CN103937334B - Welding rod lettering pigment and preparation method thereof - Google Patents

Welding rod lettering pigment and preparation method thereof Download PDF

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Publication number
CN103937334B
CN103937334B CN201410158475.3A CN201410158475A CN103937334B CN 103937334 B CN103937334 B CN 103937334B CN 201410158475 A CN201410158475 A CN 201410158475A CN 103937334 B CN103937334 B CN 103937334B
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China
Prior art keywords
pigment
welding rod
lettering
preparation
solidifying agent
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CN201410158475.3A
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CN103937334A (en
Inventor
杨光磊
公茂涛
仇陆弟
赵仕超
刘亮
翁苏华
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PowerChina SPEM Co Ltd
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PowerChina SPEM Co Ltd
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Abstract

The invention discloses welding rod lettering pigment, belong to hard fire colour technical field, this welding rod lettering pigment is mainly uniformly mixed by dispersion agent, high-temperature resisting pigment, solidifying agent and dilution material and makes.This pigment resistance to elevated temperatures is good, and physical and chemical performance is stablized, and long-time placement precipitation-free demixing phenomenon (or only have slight demixing phenomenon, stir before using), and raw materials cost is lower.

Description

Welding rod lettering pigment and preparation method thereof
Technical field
The invention belongs to high-temperature resisting pigment technical field, be specifically related to welding rod lettering pigment and preparation method thereof.
Background technology
Along with the continuous enhancing of environmental protection and energy saving synergy consciousness, do not reduce the prerequisite decline low production cost of quality product, and want raw material drawing conveniently to become trend of the times.
Welding rod lettering pigment adopted pigment dyestuff in the past, and pigment dyestuff, compared with general mineral dye, has higher tinting strength usually, and particle easily grinds and disperses, not easily precipitates, and color is also more bright-coloured, but sun-proof, heat-resisting, weather resistance is poor; And need outwards buying to be specifically designed to the organic synthesis thing starting material making pigment, and the welding rod that welder's life-time service is printed on this pigment also can cause certain harm to Occupational health.
Summary of the invention
The technical problem to be solved in the present invention is to provide provides a kind of low cost, the resistant to elevated temperatures welding rod lettering pigment not containing organic synthesis material, this pigment is imprinted on welding rod, there is high temperature when resistance to welding rod cures, scratch resistance, weather-proof, and raw material drawing is convenient, adopt the raw material that welding rod is produced, cost is lower.
For achieving the above object, technical scheme of the present invention is as follows:
Welding rod lettering pigment, according to mass parts meter, comprises following component: dispersion agent 7-10 part, high-temperature resisting pigment 10-15 part, solidifying agent 5-8 part, dilution material 75-85 part.
In a preferred embodiment of the invention, described dispersion agent is calcium-base bentonite.
In a preferred embodiment of the invention, described high-temperature resisting pigment adopts the iron oxide black of one of component identical with welding rod.
In a preferred embodiment of the invention, described solidifying agent is the one in Powdered water glass or pure potash water glass.
In a preferred embodiment of the invention, described pure potash water glass is 3.3M, the pure potash water glass of 38 ° of Be '.
In a preferred embodiment of the invention, described dilution material for mass percent be one in the aqueous sodium hydroxide solution of 1%-3% or potassium hydroxide aqueous solution.
The preparation method of welding rod lettering pigment, comprises the following steps:
First according to respective mass parts: dispersion agent 7-10 part, high-temperature resisting pigment 10-15 part, after solidifying agent 5-8 part and dilution material 75-85 part take;
Then dispersion agent, high-temperature resisting pigment, solidifying agent are mixed, then add in dilution material, fully mix, stir formation mixture;
Finally mixture is put into colloidal mill grinding, obtain pulpous state black pigment.
By technique scheme, the invention has the beneficial effects as follows:
This high-temperature resisting pigment raw material has drawn from the starting material that welding rod is produced, and be used for welding rod lettering, draw materials conveniently, preparation is simple, with low cost; And resistance to elevated temperatures is good, physical and chemical performance is stablized, and long-time placement precipitation-free demixing phenomenon (or only have slight demixing phenomenon, stir before using).
Embodiment
The technique means realized to make the present invention, creation characteristic, reaching object and effect is easy to understand, setting forth the present invention further.
Welding rod lettering pigment, according to mass parts meter, comprises following component: dispersion agent 7-10 part, high-temperature resisting pigment 10-15 part, solidifying agent 5-8 part, dilution material 75-85 part.
Above-mentioned dispersion agent is high purity calcium-base bentonite (AA type), and AA type calcium-base bentonite water-retaining capacity is strong, has good suspended dispersed effect;
Above-mentioned high-temperature resisting pigment adopts the iron oxide black of one of component identical with welding rod, and chemical formula is Fe3O4.
Above-mentioned solidifying agent is Powdered water glass (being commonly called as sodium silicate) or pure potash water glass (3.3M, 38 ° of Be '), and this solidifying agent can significantly improve pigment and be imprinted on firmness on welding rod after high bake temperature.
Aqueous sodium hydroxide solution or the potassium hydroxide aqueous solution of above-mentioned dilution material to be mass percent be 1%-3%.The effect of dilution material is the viscosity reducing mixture, obtains good mobility.
Embodiment 1
Weigh by following each raw material:
After above-mentioned raw materials takes, first AA type calcium-base bentonite, iron oxide black, powder water glass are mixed, 1% aqueous sodium hydroxide solution adding 11kg, as dilution material, fully mixes, stirs.Then mixture is put into colloidal mill grinding, obtain pulpous state black pigment, there is certain mobility.
The temperature of core wire and coating when this pigment meets welding rod stoving temperature when concrete use, welding rod burns tail end, when testing established temperature and reaching 800 DEG C, after welding rod cured through 2 hours, lettering is still high-visible, without variable color, scratch resistance.
Embodiment 2
Weigh by following each raw material:
After above-mentioned raw materials takes, first AA type calcium-base bentonite, iron oxide black dry mixing are mixed, then pour the pure potash water glass (3.3M, 38 ° of Be ') of 2kg and 1% aqueous sodium hydroxide solution of 9kg into, fully mix, stir.Then mixture is put into colloidal mill grinding, obtain pulpous state black pigment, there is certain mobility.
The temperature of core wire and coating when this pigment meets welding rod stoving temperature when concrete use, welding rod burns tail end, when testing established temperature and reaching 800 DEG C, after welding rod cured through 2 hours, lettering is still high-visible, without variable color, scratch resistance.
Embodiment 3
Weigh by following each raw material:
After above-mentioned raw materials takes, first AA type calcium-base bentonite, iron oxide black dry mixing are mixed, then pour the pure potash water glass (3.3M, 38 ° of Be ') of 2kg and 1% aqueous sodium hydroxide solution of 9kg into, fully mix, stir.Then mixture is put into colloidal mill grinding, obtain pulpous state black pigment, there is certain mobility.
The temperature of core wire and coating when this pigment meets welding rod stoving temperature when concrete use, welding rod burns tail end, when testing established temperature and reaching 800 DEG C, after welding rod cured through 2 hours, lettering is still high-visible, without variable color, scratch resistance; And existing lettering pigment in this case, there will be the phenomenons such as font is fuzzy.
More than show and describe ultimate principle of the present invention and principal character and advantage of the present invention.The technician of the industry should understand; the present invention is not restricted to the described embodiments; what describe in above-described embodiment and specification sheets just illustrates principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in the claimed scope of the invention.Application claims protection domain is defined by appending claims and equivalent thereof.

Claims (1)

1. a preparation method for welding rod lettering pigment, is characterized in that, is made up of following steps:
First according to respective mass parts: dispersion agent calcium-base bentonite 1kg, high-temperature resisting pigment iron oxide black 1.5kg, solidifying agent powder water glass 1kg, after dilution material 1% aqueous sodium hydroxide solution 11kg takes; Then dispersion agent, high-temperature resisting pigment, solidifying agent are mixed, then add in dilution material, fully mix, stir formation mixture; Finally mixture is put into colloidal mill grinding, obtain pulpous state black pigment.
CN201410158475.3A 2014-04-18 2014-04-18 Welding rod lettering pigment and preparation method thereof Active CN103937334B (en)

Priority Applications (1)

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CN201410158475.3A CN103937334B (en) 2014-04-18 2014-04-18 Welding rod lettering pigment and preparation method thereof

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Application Number Priority Date Filing Date Title
CN201410158475.3A CN103937334B (en) 2014-04-18 2014-04-18 Welding rod lettering pigment and preparation method thereof

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CN103937334A CN103937334A (en) 2014-07-23
CN103937334B true CN103937334B (en) 2016-04-13

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Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111909542A (en) * 2020-08-28 2020-11-10 湖州思源颜料有限公司 Preparation method of high-covering-power iron oxide red-bentonite composite pigment
CN116082892A (en) * 2023-01-13 2023-05-09 中国电建集团上海能源装备有限公司 Pigment for printing on welding rod and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1637079A (en) * 2003-10-01 2005-07-13 默克专利股份有限公司 Glossy black interference pigments
CN1781998A (en) * 2004-10-08 2006-06-07 默克专利股份有限公司 Effect pigments based on thin SiO2 flakes
CN1807521A (en) * 2005-01-17 2006-07-26 默克专利股份有限公司 Dye with strong angularly dependent heterochrosis
CN1814673A (en) * 2005-01-17 2006-08-09 默克专利股份有限公司 Strong bepainting red effect color

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102004023075A1 (en) * 2004-05-11 2005-12-08 Merck Patent Gmbh Stabilized BiOCl pigments

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1637079A (en) * 2003-10-01 2005-07-13 默克专利股份有限公司 Glossy black interference pigments
CN1781998A (en) * 2004-10-08 2006-06-07 默克专利股份有限公司 Effect pigments based on thin SiO2 flakes
CN1807521A (en) * 2005-01-17 2006-07-26 默克专利股份有限公司 Dye with strong angularly dependent heterochrosis
CN1814673A (en) * 2005-01-17 2006-08-09 默克专利股份有限公司 Strong bepainting red effect color

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C53 Correction of patent for invention or patent application
CB03 Change of inventor or designer information

Inventor after: Yang Guanglei

Inventor after: Gong Maotao

Inventor after: Chou Ludi

Inventor after: Zhao Shichao

Inventor after: Liu Liang

Inventor after: Weng Suhua

Inventor before: Wang Meng

Inventor before: Weng Suhua

Inventor before: Wang Yaojun

Inventor before: Chou Ludi

Inventor before: Zhao Shichao

COR Change of bibliographic data

Free format text: CORRECT: INVENTOR; FROM: WANG MENG WENG SUHUA WANG YAOJUN CHOU LUDI ZHAO SHICHAO TO: YANG GUANGLEI GONG MAOTAO CHOU LUDI ZHAO SHICHAO LIU LIANG WENG SUHUA

C53 Correction of patent for invention or patent application
CB02 Change of applicant information

Address after: 201316, Shanghai, Pudong New Area Town, barley Bay Industrial Zone, air route 80 - 86

Applicant after: POWERCHINA SPEM COMPANY LIMITED

Address before: 201316, Shanghai, Pudong New Area Town, barley Bay Industrial Zone, air route 80 - 86

Applicant before: Shanghai Power Equipment Manufacture Co., Ltd.

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Free format text: CORRECT: APPLICANT; FROM: SHANGHAI POWER BUILDING AND REPAIRING GENERAL FACTORY CO., LTD. TO: CHINAPOWER CONSTRUCTION GROUP ENERGY EQUIPMENT CO., LTD.

C14 Grant of patent or utility model
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