CN104001467A - Self-control reaction kettle - Google Patents

Self-control reaction kettle Download PDF

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Publication number
CN104001467A
CN104001467A CN201410184548.6A CN201410184548A CN104001467A CN 104001467 A CN104001467 A CN 104001467A CN 201410184548 A CN201410184548 A CN 201410184548A CN 104001467 A CN104001467 A CN 104001467A
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CN
China
Prior art keywords
self
shaft
stirring shaft
hollow
stirrer
Prior art date
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Granted
Application number
CN201410184548.6A
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Chinese (zh)
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CN104001467B (en
Inventor
周加兵
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
TONGLING QIANYI CHEMICAL EQUIPMENT CO Ltd
Original Assignee
TONGLING QIANYI CHEMICAL EQUIPMENT CO Ltd
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Application filed by TONGLING QIANYI CHEMICAL EQUIPMENT CO Ltd filed Critical TONGLING QIANYI CHEMICAL EQUIPMENT CO Ltd
Priority to CN201410184548.6A priority Critical patent/CN104001467B/en
Publication of CN104001467A publication Critical patent/CN104001467A/en
Application granted granted Critical
Publication of CN104001467B publication Critical patent/CN104001467B/en
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  • Mixers With Rotating Receptacles And Mixers With Vibration Mechanisms (AREA)

Abstract

A disclosed self-control reaction kettle comprises a motor, a stirring shaft and a reaction container; the stirring shaft is fixedly installed on the motor and is arranged in the reaction container; the connection part of the stirring shaft and the reaction container is provided with an electromagnetic block, a magnet is arranged on the stirring shaft, and the gap between the electromagnetic block and the magnet is provided with a rubber sealing ring; the stirring shaft is a hollow pipe, the upper end part is provided with a gas suction opening, and the lower end part is provided with a self-suction type stirrer and a propeller agitator; the propeller agitator is arranged at the lowest end of the stirring shaft; the reaction container is inside provided with multiple hollow shafts; and each hollow shaft is provided with a water inlet and a water outlet. The self-control reaction kettle overcomes the disadvantages of the prior art, and is simple in design and reasonable in structure. Magnetic-coupling static sealing is employed, when the hollow stirring shaft rotates, the generated centrifugal force enables the interior of the stirrer to generate self suction, so that the interior of the self-suction stirrer forms a negative-pressure area, while the interior of the self-suction stirrer is communicated with a gas phase through the hollow structure, so that gas above a liquid level is continuously sucked into the stirrer and dispersed into the liquid phase again, and thus stirring reaction is sufficient and the reaction speed is improved.

Description

A kind of automatic control reactor
Technical field
The present invention relates to reactor technical field, specifically belong to a kind of automatic control reactor.
Background technology
The test of now using is mainly comprised of there-necked flask, heating jacket, thermometer, condenser pipe and agitating device with reactor.Assembling process between these equipment is loaded down with trivial details, and the reactor control accuracy after assembling is low.In the assembly of reactor, due to a large amount of use glass apparatus, not only inconvenience is cleaned, and also makes the expensive of reactor simultaneously, and again because glassware is frangible, also reduce the service life of reactor.Existing reactor in use, adds the mode of thermal recovery for heating every sky to heating jacket, this makes thermal energy loss greatly.
Summary of the invention
The object of this invention is to provide a kind of automatic control reactor, the deficiencies in the prior art have been overcome, simplicity of design, rational in infrastructure, adopt the sealing of magnetic couple static, when the shaft of boring rotates, the centrifugal force producing produces self-priming to agitator inside, make the inner negative pressuren zone that forms of self-absorbing type stirrer, and self-absorbing type stirrer inside is connected with gas phase by hollow, thereby make the gas on liquid level be inhaled into agitator continuously and again be scattered in liquid phase, stirring reaction is abundant, improve reaction speed.
The technical solution used in the present invention is as follows:
A kind of automatic control reactor, comprise motor, shaft and reaction vessel, shaft is installed on motor, shaft is arranged in reaction vessel, described shaft and reaction vessel junction are provided with electromagnetic block, stirring is provided with magnet, between magnet and electromagnetic block, gap is provided with rubber seal, described shaft is hollow tube, upper end is provided with gas inlet scoop, and bottom is provided with self-absorbing type stirrer and propeller agitator, and propeller agitator at shaft bottom, in reaction vessel, be provided with a plurality of hollow shafts, hollow shaft is provided with water inlet and delivery port.
Described inlet scoop is provided with moving blade.
Described self-absorbing type stirrer is provided with heat transfer plate.
Compared with the prior art, beneficial effect of the present invention is as follows:
The present invention adopts the sealing of magnetic couple static, when motor passes through to drive the shaft rotation of boring, shaft drives near the fluid of agitator to circle under the effect of impeller, the centrifugal force producing produces self-priming to agitator inside, make the inner negative pressuren zone that forms of self-absorbing type stirrer, and self-absorbing type stirrer inside is connected with gas phase by hollow, thereby make the gas on liquid level be inhaled into agitator continuously and again be scattered in liquid phase, stirring reaction is abundant, improves reaction speed.
Accompanying drawing explanation
Fig. 1 is structural representation of the present invention.
The specific embodiment
Referring to accompanying drawing, a kind of automatic control reactor, comprise motor 1, shaft 2 and reaction vessel 3, shaft 2 is installed on motor 1, shaft 2 is arranged in reaction vessel 3, described shaft 2 is provided with electromagnetic block 4 with reaction vessel 3 junctions, stirring is provided with magnet 5, between magnet 5 and electromagnetic block 4, gap is provided with rubber seal 6, described shaft is hollow tube, bottom is provided with self-absorbing type stirrer 7 and propeller agitator 8, propeller agitator at shaft bottom, in reaction vessel, be provided with a plurality of hollow shafts 9, hollow shaft is provided with water inlet 901 and delivery port 902, shaft upper end is provided with gas inlet scoop 201, inlet scoop is provided with moving blade 202, moving blade drives lower end to turn at air-flow, the air improving outside hollow shaft is inhaled in negative axocoel, self-absorbing type stirrer 7 is provided with heat transfer plate 701, improve its heat transfer speed, be convenient to control reaction.

Claims (3)

1. an automatic control reactor, comprise motor, shaft and reaction vessel, shaft is installed on motor, shaft is arranged in reaction vessel, it is characterized in that: described shaft and reaction vessel junction are provided with electromagnetic block, stirring is provided with magnet, between magnet and electromagnetic block, gap is provided with rubber seal, described shaft is hollow tube, upper end is provided with gas inlet scoop, bottom is provided with self-absorbing type stirrer and propeller agitator, propeller agitator at shaft bottom, in reaction vessel, be provided with a plurality of hollow shafts, hollow shaft is provided with water inlet and delivery port.
2. a kind of automatic control reactor according to claim 1, is characterized in that: described inlet scoop is provided with moving blade.
3. a kind of automatic control reactor according to claim 1, is characterized in that: described self-absorbing type stirrer is provided with heat transfer plate.
CN201410184548.6A 2014-05-01 2014-05-01 A kind of automatic control reactor Active CN104001467B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201410184548.6A CN104001467B (en) 2014-05-01 2014-05-01 A kind of automatic control reactor

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201410184548.6A CN104001467B (en) 2014-05-01 2014-05-01 A kind of automatic control reactor

Publications (2)

Publication Number Publication Date
CN104001467A true CN104001467A (en) 2014-08-27
CN104001467B CN104001467B (en) 2016-08-24

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Family Applications (1)

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CN201410184548.6A Active CN104001467B (en) 2014-05-01 2014-05-01 A kind of automatic control reactor

Country Status (1)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104725236A (en) * 2015-01-28 2015-06-24 浙江丰虹新材料股份有限公司 Water-based production method of alkyl quaternary ammonium salt and production device thereof
CN105344277A (en) * 2015-10-27 2016-02-24 王明明 Industrial stirring and drying device
RU174080U1 (en) * 2017-06-05 2017-09-29 Автономная некоммерческая организация высшего образования "Белгородский университет кооперации, экономики и права" PLANT FOR SYNTHESIS OF CHEMICAL ADDITIVES
CN108126552A (en) * 2017-11-27 2018-06-08 河南后羿制药有限公司 A kind of agitating shaft and application suitable for hydrogenation
CN112717816A (en) * 2020-12-30 2021-04-30 赵小林 Urea mixing arrangement with real-time detection function

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2010126556A (en) * 2008-11-25 2010-06-10 Panasonic Electric Works Co Ltd Plastic decomposition apparatus
CN202823366U (en) * 2012-09-07 2013-03-27 浙江振华新能源科技有限公司 Reaction still used for preparing spherical ferric phosphate
CN203002341U (en) * 2012-12-20 2013-06-19 杭州索孚机械有限公司 Novel efficient self-suction type stirrer for gas-liquid-solid three-phase mixing
CN203790947U (en) * 2014-05-01 2014-08-27 铜陵钱谊化工设备有限责任公司 Automatic control reaction kettle

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2010126556A (en) * 2008-11-25 2010-06-10 Panasonic Electric Works Co Ltd Plastic decomposition apparatus
CN202823366U (en) * 2012-09-07 2013-03-27 浙江振华新能源科技有限公司 Reaction still used for preparing spherical ferric phosphate
CN203002341U (en) * 2012-12-20 2013-06-19 杭州索孚机械有限公司 Novel efficient self-suction type stirrer for gas-liquid-solid three-phase mixing
CN203790947U (en) * 2014-05-01 2014-08-27 铜陵钱谊化工设备有限责任公司 Automatic control reaction kettle

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
陈志平等: "《搅拌与混合设备设计选用手册》", 31 May 2004, 化学工业出版社 *

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104725236A (en) * 2015-01-28 2015-06-24 浙江丰虹新材料股份有限公司 Water-based production method of alkyl quaternary ammonium salt and production device thereof
CN105344277A (en) * 2015-10-27 2016-02-24 王明明 Industrial stirring and drying device
RU174080U1 (en) * 2017-06-05 2017-09-29 Автономная некоммерческая организация высшего образования "Белгородский университет кооперации, экономики и права" PLANT FOR SYNTHESIS OF CHEMICAL ADDITIVES
CN108126552A (en) * 2017-11-27 2018-06-08 河南后羿制药有限公司 A kind of agitating shaft and application suitable for hydrogenation
CN112717816A (en) * 2020-12-30 2021-04-30 赵小林 Urea mixing arrangement with real-time detection function

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