CN103798624B - Method for producing product with blood sugar level reducing function from buckwheat bran and barley - Google Patents

Method for producing product with blood sugar level reducing function from buckwheat bran and barley Download PDF

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Publication number
CN103798624B
CN103798624B CN201410086280.2A CN201410086280A CN103798624B CN 103798624 B CN103798624 B CN 103798624B CN 201410086280 A CN201410086280 A CN 201410086280A CN 103798624 B CN103798624 B CN 103798624B
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China
Prior art keywords
ethanol
fructus hordei
blood sugar
hordei vulgaris
product
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Expired - Fee Related
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CN201410086280.2A
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Chinese (zh)
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CN103798624A (en
Inventor
徐德平
候圆圆
吴盼盼
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Inner Mongolia Qiao Tai Biological Technology Co. Ltd.
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Jiangnan University
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L7/00Cereal-derived products; Malt products; Preparation or treatment thereof
    • A23L7/10Cereal-derived products
    • A23L7/104Fermentation of farinaceous cereal or cereal material; Addition of enzymes or microorganisms
    • A23L7/107Addition or treatment with enzymes not combined with fermentation with microorganisms
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L7/00Cereal-derived products; Malt products; Preparation or treatment thereof
    • A23L7/10Cereal-derived products
    • A23L7/115Cereal fibre products, e.g. bran, husk
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention discloses a method for producing a product with a blood sugar level reducing function from buckwheat bran and barley. The method particularly comprises the following steps: mixing the buckwheat bran and the barley; carrying out heat-insulation enzymatic conversion; and extracting, separating, blending, and spray-drying to prepare the buckwheat bran and barley compound product which can be used for reducing the blood sugar level and preventing complications.

Description

A kind of method that there is function of blood sugar reduction product using Semen Fagopyri Esculenti bran and Fructus Hordei Vulgaris production
Technical field
The invention belongs to medicine and field of food, more particularly, to a kind of have blood sugar lowering work(using Semen Fagopyri Esculenti bran and Fructus Hordei Vulgaris production The method of energy product.
Background technology
With the aggravation changing with social senilization of dietary structure, the sickness rate of China's diabetes is in that persistence rises Gesture.The up-to-date census data of Chinese Medical Association shows, China's diabeticss up to more than 9,000 ten thousand, leaps to the first in the world.Therefore, The medicine related to diabetes has good practical value with the exploitation of functional food.
Semen Fagopyri Esculenti is the miscellaneous grain crops that China generally plants, and records according to Compendium of Material Medica: " sweet cherry roots are mild-natured, cold, have physical strength profiting, delay Spiritual, sharp knowledge, sending down the abnormal ascending QI, wide intestinal, the effect of stomach invigorating ".Current clinical medicine is observed and is shown, Fagopyrum esculentum Moench powder and its product have fall blood Sugar, hyperlipidemia, strengthen the effect of body immunity.The chiro-inositol (dci) that buckwheat seed contains is hypoglycemic functional component, Again especially abundant containing dci with wheat bran in seed, but mainly existed with combined state under native state.
Fructus Hordei Vulgaris are a kind of integration of edible and medicinal herbs crops, and Chinese Traditional Medicine thinks that Fructus Hordei Vulgaris have food digesting action, and modern medicine study is sent out Now often eat the food containing Fructus Hordei Vulgaris and can reduce the probability suffering from glucagon syndrome and ii patients with type Ⅰ DM.
At present buckwheat bran is taken as feedstuff and plus the resource that utilizes, in addition to brewing beer, its functional characteristic is not yet for Fructus Hordei Vulgaris It is obtained by.The present invention is exactly using abundant enzyme in Fructus Hordei Vulgaris, and the dci being existed with combined state in wheat bran is changed into free state Dci strengthens hypoglycemic activity, simultaneously by have in Fructus Hordei Vulgaris help digestion, the constituents extraction of hypoglycemic activity out, produce with fall Hypoglycemia and the functional food of complication prevention.
Content of the invention
The present invention is directed to above-mentioned present situation, and Semen Fagopyri Esculenti bran is mixed with Fructus Hordei Vulgaris, after warm enzymatic conversion, by extracting, separates, adjusts Join, be spray-dried, prepare and there is the product reducing blood glucose and complication prevention effect.For reaching above-mentioned purpose, the present invention adopts Following technical scheme:
1st, proportioning raw materials: the Semen Fagopyri Esculenti bran of pulverizing, Fructus Hordei Vulgaris powder cross 60 mesh sieves, by Semen Fagopyri Esculenti bran 70%, the ratio of Fructus Hordei Vulgaris powder 30% Mixing.
2nd, bioconversion: mixed powder is added in extraction pot, by ethanol: mixed powder=8:1 adds 25-30% (v/w) Ethanol water.Control 25 DEG C of temperature, mixing speed 20-30 rev/min, keep more than 6 hours.Then 60 are increased the temperature to More than DEG C, keep 30 minutes, enzyme denaturing, obtain zymolyte.
3rd, ethanol extraction: zymolyte is filtered, obtains filtrate and slag, the amount that slag presses mixed powder again adds 10 times of volume (w/ The ethanol of 65-70% v), mixing speed 50-60 rev/min, 60 DEG C are extracted 2 hours, filter, and merge secondary filtrate, Concentrating under reduced pressure under the conditions of 60-70 DEG C, is concentrated into 1/10 volume, obtains alcohol extracting thing.
4th, water extraction: the amount that the slag after ethanol extraction is pressed mixed powder adds 10 times of volumes of deionized water, 60 DEG C of temperature Lower extraction 2 hours, filters to take filtrate.Filtrate concentrating under reduced pressure under the conditions of 60-70 DEG C, is concentrated into 1/10 volume, and taking-up is cooled to Room temperature, refilters, waste, takes filtrate to obtain water extract.
5th, precipitate with ethanol: water extract is added while stirring 95% ethanol, be more than 70% to concentration of alcohol, stand 12 hours More than, refilter, take filter cake, obtain water extracting alcohol hypostasis.
6th, allocate: alcohol extracting thing and the mixing of water extracting alcohol hypostasis add dextrin or Fructus Hordei Germinatus paste by the 5-10% of feed liquid quality Essence is incubated 60 DEG C after stirring.
7th, it is spray-dried: deployed material is sprayed under the conditions of inlet temperature 160-170 DEG C, 83-85 DEG C of leaving air temp Mist is dried, and obtains Semen Fagopyri Esculenti bran and Fructus Hordei Vulgaris compound collecting product.
8th, reduce blood glucose effect: streptozotocin is caused mice hyperglycemia drop by Semen Fagopyri Esculenti bran and Fructus Hordei Vulgaris compound collecting product Low effect, as shown in table 1.
Table 1. Semen Fagopyri Esculenti bran and Fructus Hordei Vulgaris compound collecting product cause the effect of mice hyperglycemia to streptozotocin
Compare with model control group: * p < 0.05;* p < 0.01.
Result shows: in middle and high dosage, product causes mice hyperglycemia to have obviously to drop to streptozotocin Low effect, and can obviously improve streptozotocin and cause mice polydipsia, polyphagia, polyuria symptom more than three.
Specific embodiment
The present invention is to be described in detail by the following examples, but is not intended that the invention is limited to this, specifically Embodiment is as follows:
It is added to after 7kg Fructus Hordei Germinatus powder and 3kg buckwheat wheat bran mix homogeneously in 200 liters of extraction pot, add 25% (v/v) 80 liters of the ethanol water of (ph is 4.5).Control 25 DEG C of temperature, 20 revs/min of mixing speed, keep 6 hours, filter, obtain filter Liquid and slag, slag is again in add-back extraction pot, then adds 100 liter 70% of ethanol in extraction pot, 50 revs/min of mixing speed, and 60 DEG C extract 2 hours, filter, filtering residue repeats extraction once, filter, merge the filtrate of three times and obtain 270 liters, subtract under the conditions of 70 DEG C Pressure concentrates, and is concentrated into 27 liters, obtains alcohol extracting thing.Filtering residue after ethanol extraction is added in Alcohol-settling tank, adds 100 liters of deionizations Water, extracts 2 hours at a temperature of 60 DEG C, filters to get filtrate 108 liters.Filtrate concentrating under reduced pressure under the conditions of 70 DEG C, is concentrated into 11 liters, takes Go out to be cooled to room temperature, refilter, waste, take filtrate to obtain 10 liters of water extract.Water extract is added while stirring 95% second Alcohol, is more than 70% to concentration of alcohol, stands more than 12 hours, refilters, take filter cake, obtain water extracting alcohol hypostasis 9kg.By alcohol extracting thing With the mixing of water extracting alcohol hypostasis, 2kg maltodextrin is added to be incubated 60 DEG C after stirring.By deployed material in inlet temperature 170 DEG C, it is spray-dried under the conditions of 85 DEG C of leaving air temp, obtains Semen Fagopyri Esculenti bran and Fructus Hordei Vulgaris compound collecting product 1.02kg.
Above preferred embodiment is merely to illustrate present disclosure, and in addition, the present invention also has other embodiment, In every case those skilled in the art enlighten because of technology involved in the present invention, and adopt equivalent or equivalent deformation mode formed Technical scheme all falls within protection scope of the present invention.

Claims (2)

1. a kind of production using Semen Fagopyri Esculenti bran and Fructus Hordei Vulgaris has the method for function of blood sugar reduction product it is characterised in that methods described has Body is:
(1) proportioning raw materials: the Semen Fagopyri Esculenti bran of pulverizing, Fructus Hordei Vulgaris powder cross 60 mesh sieves, by Semen Fagopyri Esculenti bran 70%, the ratio of Fructus Hordei Vulgaris powder 30% is mixed Close, obtain mixed powder;
(2) bioconversion: mixed powder is added in extraction pot, adds 8 liters of ethanol waters, wherein ethanol by every kg mixed powder In aqueous solution, volume fraction of ethanol is 25-30%;Control 25 DEG C of temperature, mixing speed 20-30 rev/min, keep 6 hours with On;Then increase the temperature to more than 60 DEG C, keep 30 minutes, enzyme denaturing, obtain zymolyte;
(3) ethanol extraction: zymolyte is filtered, obtains filtrate and slag, slag is pressed every kg mixed powder again and added 10 liters of ethanol waters, its In middle ethanol water, volume fraction of ethanol is 65-70%, mixing speed 50-60 rev/min, and 60 DEG C are extracted 2 hours, filter, Merge secondary filtrate, concentrating under reduced pressure under the conditions of 60-70 DEG C, be concentrated into 1/10 volume, obtain alcohol extracting thing;
(4) water extraction: the amount that the slag after ethanol extraction is pressed mixed powder adds 10 times of volumes of deionized water, extracts at a temperature of 60 DEG C 2 hours, filter to take filtrate;Filtrate concentrating under reduced pressure under the conditions of 60-70 DEG C, is concentrated into 1/10 volume, takes out and is cooled to room temperature, then Filter, waste, take filtrate to obtain water extract;
(5) precipitate with ethanol: water extract is added while stirring 95% ethanol, to concentration of alcohol be more than 70%, standing 12 hours with On, refilter, take filter cake, obtain water extracting alcohol hypostasis;
(6) allocate: alcohol extracting thing and the mixing of water extracting alcohol hypostasis add dextrin to protect after stirring by the 5-10% of feed liquid quality Temperature is to 60 DEG C;
(7) be spray-dried: by deployed material under the conditions of inlet temperature 160-170 DEG C, 83-85 DEG C of leaving air temp spray dried Dry, obtain Semen Fagopyri Esculenti bran and Fructus Hordei Vulgaris compound collecting product, that is, there is the product of function of blood sugar reduction.
2. the method that there is function of blood sugar reduction product using Semen Fagopyri Esculenti bran and Fructus Hordei Vulgaris production according to claim 1, its feature It is: this product has the effect that reduction streptozotocin causes mice hyperglycemia.
CN201410086280.2A 2014-03-11 2014-03-11 Method for producing product with blood sugar level reducing function from buckwheat bran and barley Expired - Fee Related CN103798624B (en)

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1730040A (en) * 2004-08-06 2006-02-08 香港赛马会中药研究院有限公司 The buckwheat compound and the manufacture method thereof that are used for the treatment of hyperglycemia
CN1973681A (en) * 2006-12-13 2007-06-06 山西金绿禾燕麦研究所 Technological process of producing oat diet fiber and nutritious powder with oat bran
CN101519457A (en) * 2009-03-17 2009-09-02 徐德平 Method for preparing beta-ethoxy rutinose and application thereof for reducing blood glucose
CN102948758A (en) * 2012-11-26 2013-03-06 陕西科技大学 Method for extracting buckwheat flavone from buckwheat bran
CN103315221A (en) * 2013-05-30 2013-09-25 宁国市亿邦生物科技有限公司 Instant powder having auxiliary blood sugar-reduction effect and preparation method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1730040A (en) * 2004-08-06 2006-02-08 香港赛马会中药研究院有限公司 The buckwheat compound and the manufacture method thereof that are used for the treatment of hyperglycemia
CN1973681A (en) * 2006-12-13 2007-06-06 山西金绿禾燕麦研究所 Technological process of producing oat diet fiber and nutritious powder with oat bran
CN101519457A (en) * 2009-03-17 2009-09-02 徐德平 Method for preparing beta-ethoxy rutinose and application thereof for reducing blood glucose
CN102948758A (en) * 2012-11-26 2013-03-06 陕西科技大学 Method for extracting buckwheat flavone from buckwheat bran
CN103315221A (en) * 2013-05-30 2013-09-25 宁国市亿邦生物科技有限公司 Instant powder having auxiliary blood sugar-reduction effect and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
大麦中活性多糖提取的研究;尹源明等;《中国粮油学报》;20020228;第17卷(第1期);第43页0.前言、1.2提取工艺流程、1.3试验方法 *

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Effective date of registration: 20170726

Address after: 028200 Nanshan Industrial Zone, Kulun Town, Kulun banner, the Inner Mongolia Autonomous Region, Tongliao

Patentee after: Inner Mongolia Qiao Tai Biological Technology Co. Ltd.

Address before: No. 1800 road 214122 Jiangsu Lihu Binhu District City of Wuxi Province

Patentee before: Jiangnan University

CF01 Termination of patent right due to non-payment of annual fee
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Granted publication date: 20170201

Termination date: 20190311