07 | 上海大学 | Graphene-supported octahedral nickel oxide composite material and preparation method thereof |
Non-Patent Citations (1)
Title |
---|
Bifunctional Reduced Graphene Oxide/V2O5 Composite Hydrogel: Fabrication, High Performance as Electromagnetic Wave Absorbent and Supercapacitor;Hui Zhang,等;《ChemPhysChem》;20131206;第15卷(第2期);第366-373页 * |
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Effective date of registration: 20180611 Address after: 510000 1402 office building, 383 office building, Panyu Avenue North, Panyu District Town, Guangzhou, Guangdong, Panyu, China Patentee after: Guangzhou Intellectual Property Service Co., Ltd. Address before: No. 111, Kowloon Road, Hefei, Anhui, Anhui Patentee before: Anhui University |
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Effective date of registration: 20180622 Address after: 102202 Li Zhuang village, Nan Kou Town, Changping District, Beijing Patentee after: Beijing juntong New Material Technology Co., Ltd. Address before: 510000 1402 office building, 383 office building, Panyu Avenue North, Panyu District Town, Guangzhou, Guangdong, Panyu, China Patentee before: Guangzhou Intellectual Property Service Co., Ltd. |
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Granted publication date: 20151118 Termination date: 20190426 |