CN103819916A - Emulsified coal tar pitch - Google Patents

Emulsified coal tar pitch Download PDF

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Publication number
CN103819916A
CN103819916A CN201410070578.4A CN201410070578A CN103819916A CN 103819916 A CN103819916 A CN 103819916A CN 201410070578 A CN201410070578 A CN 201410070578A CN 103819916 A CN103819916 A CN 103819916A
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China
Prior art keywords
tar pitch
coal
emulsification
pitch
coal tar
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CN201410070578.4A
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Chinese (zh)
Inventor
王诤
唐广帅
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SHANXI YUANZHENG CHEMICAL Co Ltd
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SHANXI YUANZHENG CHEMICAL Co Ltd
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Priority to CN201410070578.4A priority Critical patent/CN103819916A/en
Publication of CN103819916A publication Critical patent/CN103819916A/en
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Abstract

The invention discloses an emulsified coal tar pitch which is prepared from the following raw materials: 500 g of coal tar pitch, 500 g of water, 3 g of an asphalt emulsifier and 1 g of bentonite. A preparation method of the emulsified coal tar pitch comprises the following steps: adding bentonite into the asphalt emulsifier; mixing the mixture of bentonite and the asphalt emulsifier with water to obtain an emulsion; and using coal tar pitch and the emulsion to prepare the emulsified coal tar pitch. According to the preparation method of the emulsified coal tar pitch, coal tar pitch is emulsified by adding bentonite into the asphalt emulsifier. Thus, problems of coal tar pitch emulsification and stabilization after emulsification are solved.

Description

A kind of emulsification coal-tar pitch
Technical field
The invention belongs to pitch preparation field, relate in particular to a kind of emulsification coal-tar pitch.
Background technology
Along with Chinese society, expanding economy, enter high-speed development period from " 95 " road construction later, heavy road construction and maintenance task have determined that domestic road bitumen market is by long-term supply and demand anxiety, China's oil asphaltic products. deficiency remains on a high position to the demand of Imported oil pitch, and asphalt price is by the fluctuation with the variation of International Petroleum Price.Along with the adjustment of China's economic structure as Coal Chemical Industry product coal-tar pitch in supply exceed demand state, the coal-tar pitch that script is used for burning is for road construction, can solve the problem of highway in China coal-tar pitch anxiety, also can solve the problem of outlet of Coal Chemical Industry product, also solve the coal-tar pitch harm that environment is brought of burning, therefore, coal-tar pitch is imperative for road construction, have not yet to see the domestic pair report of coal-tar pitch emulsification that has.
Because coal-tar pitch carbon content is high, medium temperature coal pitch free carbon content is higher, thereby glue core is large especially, and dispersion medium and to play the content of resinous substances of dissemination few comparatively speaking, therefore compared with petroleum pitch, coal-tar pitch is difficult for emulsification.
Summary of the invention
The object of the present invention is to provide a kind of emulsification coal-tar pitch, be intended to solve the problem that coal-tar pitch is difficult for emulsification.
The present invention is achieved in that a kind of emulsification coal-tar pitch, and the various raw-material ratios of described emulsification coal-tar pitch are:
Figure BDA0000471077760000021
Another object of the present invention is to provide a kind of emulsification coal-tar pitch, described emulsification coal-tar pitch preparation method comprises the following steps: in petroleum pitch emulsifying agent, add wilkinite, after mixing with water, obtain emulsion, utilize coal-tar pitch and emulsion to prepare emulsification coal-tar pitch.
Concrete preparation process and method are:
By the coal-tar pitch emulsifying agent of petroleum pitch emulsifying agent and wilkinite mixture Cheng Xin;
More than water is heated to 60 degree;
Water is become to emulsion with coal-tar pitch emulsifying agent mixture;
Coal-tar pitch is heated to 115 degree left and right, becomes liquid;
By liquid coal pitch and emulsion mixture, make emulsification coal-tar pitch.
Emulsification coal-tar pitch of the present invention, utilizes petroleum pitch emulsifying agent to add and joins bentonitic method, makes coal-tar pitch obtain emulsification, has solved the stable problem after coal-tar pitch emulsification and emulsification.
Accompanying drawing explanation
Fig. 1 is the emulsification coal-tar pitch preparation method's that provides of the embodiment of the present invention schema.
Embodiment
In order to make object of the present invention, technical scheme and advantage clearer, below in conjunction with drawings and Examples, the present invention is further elaborated.Should be appreciated that specific embodiment described herein, only in order to explain the present invention, is not intended to limit the present invention.
The present invention is achieved in that a kind of emulsification coal-tar pitch comprises the following steps: in petroleum pitch emulsifying agent, add wilkinite, after mixing, obtain emulsion with water, utilize coal-tar pitch and emulsion to prepare emulsification coal-tar pitch.
The present invention prepares the various raw-material ratios of emulsification coal-tar pitch:
(coal-tar pitch) 500:(water) 500:(petroleum pitch emulsifying agent) 3:(wilkinite) 1
Figure BDA0000471077760000031
Emulsification coal-tar pitch preparation process provided by the invention and method are:
1, by the coal-tar pitch emulsifying agent of petroleum pitch emulsifying agent and wilkinite mixture Cheng Xin;
2, more than water is heated to 60 degree;
3, water is become to emulsion (also claiming soap lye) with coal-tar pitch emulsifying agent mixture;
4, coal-tar pitch is heated to 115 degree left and right, becomes liquid;
5, by liquid coal pitch and emulsion mixture, make emulsification coal-tar pitch.
Emulsification coal-tar pitch preparation method provided by the invention, utilizes petroleum pitch emulsifying agent to add and joins bentonitic method, makes coal-tar pitch obtain emulsification, has solved the stable problem after coal-tar pitch emulsification and emulsification.
Table 1 is emulsified bitumen testing data.
Emulsified bitumen testing data
Figure 20141007057841000021
By reference to the accompanying drawings the specific embodiment of the present invention is described although above-mentioned; but not limiting the scope of the invention; one of ordinary skill in the art should be understood that; on the basis of technical scheme of the present invention, those skilled in the art do not need to pay various modifications that performing creative labour can make or distortion still within protection scope of the present invention.

Claims (3)

1. an emulsification coal-tar pitch, is characterized in that, the various raw-material ratios of described emulsification coal-tar pitch are:
Figure FDA0000471077750000011
2. emulsification coal-tar pitch as claimed in claim 1, it is characterized in that, described emulsification coal-tar pitch preparation method comprises the following steps: in petroleum pitch emulsifying agent, add wilkinite, after mixing, obtain emulsion with water, utilize coal-tar pitch and emulsion to prepare emulsification coal-tar pitch.
3. emulsification coal-tar pitch preparation method as claimed in claim 2, is characterized in that, concrete preparation process and method are:
By the coal-tar pitch emulsifying agent of petroleum pitch emulsifying agent and wilkinite mixture Cheng Xin;
More than water is heated to 60 degree;
Water is become to emulsion with coal-tar pitch emulsifying agent mixture;
Coal-tar pitch is heated to 115 degree left and right, becomes liquid;
By liquid coal pitch and emulsion mixture, make emulsification coal-tar pitch.
CN201410070578.4A 2014-02-28 2014-02-28 Emulsified coal tar pitch Pending CN103819916A (en)

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Application Number Priority Date Filing Date Title
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108178933A (en) * 2017-12-29 2018-06-19 重庆市盛百利防水建材有限公司 A kind of modified pitch and preparation method thereof

Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3567476A (en) * 1969-04-04 1971-03-02 United States Steel Corp Method of coloring bituminous materials and the resulting product
US20030192456A1 (en) * 2001-06-22 2003-10-16 Yap Michael L. Emulsion of bitumen in a colloidal clay and water slurry
CN1939977A (en) * 2006-09-20 2007-04-04 铁道科学研究院金属及化学研究所 Special emusified asphalt for railway or light underground plated non-fragment rail and its production
CN102031001A (en) * 2010-12-09 2011-04-27 辽宁省交通科学研究院 Road bentonite-based emulsified asphalt and preparation method thereof
CN102286205A (en) * 2011-06-28 2011-12-21 中国海洋石油总公司 Anionic emulsified asphalt and preparation method thereof
CN102558885A (en) * 2011-12-30 2012-07-11 上海龙孚材料技术有限公司 Emulsified asphalt used for high-speed railway, mortar containing emulsified asphalt and preparation method of mortar
CN102675890A (en) * 2012-05-23 2012-09-19 长安大学 Demulsifying slow breaking and quick setting modified emulsified asphalt by microwave heating and preparation method thereof
CN102898850A (en) * 2012-11-10 2013-01-30 广西金雨伞防水装饰有限公司 Modified emulsified asphalt waterproof sealant and preparation method thereof
CN103059589A (en) * 2012-12-28 2013-04-24 中国铁道科学研究院金属及化学研究所 Emulsified asphalt for ballastless slab track in severe cold region and preparation method thereof
CN103232710A (en) * 2013-05-02 2013-08-07 中国铁道科学研究院金属及化学研究所 Emulsified asphalt for CRTS I and CRTS II slab ballastless tracks and preparation method of emulsified asphalt

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3567476A (en) * 1969-04-04 1971-03-02 United States Steel Corp Method of coloring bituminous materials and the resulting product
US20030192456A1 (en) * 2001-06-22 2003-10-16 Yap Michael L. Emulsion of bitumen in a colloidal clay and water slurry
CN1939977A (en) * 2006-09-20 2007-04-04 铁道科学研究院金属及化学研究所 Special emusified asphalt for railway or light underground plated non-fragment rail and its production
CN102031001A (en) * 2010-12-09 2011-04-27 辽宁省交通科学研究院 Road bentonite-based emulsified asphalt and preparation method thereof
CN102286205A (en) * 2011-06-28 2011-12-21 中国海洋石油总公司 Anionic emulsified asphalt and preparation method thereof
CN102558885A (en) * 2011-12-30 2012-07-11 上海龙孚材料技术有限公司 Emulsified asphalt used for high-speed railway, mortar containing emulsified asphalt and preparation method of mortar
CN102675890A (en) * 2012-05-23 2012-09-19 长安大学 Demulsifying slow breaking and quick setting modified emulsified asphalt by microwave heating and preparation method thereof
CN102898850A (en) * 2012-11-10 2013-01-30 广西金雨伞防水装饰有限公司 Modified emulsified asphalt waterproof sealant and preparation method thereof
CN103059589A (en) * 2012-12-28 2013-04-24 中国铁道科学研究院金属及化学研究所 Emulsified asphalt for ballastless slab track in severe cold region and preparation method thereof
CN103232710A (en) * 2013-05-02 2013-08-07 中国铁道科学研究院金属及化学研究所 Emulsified asphalt for CRTS I and CRTS II slab ballastless tracks and preparation method of emulsified asphalt

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108178933A (en) * 2017-12-29 2018-06-19 重庆市盛百利防水建材有限公司 A kind of modified pitch and preparation method thereof
CN108178933B (en) * 2017-12-29 2020-06-02 重庆市盛百利防水建材有限公司 Modified asphalt and preparation method thereof

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Application publication date: 20140528