CN103923783A - Whole-process dissolved oxygen control process in grape wine production - Google Patents
Whole-process dissolved oxygen control process in grape wine production Download PDFInfo
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Abstract
The invention relates to a grape wine brewing technology, and in particular relates to a whole-process dissolved oxygen control process in grape wine production. The process comprises a fermentation stage, an aftertreatment stage and an ageing stage, wherein during the fermentation stage, sulfur dioxide is added for regulation; during the aftertreatment stage, a nitrogen-oxygen displacement device is used, the cold treatment time is shortened, and a certain vacuum-pumping effect is kept in a filling stage; during the ageing stage, filling, boxing, ageing and storing are performed in a scientific manner, and the temperature and humidity are kept constant; and during each stage, nitrogen gas is pre-introduced into tanks and pipelines, and conveying pipelines are exhausted in time. According to the production process, nitrogen gas is utilized for protection, the dissolved oxygen content is scientifically controlled, quantitative criteria is made for a reasonable control level of dissolved oxygen in a brewing process; and a visual numeric indicator is established for change rules of dissolved oxygen in the whole grape wine brewing process, the ageing and maturing promoting effect of micro oxygen is fully exerted, and the production process is concise, convenient to control, economical, low in cost and convenient in extensive popularization.
Description
Technical field
The present invention relates to wine making technical field, is that in a kind of Production of Wine, omnidistance dissolved oxygen is controlled technique specifically.
background technology
Dissolved oxygen in grape wine refers to molecularity and is dissolved in the oxygen in grape wine.Oxygen level in grape wine is in dynamic change, and one side reacts and is consumed with the component in grape wine, on the other hand, in brewing grape wine, storage, the process of circulation, can dissolve in because of certain operations.The nineties in 20th century, the people such as Patrick proposed by special instrument, lentamente, controlledly in wine, add micro-oxygen, and add oak chip, the condition of analogy oak barrel during aging, wine is carried out to micro-oxygen technology of slaking ageing, since then, at Grape Wine Industry, about oxygen, the research of grape wine quality impact is become common practise.Yet people pay close attention to micro-oxygen in the effect of the aspects such as help fermentation, reduction Reduction Smell, raw blue or green taste, softening tannin, softening mouthfeel, raising colour stability, have but ignored excessive dissolution oxygen to hazardness vinous.
For the weak daily wine of going with rice or bread of self resistance of oxidation, if brewage, be not good at causing dissolved oxygen excessive because of process management in storage at it, will cause a series of wicked problems such as fruital disappearance, wine body deterioration by oxidation, pigementation, shelf-lives shortening.Therefore, grasp the Changing Pattern of dissolved oxygen in whole brewing process comprehensively, and apply to neatly each operation stage, give full play to the Chen Zuoyong that urges of dissolved oxygen, become the difficult problem that each EnologistWinemaker will face.And at present in Grape Wine Industry, for measure how the to take science system of going, control dissolved oxygen, make it maintain the problems such as what kind of reasonable level also not explore a set of complete effective technical process.
Summary of the invention
The object of the invention is to solve the deficiency that above-mentioned prior art exists, provide a kind of science to control dissolved oxygen, the reasonable level of control of dissolved oxygen in brewing process made to omnidistance dissolved oxygen in the Production of Wine of quantitative criterion and control technique.
In Production of Wine of the present invention, omnidistance dissolved oxygen is controlled technique, comprises fermentation stage, post-processing stages, ageing stage, and described post-processing stages comprises homogeneous stage, lower glue stage, deepfreeze stage and filling stage.Special character is in treating the fermentor tank of pan feeding, to be filled with nitrogen in advance in fermentation stage, in the transport pipe of destemming fragmentation, being filled with in advance after nitrogen is the sulfurous gas of 40-60mg/L to adding concentration in the grape mash of destemming fragmentation, and to carrying the pipeline nitrogen head space after grape mash, after 12-24h, add yeast and start fermentation, the dissolved oxygen of grape mash after destemming fragmentation is controlled at below 4mg/L, and the dissolved oxygen adding after yeast 24h is controlled at 0.02-0.1mg/L;
In post-processing stages, in advance preparation tank, pipeline are filled with to nitrogen, turn and in tank tank process, use nitrogen oxygen displacement apparatus, after turning tank tank, use nitrogen head space pipeline, and reduce and to turn tank tank, stirring operation operation, in operating process, keep canful completely to deposit state, and shorten the deepfreeze time to 10-14 days, the vacuumizing effect of pre-inflated with nitrogen and maintenance-10 during the filling stage--20KPa;
A modification of the present invention is, the described homogeneous stage relates to and turns tank tank, whipping process, in this stage, preparation tank and pumping line are filled with to nitrogen in advance, in pumping procedure, use nitrogen oxygen displacement apparatus, after pumping, with nitrogen head space pipeline, in operating process, keep canful storing state, make the front dissolved oxygen of homogeneous be controlled at 0.02-0.03mg/L, homogeneous dissolved oxygen on the same day is controlled at below 1.0mg/L, and after homogeneous, 5-7 days dissolved oxygens return to 0.02-0.03mg/L.
Another improvement of the present invention is, described lower glue is in the stage, carry out enclosed circulation, after standing, pass through tank switching, filter implementation phase target, in this stage, preparation tank and pumping line are filled with to nitrogen in advance, in pumping procedure, use nitrogen oxygen displacement apparatus, after pumping, use nitrogen head space pipeline, in operating process, keep canful storing state, before making lower glue, dissolved oxygen is controlled at 0.02-0.03mg/L, lower glue dissolved oxygen on the same day is controlled at 0.4-0.6mg/L, and after lower glue, 5-7 days dissolved oxygens return to 0.02-0.03mg/L.
Another improvement of the present invention is, in the described deepfreeze stage, preparation tank and pumping line are filled with to nitrogen in advance, in pumping procedure, use nitrogen oxygen displacement apparatus, after pumping, use nitrogen head space pipeline, and in insulated and stirred process, treat treatment tank top and be filled with in advance nitrogen, in enclosed circulation process, use nitrogen oxygen displacement apparatus, shorten the deepfreeze time to 10-14 days, in operating process, keep canful storing state, before making deepfreeze, dissolved oxygen is controlled at 0.02-0.03mg/L, in cold-treating process, dissolved oxygen is controlled at below 3.0mg/L, after going out refrigerated cylinder, 3-5 days dissolved oxygens return to 0.02-0.03mg/L.
Another improvement of the present invention is; in the described filling stage; filling machine is poured to nitrogen in advance; filling machine foreshot is adjusted downward to the liquid level of pressing close to deposit drinking vessel; the space of bottleneck after the difference of altitude that minimizing wine liquid falls and the bottling of wine liquid; the vacuumizing effect that keeps filling machine-10--20KPa; make to deposit the negative pressure state of drinking vessel in nitrogen protection; by the be controlled at-30-30KPa of pressure in the space, wine sample bottle top after bottling; adjust Free sulfur dioxide content and make it be controlled at 35-40mg/L, the wine after bottling is controlled at below 2mg/L.
Another improvement of the present invention is, described fermentation stage, and dissolved oxygen is controlled at 0-0.08mg/L at fermentation animated period, turns tank frequency control at 2-3 time, keeps canful storing state after fermentation ends.
Another improvement of the present invention is that, in described fermentation stage, grape material adopts the Atmosphere Presser with automatic nitrogen-charging function to squeeze, at any time grape mash is carried out to nitrogen protection.
Another improvement of the present invention is, described tank inflated with nitrogen fills for institute the 1/3-1/2 that tank holds, and nitrogen and wine liquid are to be all filled with by pot bottom, along with the rising of wine liquid liquid level, can force surplus air discharge.
Another improvement of the present invention is, the nitrogen that described pipeline inflated with nitrogen is purity >=99.99%, and it is >=30% going out wine end concentration, with this, rationally controls the input of nitrogen in pipeline.
In Production of Wine of the present invention, omnidistance dissolved oxygen is controlled technique, utilize nitrogen protection, reduce and turn tank, and tank, the schedule of operation such as stirring, keep canful to store, shorten the deepfreeze time, change storage condition, science is controlled dissolved oxygen content, and the reasonable level of control of dissolved oxygen in brewing process is made to quantitative criterion, Changing Pattern to dissolved oxygen in whole wine making has been set up visual numerical index, brought into play fully the old maturing of urging of micro-oxygen, the oxidation of avoiding excessive dissolution oxygen to bring, the problems such as precipitation, and concise production process, it is convenient to control, Financial cost is low, be convenient to extensive popularization.
Embodiment
Below provide the specific embodiment of the present invention, be used for the present invention to be further described.
In the Production of Wine of following examples, omnidistance dissolved oxygen is controlled technique, has all both been applicable to the brewing process that red wine is also applicable to white wine.Its concrete technology flow process is as follows:
Embodiment 1
In the Production of Wine of the present embodiment, omnidistance dissolved oxygen is controlled technique, and its concrete technology flow process is as follows:
1, fermentation stage: treat in advance the nitrogen that the fermentor tank of pan feeding and the transport pipe of destemming fragmentation are filled with purity >=99.99%, in fermentor tank, be filled with the nitrogen that 1/2 tank holds, the nitrogen that is filled with of the transport pipe of destemming fragmentation guarantees to test nitrogen gas concn >=30% at the wine end that goes out of pipeline.After pre-inflated with nitrogen, to adding immediately concentration in the grape mash of destemming fragmentation, be the sulfurous gas of 40mg/L, and to carrying the pipeline nitrogen head space after grape mash.To grape material, adopt the Atmosphere Presser with automatic nitrogen-charging function to squeeze, after 12h, add yeast and start fermentation, make the dissolved oxygen of grape mash after destemming fragmentation be controlled at 3-4mg/L, add yeast 24h after dissolved oxygen in 0.08-0.1mg/L level.Enter fermentation during animated period, dissolved oxygen is extremely low-level in 0.01-0.03mg/L all, until fermentation ends.
Wherein, the Sucus Vitis viniferae of Fructus Vins raw material after clarification enters after fermentor tank, after 12h by 1/2 the yeast fully activate in tank deck pumps into fermentor tank, 1/2 from pumping at the bottom of tank in fermentor tank, in rear unlatching fermentor tank, carries recycle pump, internal recycle 5min, i.e. startup is fermented; The grape mash of red grape raw material after destemming fragmentation enters after fermentor tank, after 12h, the yeast fully having activated pumped into fermentor tank from tank deck, and rear unlatching fermentor tank carries recycle pump, makes the grape mash amount of circulation be controlled at 1/4 of the interior total feeding of fermentor tank.
Between yeast phase, reasonably reduce and turn tank frequency under processing requirement as far as possible, after fermentation ends, keep canful storing state.
2, post-processing stages:
Post-processing stages comprises the critical process nodes such as homogeneous stage, lower glue stage, deepfreeze stage and filling stage, and measure of control and the reasonable level of its dissolved oxygen are specific as follows:
1. homogeneous stage: by taking that preparation tank and pumping line are taked to conventional way; but take to use in pumping procedure after SPRO1010 nitrogen oxygen displacement instrument, pumping with nitrogen head space pipeline, keep the measures such as canful storing state to carry out nitrogen protection in subsequent handling; before making homogeneous, dissolved oxygen is controlled at 0.026-0.03mg/L level; homogeneous dissolved oxygen on the same day is controlled at 0.2-0.4mg/L, and after homogeneous, 5-7 days dissolved oxygens return to 0.026-0.03mg/L level.
Nitrogen oxygen displacement instrument is arranged on pump and proceeds on the pipeline between tank, mainly comprises the tubing system of nitrogen gas generating system, pressure regulator valve, magnetic valve, tensimeter, displacement head and connecting components.The nitrogen amount passing into is by solenoid control, and unit is mg/L; Displacement head makes nitrogen dispersion become small bubble, after by the film covering on a displacement core cylinder, be slowly scattered in wine, guarantee that nitrogen can dissolve completely.Utilize solubleness and the Henry's law of gas in liquid, the dissolved oxygen in grape wine is cemented out, thereby reduce the amount of oxygen in grape wine, prevent the oxidation of wine body.What the present invention used is the SPRO1010 type nitrogen oxygen displacement instrument apparatus system by Beijing Sai Puruishen development in science and technology company limited imported with original packaging.
With nitrogen head space pipeline, the wine liquid in pipeline can be ejected first, avoid waste, second can avoid airborne oxygen to dissolve in wine body, adopt nitrogen to completely cut off protection.Thereby coordinate above measure to carry out nitrogen protection to the wine body in homogeneous stage.
2. play the glue stage: enclosed circulation process and pumping procedure are regular circulation process; by taking to treat before treatment tank top is filled with the operations such as nitrogen, tank switching and filtration in advance, preparation tank is filled with in advance after nitrogen, pumping line are filled with nitrogen, pumping in advance, with measures such as nitrogen head space pipeline, maintenance canful storing states, wine body is carried out to nitrogen protection; before making lower glue, dissolved oxygen is controlled at 0.026-0.03mg/L level; lower glue dissolved oxygen on the same day is controlled at 0.4-0.48mg/L level, and after lower glue, 5-7 days dissolved oxygens return to 0.026-0.03mg/L level.
3. deepfreeze stage: adopt deepfreeze mode conventional in prior art to carry out the relevant treatment of grape wine body.
4. filling stage: by filling machine is filled with to nitrogen in advance, make filling machine foreshot lower when filling, press close to liquid level, reduce the space of bottleneck after difference of altitude that wine liquid falls and wine bottling.Check the vacuumizing effect of filling machine; make to deposit the drinking vessel negative pressure state of-15--10KPa under nitrogen protection all the time; space, wine sample bottle top pressure after bottling is controlled at-30--10KPa; and adjust Free sulfur dioxide content and make it be controlled at 35-40mg/L level, above measure compounding practice is controlled at below 2mg/L the wine after bottling.
3, the ageing stage: by taking to select the high-quality bottle stopper identical with bottle, the filling process of science, the sleeping packing method of putting or putting upside down etc., and in circulation sale process, select the good mode of displaying and storage condition, keep humiture constant, the measures such as the physical and chemical indexs such as dissolved oxygen, sulfurous gas, volatile acid, colourity, tone, redox potential and aesthetic quality that detect in wine are controlled, and predict its oxidation potential and life cycle, for the shelf-lives of product provides reference frame.
Embodiment 2
1, fermentation stage: treat in advance the nitrogen that the fermentor tank of pan feeding and the transport pipe of destemming fragmentation are filled with purity >=99.99%, in fermentor tank, be filled with the nitrogen that 1/3 tank holds, the nitrogen that is filled with of the transport pipe of destemming fragmentation guarantees to test nitrogen gas concn >=30% at the wine end that goes out of pipeline.After pre-inflated with nitrogen, to adding immediately concentration in the grape mash of destemming fragmentation, be the sulfurous gas of 50mg/L, and to carrying the pipeline nitrogen head space after grape mash.To grape material, adopt the Atmosphere Presser with automatic nitrogen-charging function to squeeze, after 18h, add yeast and start fermentation, make the dissolved oxygen of grape mash after destemming fragmentation be controlled at 2-3mg/L, add yeast 24h after dissolved oxygen in 0.05-0.08mg/L level.Enter fermentation during animated period, dissolved oxygen is extremely low-level in 0.03-0.05mg/L all, until fermentation ends.
Wherein, the Sucus Vitis viniferae of Fructus Vins raw material after clarification enters after fermentor tank, after 18h by 1/2 the yeast fully activate in tank deck pumps into fermentor tank, 1/2 from pumping at the bottom of tank in fermentor tank, in rear unlatching fermentor tank, carries recycle pump, internal recycle 5min, i.e. startup is fermented; The grape mash of red grape raw material after destemming fragmentation enters after fermentor tank, after 18h, the yeast fully having activated pumped into fermentor tank from tank deck, and rear unlatching fermentor tank carries recycle pump, makes the grape mash amount of circulation be controlled at 3/10 of the interior total feeding of fermentor tank.
Between yeast phase, reasonably reduce and turn tank frequency under processing requirement as far as possible, after fermentation ends, keep canful storing state.
2, post-processing stages:
Post-processing stages comprises the critical process nodes such as homogeneous stage, lower glue stage, deepfreeze stage and filling stage, and measure of control and the reasonable level of its dissolved oxygen are specific as follows:
1. homogeneous stage: be filled with in advance after using SPRO1010 nitrogen oxygen displacement instrument, pumping in nitrogen, pumping procedure and carry out omnidistance nitrogen protection with measures such as nitrogen head space pipeline, maintenance canful storing states by taking that preparation tank is filled with to nitrogen, pumping line in advance; before making homogeneous, dissolved oxygen is controlled at 0.023-0.026mg/L level; homogeneous dissolved oxygen on the same day is controlled at below 0.4-0.8mg/L, and after homogeneous, 5-7 days dissolved oxygens return to 0.023-0.026mg/L level.
2. play the glue stage: adopt glue stage processing mode under wine production processes conventional in prior art to carry out the relevant treatment of grape wine body.
3. deepfreeze stage: by taking that preparation tank is filled with to nitrogen in advance, pumping line is filled with nitrogen in advance, in pumping procedure, use SPRO1010 nitrogen oxygen displacement instrument, after pumping, use nitrogen head space pipeline, in insulated and stirred process, treat treatment tank top and be filled with in advance nitrogen, in enclosed circulation process, use nitrogen oxygen displacement apparatus, shorten the deepfreeze time to 10 day, keep the measures such as canful storing state to carry out whole process protection, before making deepfreeze, dissolved oxygen is controlled at 0.023-0.026mg/L level, in cold-treating process, dissolved oxygen is controlled at 2.0-3.0mg/L, after going out refrigerated cylinder, 3-5 days dissolved oxygens return to 0.023-0.026mg/L level.
4. filling stage: by filling machine is filled with to nitrogen in advance, make filling machine foreshot lower when filling, press close to liquid level, reduce the space of bottleneck after difference of altitude that wine liquid falls and wine bottling.Check the vacuumizing effect of filling machine; make to deposit the drinking vessel negative pressure state of-20--18KPa under nitrogen protection all the time; space, wine sample bottle top pressure after bottling is controlled at 10-30KPa; and adjust Free sulfur dioxide content and make it be controlled at 35-40mg/L level, above measure compounding practice is controlled at below 2mg/L the wine after bottling.
3, the ageing stage: by taking to select the high-quality bottle stopper identical with bottle, the filling process of science, the sleeping packing method of putting or putting upside down etc., and in circulation sale process, select the good mode of displaying and storage condition, keep humiture constant, the measures such as the physical and chemical indexs such as dissolved oxygen, sulfurous gas, volatile acid, colourity, tone, redox potential and aesthetic quality that detect in wine are controlled, and predict its oxidation potential and life cycle, for the shelf-lives of product provides reference frame.
Embodiment 3
1, fermentation stage: treat in advance the nitrogen that the fermentor tank of pan feeding and the transport pipe of destemming fragmentation are filled with purity >=99.99%, in fermentor tank, be filled with the nitrogen that 2/5 tank holds, the nitrogen that is filled with of the transport pipe of destemming fragmentation guarantees to test nitrogen gas concn >=30% at the wine end that goes out of pipeline.After pre-inflated with nitrogen, to adding immediately concentration in the grape mash of destemming fragmentation, be the sulfurous gas of 60mg/L, and to carrying the pipeline nitrogen head space after grape mash.To grape material, adopt the Atmosphere Presser with automatic nitrogen-charging function to squeeze, after 24h, add yeast and start fermentation, make the dissolved oxygen of grape mash after destemming fragmentation be controlled at 1-2mg/L, add yeast 24h after dissolved oxygen in 0.02-0.05mg/L level.Enter fermentation during animated period, dissolved oxygen is extremely low-level in 0.05-0.08mg/L all, until fermentation ends.
Wherein, the Sucus Vitis viniferae of Fructus Vins raw material after clarification enters after fermentor tank, after 24h by 1/2 the yeast fully activate in tank deck pumps into fermentor tank, 1/2 from pumping at the bottom of tank in fermentor tank, in rear unlatching fermentor tank, carries recycle pump, internal recycle 5min, i.e. startup is fermented; The grape mash of red grape raw material after destemming fragmentation enters after fermentor tank, after 18h, the yeast fully having activated pumped into fermentor tank from tank deck, and rear unlatching fermentor tank carries recycle pump, makes the grape mash amount of circulation be controlled at 1/3 of the interior total feeding of fermentor tank.
Between yeast phase, reasonably reduce and turn tank frequency under processing requirement as far as possible, after fermentation ends, keep canful storing state.
2, post-processing stages:
Post-processing stages comprises the critical process nodes such as homogeneous stage, lower glue stage, deepfreeze stage and filling stage, and measure of control and the reasonable level of its dissolved oxygen are specific as follows:
1. homogeneous stage: be filled with in advance after using SPRO1010 nitrogen oxygen displacement instrument, pumping in nitrogen, pumping procedure and carry out omnidistance nitrogen protection with measures such as nitrogen head space pipeline, maintenance canful storing states by taking that preparation tank is filled with to nitrogen, pumping line in advance; before making homogeneous, dissolved oxygen is controlled at 0.02-0.023mg/L level; homogeneous dissolved oxygen on the same day is controlled at 0.8-1.0mg/L, and after homogeneous, 5-7 days dissolved oxygens return to 0.02-0.023mg/L level.
2. play the glue stage: by taking to treat treatment tank top, be filled with in advance nitrogen, in enclosed circulation process, use nitrogen oxygen displacement apparatus, before the operation such as tank switching and filtration, preparation tank is filled with to nitrogen in advance, pumping line is filled with nitrogen in advance, in pumping procedure, use SPRO1010 nitrogen oxygen displacement instrument, after pumping, use nitrogen head space pipeline, keep the measures such as canful storing state to carry out whole process protection to wine body, before making lower glue, dissolved oxygen is controlled at 0.02-0.023mg/L level, lower glue dissolved oxygen on the same day is controlled at 0.54-0.6mg/L level, after lower glue, 5-7 days dissolved oxygens return to 0.02-0.023mg/L level.
3. deepfreeze stage: by taking that preparation tank is filled with to nitrogen in advance, pumping line is filled with nitrogen in advance, in pumping procedure, use SPRO1010 nitrogen oxygen displacement instrument, after pumping, use nitrogen head space pipeline, in insulated and stirred process, treat treatment tank top and be filled with in advance nitrogen, in enclosed circulation process, use nitrogen oxygen displacement apparatus, shorten the deepfreeze time to 14 day, keep the measures such as canful storing state to carry out whole process protection, before making deepfreeze, dissolved oxygen is controlled at 0.02-0.023mg/L level, in cold-treating process, dissolved oxygen is controlled at 1.0-2.0mg/L, after going out refrigerated cylinder, 3-5 days dissolved oxygens return to 0.02-0.023mg/L level.
4. filling stage: by filling machine is filled with to nitrogen in advance, make filling machine foreshot lower when filling, press close to liquid level, reduce the space of bottleneck after difference of altitude that wine liquid falls and wine bottling.Check the vacuumizing effect of filling machine; make to deposit the drinking vessel negative pressure state of-18--15KPa under nitrogen protection all the time; space, wine sample bottle top be controlled at-10-10KPa of pressure after bottling; and adjust Free sulfur dioxide content and make it be controlled at 35-40mg/L level, above measure compounding practice is controlled at below 2mg/L the wine after bottling.
3, the ageing stage: by taking to select the high-quality bottle stopper identical with bottle, the filling process of science, the sleeping packing method of putting or putting upside down etc., and in circulation sale process, select the good mode of displaying and storage condition, keep humiture constant, the measures such as the physical and chemical indexs such as dissolved oxygen, sulfurous gas, volatile acid, colourity, tone, redox potential and aesthetic quality that detect in wine are controlled, and predict its oxidation potential and life cycle, for the shelf-lives of product provides reference frame.
Above embodiment is not exhaustive; its protection domain is not limited to given embodiment; inflated with nitrogen or use nitrogen oxygen displacement apparatus or keep the measures such as canful storage can random combine in advance in homogeneous stage, lower glue stage, deepfreeze stage and the filling stage comprising as post-processing stages; some stages are taked nitrogen protection; some stages adopt usual manner, and many measure random combines play nitrogen protection in various degree.The achieved all technical schemes of every thinking according to the present invention, all belong to protection scope of the present invention.
Claims (10)
1. in Production of Wine, omnidistance dissolved oxygen is controlled technique, comprise fermentation stage, post-processing stages, the ageing stage, described post-processing stages comprises the homogeneous stage, the lower glue stage, deepfreeze stage and filling stage, it is characterized in that: in fermentation stage, in fermentor tank, be filled with in advance nitrogen, in the transport pipe of destemming fragmentation, being filled with in advance after nitrogen is the sulfurous gas of 40-60mg/L to adding concentration in the grape mash of destemming fragmentation, and to carrying the pipeline nitrogen head space after grape mash, after 12-24h, add yeast and start fermentation, the dissolved oxygen of grape mash after destemming fragmentation is controlled at below 4mg/L, the dissolved oxygen adding after yeast 24h is controlled at 0.02-0.1mg/L,
In post-processing stages, in advance preparation tank, pipeline are filled with to nitrogen, turn and in tank tank process, use nitrogen oxygen displacement apparatus, after turning tank tank, use nitrogen head space pipeline, and reduce and to turn tank tank, stirring operation operation, in operating process, keep canful completely to deposit state, and shorten the deepfreeze time to 10-14 days, the vacuumizing effect of pre-inflated with nitrogen and maintenance-20 during the filling stage--10KPa.
2. in Production of Wine as claimed in claim 1, omnidistance dissolved oxygen is controlled technique, it is characterized in that: described homogeneous is in the stage, preparation tank and pumping line are filled with to nitrogen in advance, in pumping procedure, use nitrogen oxygen displacement apparatus, after pumping, with nitrogen head space pipeline, in operating process, keep canful storing state, make the front dissolved oxygen of homogeneous be controlled at 0.02-0.03mg/L, homogeneous dissolved oxygen on the same day is controlled at below 1.0mg/L, and after homogeneous, 5-7 days dissolved oxygens return to 0.02-0.03mg/L.
3. in Production of Wine as claimed in claim 1 or 2, omnidistance dissolved oxygen is controlled technique, it is characterized in that: described lower glue is in the stage, preparation tank and pumping line are filled with to nitrogen in advance, in pumping procedure, use nitrogen oxygen displacement apparatus, after pumping, with nitrogen head space pipeline, in operating process, keep canful storing state, make the front dissolved oxygen of lower glue be controlled at 0.02-0.03mg/L, lower glue dissolved oxygen on the same day is controlled at 0.4-0.6mg/L, and after lower glue, 5-7 days dissolved oxygens return to 0.02-0.03mg/L.
4. in Production of Wine as claimed in claim 1 or 2, omnidistance dissolved oxygen is controlled technique, it is characterized in that: in the described deepfreeze stage, preparation tank and pumping line are filled with to nitrogen in advance, in pumping procedure, use nitrogen oxygen displacement apparatus, after pumping, use nitrogen head space pipeline, and in insulated and stirred process, treat treatment tank top and be filled with in advance nitrogen, in enclosed circulation process, use nitrogen oxygen displacement apparatus, shorten the deepfreeze time to 10-14 days, in operating process, keep canful storing state, before making deepfreeze, dissolved oxygen is controlled at 0.02-0.03mg/L, in cold-treating process, dissolved oxygen is controlled at 2.5-3.5mg/L, after going out refrigerated cylinder, 3-5 days dissolved oxygens return to 0.02-0.03mg/L.
5. in Production of Wine as claimed in claim 3, omnidistance dissolved oxygen is controlled technique, it is characterized in that: in the described deepfreeze stage, preparation tank and pumping line are filled with to nitrogen in advance, in pumping procedure, use nitrogen oxygen displacement apparatus, after pumping, use nitrogen head space pipeline, and in insulated and stirred process, treat treatment tank top and be filled with in advance nitrogen, in enclosed circulation process, use nitrogen oxygen displacement apparatus, shorten the deepfreeze time to 10-14 days, in operating process, keep canful storing state, before making deepfreeze, dissolved oxygen is controlled at 0.02-0.03mg/L, in cold-treating process, dissolved oxygen is controlled at 2.5-3.5mg/L, after going out refrigerated cylinder, 3-5 days dissolved oxygens return to 0.02-0.03mg/L.
6. in Production of Wine as claimed in claim 1 or 2, omnidistance dissolved oxygen is controlled technique, it is characterized in that: in the described filling stage, filling machine is poured to nitrogen in advance, filling machine foreshot is adjusted downward to the liquid level of pressing close to deposit drinking vessel, the vacuumizing effect that keeps filling machine-20--10KPa, by the be controlled at-30-30KPa of pressure in the space, wine sample bottle top after bottling, to adjust Free sulfur dioxide content and make it be controlled at 35-40mg/L, the wine after bottling is controlled at below 2mg/L.
7. in Production of Wine as claimed in claim 5, omnidistance dissolved oxygen is controlled technique, it is characterized in that: described fermentation stage, dissolved oxygen is controlled at 0-0.08mg/L at fermentation animated period, turns tank frequency control at 2-3 time, keeps canful storing state after fermentation ends.
8. in Production of Wine as claimed in claim 7, omnidistance dissolved oxygen is controlled technique, it is characterized in that: in described fermentation stage, grape material adopts the Atmosphere Presser with automatic nitrogen-charging function to squeeze.
9. in Production of Wine as claimed in claim 8, omnidistance dissolved oxygen is controlled technique, it is characterized in that: the 1/3-1/2 that described tank inflated with nitrogen is held for fill tank.
10. in Production of Wine as claimed in claim 9, omnidistance dissolved oxygen is controlled technique, it is characterized in that: the nitrogen that described pipeline inflated with nitrogen is purity >=99.99%, it is going out wine end concentration >=30%.
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| CN104195025A (en) * | 2014-08-18 | 2014-12-10 | 中粮绍兴酒有限公司 | On-line-monitoring yellow wine micro-oxygenation maturing and storage system and application method thereof |
| CN108384684A (en) * | 2018-05-22 | 2018-08-10 | 火龙源（厦门）生物科技有限公司 | A kind of brewing method and red pitaya wine of red pitaya wine |
| CN110002386A (en) * | 2019-04-30 | 2019-07-12 | 宁夏沙泉葡萄酿酒有限公司 | Using the filling process for vacuumizing dozen nitrogen and cork during wine filing |
| CN110317701A (en) * | 2019-08-24 | 2019-10-11 | 湖南溆浦湘妃酒业有限责任公司 | Continuously fermented the production method and system of technology brewing wine of fruit of cherokee rose based on low temperature |
| CN110747295A (en) * | 2019-09-20 | 2020-02-04 | 华南理工大学 | Quality-guaranteeing storage method of high fructose corn syrup product |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4624391A (en) * | 1983-10-20 | 1986-11-25 | American Business Computers | Automatic wine dispenser |
| WO2009017428A1 (en) * | 2007-08-01 | 2009-02-05 | Ian Stuart Williams | Combined brewing system |
| CN102323313A (en) * | 2011-08-03 | 2012-01-18 | 华南理工大学 | Method and device for detecting ageing time of dry wine |
| CN103068265A (en) * | 2010-05-21 | 2013-04-24 | 弗朗西斯科·乔斯·杜阿尔特维埃拉 | Method and appliances for low temperature pasteurisation of liquid foods and removal of oxygen from liquid foods by decompression and/or high linear or rotary acceleration |
-
2014
- 2014-04-25 CN CN201410169805.9A patent/CN103923783B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4624391A (en) * | 1983-10-20 | 1986-11-25 | American Business Computers | Automatic wine dispenser |
| WO2009017428A1 (en) * | 2007-08-01 | 2009-02-05 | Ian Stuart Williams | Combined brewing system |
| CN103068265A (en) * | 2010-05-21 | 2013-04-24 | 弗朗西斯科·乔斯·杜阿尔特维埃拉 | Method and appliances for low temperature pasteurisation of liquid foods and removal of oxygen from liquid foods by decompression and/or high linear or rotary acceleration |
| CN102323313A (en) * | 2011-08-03 | 2012-01-18 | 华南理工大学 | Method and device for detecting ageing time of dry wine |
Non-Patent Citations (2)
| Title |
|---|
| 周鹏辉，等: "SPRO1010型氮氧置换仪在葡萄酒后处理阶段的应用", 《酿酒科技》, no. 9, 31 December 2013 (2013-12-31) * |
| 杨雪峰，等: "葡萄酒酿造中溶解氧变化研究", 《酿酒科技》, no. 7, 31 December 2006 (2006-12-31), pages 55 - 56 * |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104195025A (en) * | 2014-08-18 | 2014-12-10 | 中粮绍兴酒有限公司 | On-line-monitoring yellow wine micro-oxygenation maturing and storage system and application method thereof |
| CN108384684A (en) * | 2018-05-22 | 2018-08-10 | 火龙源（厦门）生物科技有限公司 | A kind of brewing method and red pitaya wine of red pitaya wine |
| CN110002386A (en) * | 2019-04-30 | 2019-07-12 | 宁夏沙泉葡萄酿酒有限公司 | Using the filling process for vacuumizing dozen nitrogen and cork during wine filing |
| CN110317701A (en) * | 2019-08-24 | 2019-10-11 | 湖南溆浦湘妃酒业有限责任公司 | Continuously fermented the production method and system of technology brewing wine of fruit of cherokee rose based on low temperature |
| CN110317701B (en) * | 2019-08-24 | 2024-03-22 | 湖南溆浦湘妃酒业有限责任公司 | Production method and system for brewing cherokee rose fruit wine based on low-temperature continuous fermentation technology |
| CN110747295A (en) * | 2019-09-20 | 2020-02-04 | 华南理工大学 | Quality-guaranteeing storage method of high fructose corn syrup product |
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| CN103923783B (en) | 2016-05-04 |
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