CN103937399A - Harmful substance adsorbing coating and preparation method thereof - Google Patents
Harmful substance adsorbing coating and preparation method thereof Download PDFInfo
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- CN103937399A CN103937399A CN201410107247.3A CN201410107247A CN103937399A CN 103937399 A CN103937399 A CN 103937399A CN 201410107247 A CN201410107247 A CN 201410107247A CN 103937399 A CN103937399 A CN 103937399A
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- coating
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- 239000011248 coating agent Substances 0.000 title claims abstract description 25
- 238000000576 coating method Methods 0.000 title claims abstract description 25
- 238000002360 preparation method Methods 0.000 title claims description 7
- 239000000126 substance Substances 0.000 title abstract description 4
- SWXVUIWOUIDPGS-UHFFFAOYSA-N diacetone alcohol Chemical compound CC(=O)CC(C)(C)O SWXVUIWOUIDPGS-UHFFFAOYSA-N 0.000 claims abstract description 14
- DKPFZGUDAPQIHT-UHFFFAOYSA-N Butyl acetate Natural products CCCCOC(C)=O DKPFZGUDAPQIHT-UHFFFAOYSA-N 0.000 claims abstract description 13
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000002808 molecular sieve Substances 0.000 claims abstract description 9
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 claims abstract description 9
- JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 claims abstract description 8
- HQKMJHAJHXVSDF-UHFFFAOYSA-L magnesium stearate Chemical compound [Mg+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O HQKMJHAJHXVSDF-UHFFFAOYSA-L 0.000 claims abstract description 8
- 229920001225 polyester resin Polymers 0.000 claims abstract description 7
- 239000004645 polyester resin Substances 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 229920002367 Polyisobutene Polymers 0.000 claims abstract description 4
- GBAOBIBJACZTNA-UHFFFAOYSA-L calcium sulfite Chemical compound [Ca+2].[O-]S([O-])=O GBAOBIBJACZTNA-UHFFFAOYSA-L 0.000 claims abstract description 4
- 235000010261 calcium sulphite Nutrition 0.000 claims abstract description 4
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 4
- 235000019359 magnesium stearate Nutrition 0.000 claims abstract description 4
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 claims description 18
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 18
- 238000003756 stirring Methods 0.000 claims description 18
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 12
- 239000012535 impurity Substances 0.000 claims description 11
- -1 methyl-isobutyl Chemical group 0.000 claims description 10
- 150000002148 esters Chemical class 0.000 claims description 9
- 239000000741 silica gel Substances 0.000 claims description 7
- 229910002027 silica gel Inorganic materials 0.000 claims description 7
- PSGCQDPCAWOCSH-UHFFFAOYSA-N (4,7,7-trimethyl-3-bicyclo[2.2.1]heptanyl) prop-2-enoate Chemical compound C1CC2(C)C(OC(=O)C=C)CC1C2(C)C PSGCQDPCAWOCSH-UHFFFAOYSA-N 0.000 claims description 6
- WSLDOOZREJYCGB-UHFFFAOYSA-N 1,2-Dichloroethane Chemical compound ClCCCl WSLDOOZREJYCGB-UHFFFAOYSA-N 0.000 claims description 6
- DAKWPKUUDNSNPN-UHFFFAOYSA-N Trimethylolpropane triacrylate Chemical compound C=CC(=O)OCC(CC)(COC(=O)C=C)COC(=O)C=C DAKWPKUUDNSNPN-UHFFFAOYSA-N 0.000 claims description 6
- 239000012752 auxiliary agent Substances 0.000 claims description 6
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 6
- 150000002576 ketones Chemical class 0.000 claims description 6
- PBOSTUDLECTMNL-UHFFFAOYSA-N lauryl acrylate Chemical compound CCCCCCCCCCCCOC(=O)C=C PBOSTUDLECTMNL-UHFFFAOYSA-N 0.000 claims description 6
- 229920001084 poly(chloroprene) Polymers 0.000 claims description 6
- 229920000728 polyester Polymers 0.000 claims description 6
- 229920002803 thermoplastic polyurethane Polymers 0.000 claims description 6
- NKFIBMOQAPEKNZ-UHFFFAOYSA-N 5-amino-1h-indole-2-carboxylic acid Chemical compound NC1=CC=C2NC(C(O)=O)=CC2=C1 NKFIBMOQAPEKNZ-UHFFFAOYSA-N 0.000 claims description 3
- 239000003109 Disodium ethylene diamine tetraacetate Substances 0.000 claims description 3
- 239000004721 Polyphenylene oxide Substances 0.000 claims description 3
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 3
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 claims description 3
- 229910021502 aluminium hydroxide Inorganic materials 0.000 claims description 3
- 238000006243 chemical reaction Methods 0.000 claims description 3
- 238000004581 coalescence Methods 0.000 claims description 3
- 239000007822 coupling agent Substances 0.000 claims description 3
- 235000019301 disodium ethylene diamine tetraacetate Nutrition 0.000 claims description 3
- UHESRSKEBRADOO-UHFFFAOYSA-N ethyl carbamate;prop-2-enoic acid Chemical compound OC(=O)C=C.CCOC(N)=O UHESRSKEBRADOO-UHFFFAOYSA-N 0.000 claims description 3
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 claims description 3
- 238000000034 method Methods 0.000 claims description 3
- 229920006380 polyphenylene oxide Polymers 0.000 claims description 3
- 238000001132 ultrasonic dispersion Methods 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 3
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical compound [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 abstract description 2
- 229910002012 Aerosil® Inorganic materials 0.000 abstract 2
- NTIZESTWPVYFNL-UHFFFAOYSA-N Methyl isobutyl ketone Chemical compound CC(C)CC(C)=O NTIZESTWPVYFNL-UHFFFAOYSA-N 0.000 abstract 1
- UIHCLUNTQKBZGK-UHFFFAOYSA-N Methyl isobutyl ketone Natural products CCC(C)C(C)=O UIHCLUNTQKBZGK-UHFFFAOYSA-N 0.000 abstract 1
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 abstract 1
- 239000012948 isocyanate Substances 0.000 abstract 1
- 150000002513 isocyanates Chemical class 0.000 abstract 1
- 229920005749 polyurethane resin Polymers 0.000 abstract 1
- 238000001179 sorption measurement Methods 0.000 abstract 1
- 230000032683 aging Effects 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000004568 cement Substances 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000003628 erosive effect Effects 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 230000000750 progressive effect Effects 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
Abstract
The invention relates to a harmful substance adsorbing coating, which is prepared from the following raw materials by weight part: 8-10 of polyurethane resin, 34-37 of linear polyester resin, 13-15 of isocyanate, 10-15 of butyl acetate, 6-9 of methyl isobutyl ketone, 3-5 of aerosil, 1-2 of magnesium stearate, 2-4 of ethylenediamine tetraacetic acid disodium salt, 13-16 of diacetone alcohol, 3-4 of cyclohexanone, 5-8 of a molecular sieve, 3-5 of polyisobutylene, 2-4 of calcium sulfite, 0.4-0.5 of a leveling agent, and 4-6 of an adhesion assistant. The coating provided by the invention has the advantages of good adhesion, strong versatility, good weather resistance and flexibility, high tear strength, and good water resistance. At the same time, by adding the molecular sieve and aerosil, the adsorption properties of the coating are increased, so that the coating can adsorb harmful substances. Also, the adhesion of the coating is increased.
Description
Technical field
The invention belongs to paint field, relate in particular to and a kind ofly can adsorb objectionable impurities coating and preparation method thereof.
Background technology
The use field of coating is a lot of now, owing to being often exposed among atmosphere, be subject to the erosion of oxygen, moisture etc., easily cause the phenomenons such as corrosion of metal, foxy, cement weathering, raising along with people's living standard, requirement to coating each side all increases, especially more and more higher to the requirement of the aspects such as performance such as the hardness of coating, wear resistance, fullness ratio, shock-resistance, ageing resistance, anticorrosion, waterproof, grease proofing, chemicals-resistant, fast light, heatproof, therefore need the more progressive coating of research to meet people's needs.
Summary of the invention
The object of the present invention is to provide and a kind ofly can adsorb objectionable impurities coating and preparation method thereof, this coating characteristic is that sticking power is good, highly versatile, and weather resisteant, snappiness is good, tear strength is high, water tolerance is better, can adsorb objectionable impurities.
Technical scheme of the present invention is as follows:
Can adsorb an objectionable impurities coating, it is characterized in that being made by the raw material of following weight part: urethane resin 8-10, linear polyester resin 34-37, isocyanic ester 13-15, N-BUTYL ACETATE 10-15, methyl-isobutyl (first) ketone 6-9, micropowder silica gel 3-5, Magnesium Stearate 1-2, disodium ethylene diamine tetraacetate 2-4, diacetone alcohol 13-16, pimelinketone 3-4, molecular sieve 5-8, polyisobutene 3-5, calcium sulfite 2-4, flow agent 0.4-0.5, adhere to auxiliary agent 4-6;
The described auxiliary agent that adheres to is made by the raw material of following weight part: isobornyl acrylate 5-7, Viscoat 295 5-7, lauryl acrylate 4-7, chloroprene rubber 6-8, polyester glycol 7-9, polyphenylene oxide 2-3, aluminium hydroxide 0.1-0.2, alcohol ester 12 film coalescence aid 5-7, titanate coupling agent TMC-TTS0.6-1, calcium naphthenate 1-2, ethylene dichloride 8-13, methylethylketone 8-11, isocyanic ester 2-3, ethyl acetate 5-8, toxilic acid 1-2, urethane acrylate 4-5; Making method is: methylethylketone, ethylene dichloride, ethyl acetate are mixed, under 4000-6000 rev/min, add Viscoat 295, chloroprene rubber, after dissolving, add again isobornyl acrylate, lauryl acrylate, polyester glycol, stir 40-60 minute, add other remaining components, be heated to 80-90 ℃, stirring reaction 40-60 minute, obtains.
The described preparation method that can adsorb objectionable impurities coating, is characterized in that comprising the following steps:
(1) prepare A component: N-BUTYL ACETATE, methyl-isobutyl (first) ketone are mixed, under 4000-6000 rev/min, add molecular sieve, micropowder silica gel, stir 10-15 minute, add again linear polyester resin, stir 1-2 hour, ultrasonic dispersion 6-9 minute, makes A component;
(2) prepare B component: in airtight agitator, diacetone alcohol, pimelinketone are mixed, under 4000-6000 rev/min, add urethane resin, isocyanic ester, stir 50-70 minute, make B component;
(3) other remaining components are mixed, add A component and B component, stir 30-40 minute, obtain.
Beneficial effect of the present invention
Coating characteristic of the present invention is that sticking power is good, highly versatile, and weather resisteant, snappiness is good, tear strength is high, water tolerance is better; By adding molecular sieve, micropowder silica gel, increased the absorption property of coating simultaneously, can adsorb objectionable impurities, and increase the cohesiveness of coating.
Embodiment
Can adsorb an objectionable impurities coating, by following weight part (kilogram) raw material make: urethane resin 9, linear polyester resin 35, isocyanic ester 14, N-BUTYL ACETATE 13, methyl-isobutyl (first) ketone 8, micropowder silica gel 4, Magnesium Stearate 1.5, disodium ethylene diamine tetraacetate 3, diacetone alcohol 15, pimelinketone 3.5, molecular sieve 6, polyisobutene 4, calcium sulfite 3, flow agent 0.4, adhere to auxiliary agent 5;
Described adhere to auxiliary agent by following weight part (kilogram) raw material make: isobornyl acrylate 6, Viscoat 295 6, lauryl acrylate 6, chloroprene rubber 7, polyester glycol 8, polyphenylene oxide 2.5, aluminium hydroxide 0.2, alcohol ester 12 film coalescence aid 6, titanate coupling agent TMC-TTS0.8, calcium naphthenate 1.5, ethylene dichloride 11, methylethylketone 9, isocyanic ester 2.5, ethyl acetate 6, toxilic acid 1.5, urethane acrylate 4.5; Making method is: methylethylketone, ethylene dichloride, ethyl acetate are mixed, under 5000 revs/min, add Viscoat 295, chloroprene rubber, after dissolving, add again isobornyl acrylate, lauryl acrylate, polyester glycol, stir 50 minutes, add other remaining components, be heated to 85 ℃, stirring reaction 50 minutes, obtains.
The described preparation method that can adsorb objectionable impurities coating, comprises the following steps:
(1) prepare A component: N-BUTYL ACETATE, methyl-isobutyl (first) ketone are mixed, add molecular sieve, micropowder silica gel under 5000 revs/min, stir 13 minutes, then add linear polyester resin, stir 1.5 hours, ultrasonic dispersion 7 minutes, makes A component;
(2) prepare B component: in airtight agitator, diacetone alcohol, pimelinketone are mixed, under 5000 revs/min, add urethane resin, isocyanic ester, stir 60 minutes, make B component;
(3) other remaining components are mixed, add A component and B component, stir 35 minutes, obtain.
This coating artificial ageing resistance 3700 hours, coating thicknesses of layers under the prerequisite that keeps low-luster and high-wearing feature reaches more than 35 microns, and sticking power is 2 grades, resistance to impact shock >=50kgcm, snappiness is 3mm.
Claims (2)
1. can adsorb an objectionable impurities coating, it is characterized in that being made by the raw material of following weight part: urethane resin 8-10, linear polyester resin 34-37, isocyanic ester 13-15, N-BUTYL ACETATE 10-15, methyl-isobutyl (first) ketone 6-9, micropowder silica gel 3-5, Magnesium Stearate 1-2, disodium ethylene diamine tetraacetate 2-4, diacetone alcohol 13-16, pimelinketone 3-4, molecular sieve 5-8, polyisobutene 3-5, calcium sulfite 2-4, flow agent 0.4-0.5, adhere to auxiliary agent 4-6;
The described auxiliary agent that adheres to is made by the raw material of following weight part: isobornyl acrylate 5-7, Viscoat 295 5-7, lauryl acrylate 4-7, chloroprene rubber 6-8, polyester glycol 7-9, polyphenylene oxide 2-3, aluminium hydroxide 0.1-0.2, alcohol ester 12 film coalescence aid 5-7, titanate coupling agent TMC-TTS0.6-1, calcium naphthenate 1-2, ethylene dichloride 8-13, methylethylketone 8-11, isocyanic ester 2-3, ethyl acetate 5-8, toxilic acid 1-2, urethane acrylate 4-5; Making method is: methylethylketone, ethylene dichloride, ethyl acetate are mixed, under 4000-6000 rev/min, add Viscoat 295, chloroprene rubber, after dissolving, add again isobornyl acrylate, lauryl acrylate, polyester glycol, stir 40-60 minute, add other remaining components, be heated to 80-90 ℃, stirring reaction 40-60 minute, obtains.
2. the preparation method that can adsorb objectionable impurities coating according to claim 1, is characterized in that comprising the following steps:
(1) prepare A component: N-BUTYL ACETATE, methyl-isobutyl (first) ketone are mixed, under 4000-6000 rev/min, add molecular sieve, micropowder silica gel, stir 10-15 minute, add again linear polyester resin, stir 1-2 hour, ultrasonic dispersion 6-9 minute, makes A component;
(2) prepare B component: in airtight agitator, diacetone alcohol, pimelinketone are mixed, under 4000-6000 rev/min, add urethane resin, isocyanic ester, stir 50-70 minute, make B component;
(3) other remaining components are mixed, add A component and B component, stir 30-40 minute, obtain.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410107247.3A CN103937399B (en) | 2014-03-21 | 2014-03-21 | One can be adsorbed harmful substance coating and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410107247.3A CN103937399B (en) | 2014-03-21 | 2014-03-21 | One can be adsorbed harmful substance coating and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103937399A true CN103937399A (en) | 2014-07-23 |
| CN103937399B CN103937399B (en) | 2016-05-11 |
Family
ID=51185284
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410107247.3A Active CN103937399B (en) | 2014-03-21 | 2014-03-21 | One can be adsorbed harmful substance coating and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103937399B (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105111838A (en) * | 2015-08-13 | 2015-12-02 | 蚌埠南自仪表有限公司 | Blended graphene and silicon dioxide dispersing and heat-dispersion paint and preparation method therefor |
| CN109705691A (en) * | 2019-01-22 | 2019-05-03 | 段小宁 | A kind of preparation method of fast, waterproof the aqueous, environmental protective paint of film forming |
| CN114471490A (en) * | 2022-03-01 | 2022-05-13 | 吉林省国吉控股集团有限公司 | Harmful substance adsorption material and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4289813A (en) * | 1973-02-01 | 1981-09-15 | Bayer Aktiengesellschaft | Process for coating solvent-free lacquers |
| JPH0586327A (en) * | 1991-09-25 | 1993-04-06 | Tanabe Kagaku Kogyo Kk | Coating composition for thermoplastic elastomer |
| CN102181222A (en) * | 2011-04-19 | 2011-09-14 | 三友（天津）高分子技术有限公司 | One-component polyurethane skirt coating used for automotive |
| CN102814167A (en) * | 2012-08-14 | 2012-12-12 | 洛阳市建龙化工有限公司 | Paste molecular sieve activation powder, preparation method and application thereof |
-
2014
- 2014-03-21 CN CN201410107247.3A patent/CN103937399B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4289813A (en) * | 1973-02-01 | 1981-09-15 | Bayer Aktiengesellschaft | Process for coating solvent-free lacquers |
| JPH0586327A (en) * | 1991-09-25 | 1993-04-06 | Tanabe Kagaku Kogyo Kk | Coating composition for thermoplastic elastomer |
| CN102181222A (en) * | 2011-04-19 | 2011-09-14 | 三友（天津）高分子技术有限公司 | One-component polyurethane skirt coating used for automotive |
| CN102814167A (en) * | 2012-08-14 | 2012-12-12 | 洛阳市建龙化工有限公司 | Paste molecular sieve activation powder, preparation method and application thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105111838A (en) * | 2015-08-13 | 2015-12-02 | 蚌埠南自仪表有限公司 | Blended graphene and silicon dioxide dispersing and heat-dispersion paint and preparation method therefor |
| CN109705691A (en) * | 2019-01-22 | 2019-05-03 | 段小宁 | A kind of preparation method of fast, waterproof the aqueous, environmental protective paint of film forming |
| CN114471490A (en) * | 2022-03-01 | 2022-05-13 | 吉林省国吉控股集团有限公司 | Harmful substance adsorption material and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103937399B (en) | 2016-05-11 |
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Effective date of registration: 20160325 Address after: 238200, Anhui, Ma'anshan and Wujiang County Town Chen Lu new street Applicant after: He County Chuangzhi Technology Information Service Co., Ltd Address before: 238251 Industrial Zone, Wujiang Town, Ma'anshan County, Anhui Applicant before: Anhui Lanke Composite Materials Co., Ltd. |
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Effective date of registration: 20171208 Address after: 541000 Dongyuan building, Seven Star District, Guilin City, the Guangxi Zhuang Autonomous Region 801 Patentee after: Ni Ke Address before: 238200, Anhui, Ma'anshan and Wujiang County Town Chen Lu new street Patentee before: Hexian Chuangzhi Technology Information Service Co.,Ltd. |
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| CB03 | Change of inventor or designer information |
Inventor after: Liu Fenggao Inventor before: Liu Xuefeng Inventor before: Chen Xinguo Inventor before: Xu Jin Inventor before: Zhang Guangxiao Inventor before: Yuan Ming Inventor before: Zou Yuhong |
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Effective date of registration: 20171214 Address after: 528325 Guangdong Province, Foshan City Road Xingtan town of Nam Long Industrial Zone Shunde District No. 7, 2 Patentee after: Guangdong new building materials Co., Ltd. Address before: 541000 Dongyuan building, Seven Star District, Guilin City, the Guangxi Zhuang Autonomous Region 801 Patentee before: Ni Ke |
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| TR01 | Transfer of patent right |