CN103771373B - A kind of electron-level phosphoric acid Hot-blast Heating crystallization apparatus - Google Patents
A kind of electron-level phosphoric acid Hot-blast Heating crystallization apparatus Download PDFInfo
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- CN103771373B CN103771373B CN201310744658.9A CN201310744658A CN103771373B CN 103771373 B CN103771373 B CN 103771373B CN 201310744658 A CN201310744658 A CN 201310744658A CN 103771373 B CN103771373 B CN 103771373B
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- Prior art keywords
- acid
- phosphoric acid
- crystallizer
- hot
- electron
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- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 title claims abstract description 138
- 229910000147 aluminium phosphate Inorganic materials 0.000 title claims abstract description 69
- 238000010438 heat treatment Methods 0.000 title claims abstract description 42
- 238000002425 crystallisation Methods 0.000 title claims abstract description 32
- 230000008025 crystallization Effects 0.000 title claims abstract description 31
- 239000002253 acid Substances 0.000 claims description 47
- 239000007788 liquid Substances 0.000 claims description 15
- 239000013078 crystal Substances 0.000 claims description 14
- 230000008676 import Effects 0.000 claims description 11
- 239000000463 material Substances 0.000 claims description 8
- 239000007921 spray Substances 0.000 claims description 8
- 239000011521 glass Substances 0.000 claims description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 238000013022 venting Methods 0.000 claims description 6
- 229910001220 stainless steel Inorganic materials 0.000 claims description 5
- 239000010935 stainless steel Substances 0.000 claims description 5
- 238000005406 washing Methods 0.000 claims description 3
- 230000008901 benefit Effects 0.000 abstract description 7
- 238000005265 energy consumption Methods 0.000 abstract description 3
- 230000007812 deficiency Effects 0.000 abstract description 2
- 238000009776 industrial production Methods 0.000 abstract 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 15
- 238000000034 method Methods 0.000 description 13
- 239000011574 phosphorus Substances 0.000 description 12
- 229910052698 phosphorus Inorganic materials 0.000 description 12
- 238000002844 melting Methods 0.000 description 8
- 238000004519 manufacturing process Methods 0.000 description 7
- OBSZRRSYVTXPNB-UHFFFAOYSA-N tetraphosphorus Chemical group P12P3P1P32 OBSZRRSYVTXPNB-UHFFFAOYSA-N 0.000 description 7
- 239000007791 liquid phase Substances 0.000 description 6
- 230000008018 melting Effects 0.000 description 6
- 239000000126 substance Substances 0.000 description 6
- 238000002485 combustion reaction Methods 0.000 description 5
- 239000012535 impurity Substances 0.000 description 5
- 239000002994 raw material Substances 0.000 description 5
- 238000005507 spraying Methods 0.000 description 5
- 238000009841 combustion method Methods 0.000 description 4
- GNTDGMZSJNCJKK-UHFFFAOYSA-N divanadium pentaoxide Chemical compound O=[V](=O)O[V](=O)=O GNTDGMZSJNCJKK-UHFFFAOYSA-N 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- 101100298222 Caenorhabditis elegans pot-1 gene Proteins 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- 230000007423 decrease Effects 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- BHEPBYXIRTUNPN-UHFFFAOYSA-N hydridophosphorus(.) (triplet) Chemical compound [PH] BHEPBYXIRTUNPN-UHFFFAOYSA-N 0.000 description 3
- 239000012452 mother liquor Substances 0.000 description 3
- 238000000746 purification Methods 0.000 description 3
- XYFCBTPGUUZFHI-UHFFFAOYSA-N Phosphine Chemical compound P XYFCBTPGUUZFHI-UHFFFAOYSA-N 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 230000004927 fusion Effects 0.000 description 2
- 239000012071 phase Substances 0.000 description 2
- 239000002367 phosphate rock Substances 0.000 description 2
- 230000003068 static effect Effects 0.000 description 2
- 230000035900 sweating Effects 0.000 description 2
- ISIJQEHRDSCQIU-UHFFFAOYSA-N tert-butyl 2,7-diazaspiro[4.5]decane-7-carboxylate Chemical compound C1N(C(=O)OC(C)(C)C)CCCC11CNCC1 ISIJQEHRDSCQIU-UHFFFAOYSA-N 0.000 description 2
- 241000208125 Nicotiana Species 0.000 description 1
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- -1 during melting Substances 0.000 description 1
- 239000003337 fertilizer Substances 0.000 description 1
- 235000007983 food acid Nutrition 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000012476 oxidizable substance Substances 0.000 description 1
- 229910000073 phosphorus hydride Inorganic materials 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
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Abstract
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Claims (5)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201310744658.9A CN103771373B (en) | 2013-12-30 | 2013-12-30 | A kind of electron-level phosphoric acid Hot-blast Heating crystallization apparatus |
Applications Claiming Priority (1)
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CN201310744658.9A CN103771373B (en) | 2013-12-30 | 2013-12-30 | A kind of electron-level phosphoric acid Hot-blast Heating crystallization apparatus |
Publications (2)
Publication Number | Publication Date |
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CN103771373A CN103771373A (en) | 2014-05-07 |
CN103771373B true CN103771373B (en) | 2015-10-28 |
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CN201310744658.9A Active CN103771373B (en) | 2013-12-30 | 2013-12-30 | A kind of electron-level phosphoric acid Hot-blast Heating crystallization apparatus |
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CN (1) | CN103771373B (en) |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102580345A (en) * | 2012-01-13 | 2012-07-18 | 四川大学 | Crystallization tower for purifying phosphoric acid |
CN102795609A (en) * | 2011-05-23 | 2012-11-28 | 杨志勇 | Apparatus for producing high purity electronic grade phosphoric acid |
CN203781850U (en) * | 2013-12-30 | 2014-08-20 | 广西明利化工有限公司 | Electronic grade phosphoric acid hot blast heating crystallization device |
-
2013
- 2013-12-30 CN CN201310744658.9A patent/CN103771373B/en active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102795609A (en) * | 2011-05-23 | 2012-11-28 | 杨志勇 | Apparatus for producing high purity electronic grade phosphoric acid |
CN102580345A (en) * | 2012-01-13 | 2012-07-18 | 四川大学 | Crystallization tower for purifying phosphoric acid |
CN203781850U (en) * | 2013-12-30 | 2014-08-20 | 广西明利化工有限公司 | Electronic grade phosphoric acid hot blast heating crystallization device |
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CN103771373A (en) | 2014-05-07 |
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