CN103756788B - The acquisition system of aromatic plant volatile matter - Google Patents
The acquisition system of aromatic plant volatile matter Download PDFInfo
- Publication number
- CN103756788B CN103756788B CN201410030939.2A CN201410030939A CN103756788B CN 103756788 B CN103756788 B CN 103756788B CN 201410030939 A CN201410030939 A CN 201410030939A CN 103756788 B CN103756788 B CN 103756788B
- Authority
- CN
- China
- Prior art keywords
- vasculum
- volatile matter
- acquisition system
- water
- activated carbon
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Landscapes
- Water Treatment By Sorption (AREA)
- Separation Of Gases By Adsorption (AREA)
Abstract
The invention discloses a kind of acquisition system of aromatic plant volatile matter, comprise vasculum, breeding apparatus and adsorbent equipment, described vasculum has air inlet, gas outlet, water inlet and delivery port, described breeding apparatus is positioned at described vasculum, described breeding apparatus comprises drip irrigation appliance, described drip irrigation appliance has water-supply-pipe, described water-supply-pipe one end is communicated in described water inlet, the other end is toward in described vasculum, described adsorbent equipment comprises vavuum pump and activated carbon adsorption layer, described vavuum pump, activated carbon adsorption layer and described gas outlet are communicated with successively by pipeline.The acquisition system of the aromatic plant volatile matter that the present invention relates to, can carry out original position, continuous print collection to volatile matter, not produce any impact, sustainable use natural resources on the normal growth of plant, has continuously, efficiently, original position, natural, the feature of low-carbon (LC); And the using method of the phytovolatilization matter collection device that the present invention relates to is simple, easy and simple to handle, use manpower and material resources sparingly.
Description
Technical field
The present invention relates to the assembling sphere of plant volatile, particularly relate to a kind of acquisition system of aromatic plant volatile matter.
Background technology
Plants essential oil is a kind of volatile secondary metabolites with aromatic odor produced in plant, and being combined by the simple compounds of molecular weight, can, with steam distillation, be the general name of the volatility oily liquid substance with certain smell.
At present, the extraction of plants essential oil is all picked by active component without exception, then carries out the extraction of distinct methods.The active component of plant is picked and carries out extraction of essential oil, the self-sow of plant is had a certain impact.Such as, plucking flower would not fructufy, plucks leaf, stem and root, and the normal growth that will affect plant even makes plant dead.Active component under plucking, except essential oil, also contains other very many compositions, as polysaccharide, and polyphenol, albumen, lipid etc.This makes leaching process can more complicated, and the purity of essential oil and yield all can be lower, and does not also have a kind of original position, continuous print and do not affect the plants essential oil acquisition system of the normal growth of plant at present.
Summary of the invention
Based on this, be necessary to provide a kind of original position, continuous print collection, active component of not plucking a plant, not to the acquisition system of the aromatic plant volatile matter that the normal growth of plant has an impact.
An acquisition system for aromatic plant volatile matter, comprises vasculum, breeding apparatus and adsorbent equipment, and described vasculum has air inlet, gas outlet, water inlet and delivery port, and described breeding apparatus is positioned at described vasculum;
Described breeding apparatus comprises drip irrigation appliance, and described drip irrigation appliance has water-supply-pipe, and described water-supply-pipe one end is communicated in described water inlet, and the other end is toward in described vasculum;
Described adsorbent equipment comprises vavuum pump and activated carbon adsorption layer, and described vavuum pump, activated carbon adsorption layer and described gas outlet are communicated with successively by pipeline.
Wherein in an embodiment, also comprise light supply apparatus, described light supply apparatus is connected to the top of described vasculum.
Wherein in an embodiment, described light supply apparatus adopts LED light source.
Wherein in an embodiment, one end that described water-supply-pipe is opened in described vasculum is connected with water-dropper.
Wherein in an embodiment, described water-supply-pipe is arranged at the bottom of described vasculum.
Wherein in an embodiment, between described vavuum pump and described activated carbon adsorption layer, be also communicated with surge flask.
Wherein in an embodiment, between described activated carbon adsorption layer and described gas outlet, between described activated carbon adsorption layer and described vavuum pump, be equipped with packed layer.
Wherein in an embodiment, the air inlet of described vasculum is provided with the air filtration layer matched.
Wherein in an embodiment, described vasculum is provided with case lid, and described case lid is provided with handle.
The acquisition system of the aromatic plant volatile matter that the present invention relates to; original position, continuous print collection can be carried out to volatile matter; any impact is not produced on the normal growth of plant, sustainable use natural resources, have continuously; efficiently; original position, natural, the feature of low-carbon (LC); to protection of the environment, maximum resource utilization, use value maximize and the sustainable development of resource utilizes significant.
The acquisition system of the aromatic plant volatile matter that the present invention relates to, also comprises light supply apparatus, and described light supply apparatus is connected to the top of described vasculum, and the sunlight providing plant strain growth to need by light supply apparatus is convenient to the long term growth of plant.
The acquisition system of the aromatic plant volatile matter that the present invention relates to, described light supply apparatus adopts LED light source, the features such as LED has adjustable light intensity and spectrum, cooling load is low, electro-optical efficiency is high, volume is little, the life-span is long, use direct current and can set specific wavelength, wavelength is fixed, and environmental-protecting performance is good.
The acquisition system of the aromatic plant volatile matter that the present invention relates to, one end that described water-supply-pipe is opened in described vasculum is connected with water-dropper, and the filtered water in water-supply-pipe slowly and equably instills soil near plant root by water-dropper.
The acquisition system of the aromatic plant volatile matter that the present invention relates to, described water-supply-pipe is arranged at the bottom of described vasculum, and make the water droplet in water-dropper go out the rear root directly flowing through plant, avoid the waste of water, the utilization rate of water resource is high.
The acquisition system of the aromatic plant volatile matter that the present invention relates to, is also connected with surge flask between described vavuum pump and described activated carbon adsorption layer, when preventing vavuum pump pressure excessive, active carbon particle is directly sucked vavuum pump, reduces the service life of vavuum pump.
The acquisition system of the aromatic plant volatile matter that the present invention relates to, is equipped with packed layer between described activated carbon adsorption layer and described gas outlet, between described activated carbon adsorption layer and described vavuum pump, to prevent the dissipation of active carbon particle.
The acquisition system of the aromatic plant volatile matter that the present invention relates to, the air inlet of described vasculum is provided with the air filtration layer matched, and avoids the impurity in air to enter in described vasculum.
The acquisition system of the aromatic plant volatile matter that the present invention relates to, described vasculum is provided with case lid, and described case lid is provided with handle, is convenient to putting into and taking out, handled easily of plant.
Accompanying drawing explanation
Fig. 1 is the embodiment of the present invention 1 schematic diagram;
Fig. 2 is the embodiment of the present invention 1 vasculum front view;
Fig. 3 is the embodiment of the present invention 1 drip irrigation appliance front view;
Fig. 4 is the GC/MS chromatogram that the embodiment of the present invention 2 situ extracts Jasmine essential oil.
Accompanying drawing explanation
10, vasculum; 12, air inlet; 13, water inlet; 14, gas outlet; 15, delivery port; 16, case lid; 18, handle; 20, LED light source; 30, activated carbon adsorption layer; 32, vavuum pump; 34, surge flask; 36, packed layer; 40, water-supply-pipe; 42, water-dropper; 50, air filtration layer.
Detailed description of the invention
Below with reference to embodiment and accompanying drawing, the present invention is described further.
Embodiment 1
A kind of acquisition system of aromatic plant volatile matter, see Fig. 1 ~ Fig. 3, comprise vasculum 10, light supply apparatus, breeding apparatus, drip irrigation appliance and adsorption system, described vasculum 10 is lucite casing, described vasculum 10 has the case lid 16 at top, described case lid 16 have two handles 18, described vasculum 10 has air inlet 12, gas outlet 14, water inlet 13 and delivery port 14, described delivery port is arranged at the bottom of described vasculum 10, and be provided with the lid matched, close when the water yield in vasculum 10 is moderate, when hypervolia in vasculum 10, open and discharge water, the air inlet 12 of described vasculum 10 is provided with the air filtration layer 50 matched, air filtration cotton is filled with in described air filtration layer 50, described adsorption system comprises activated carbon adsorption layer 30, vavuum pump 32, surge flask 34, described vavuum pump 32, activated carbon adsorption layer 30 and gas outlet 14 are communicated with successively, described surge flask 34 is connected between described vavuum pump 32 and described activated carbon adsorption layer 30, between described activated carbon adsorption layer 30 and described gas outlet 14, is equipped with packed layer 36 between described activated carbon adsorption layer 30 and described vavuum pump 32, described light supply apparatus adopts LED light source 20, it is inner that described breeding apparatus is arranged at described vasculum 10, described breeding apparatus comprises drip irrigation appliance, described drip irrigation appliance is communicated with water-supply-pipe 40, described water-supply-pipe 40 one end is communicated in described water inlet 13, the other end is toward in described vasculum 10, and this end is connected with water-dropper 42, described water-supply-pipe 40 is connected with the bottom being placed in described vasculum 10, extends in described vasculum 10.
The present invention in use, the plant of wounded in the battle volatile matter to be collected is placed in the breeding apparatus in vasculum 10, opens LED light source 20 and drip irrigation appliance, after plant to be planted produces the volatile matter of aromatic odor, open adsorption system, make the volatile matter of plant be adsorbed in described activated carbon adsorption layer 30.
Embodiment 2
Present embodiments provide a kind of acquisition method of Jasminum sambac Air volatile matter, and use the acquisition system described in embodiment 1, comprise the steps:
(1) absorption of volatile matter: wounded in the battle Jasminum sambac Air plant is incubated in vasculum, after the plant of Jasminum sambac Air produces the volatile matter of aromatic odor, start vavuum pump to bleed, make the volatile matter of Jasminum sambac Air be adsorbed in the active carbon of activated carbon adsorption layer;
(2) refluxing extraction: get the activated carbon that step (1) obtains, put into the conical flask of 250mL specification, adding ether to not having described activated carbon, loading onto spherical condensation tube, 40 DEG C of water-baths, when after ether boiling, adds hot reflux 3h, cools and leaves standstill and soak 2h;
(3) filter: obtain supernatant after step (2) is left standstill the liquid filtering obtained, separately get washed with diethylether filter residue twice, and each cleaning solution is incorporated in described supernatant;
(4) rotary distillation: by step (3) to supernatant pour in the pyriform cucurbit of Rotary Evaporators, the distillation of 40 DEG C of heating water baths, reclaims ether, when Liquid Residue be faint yellow oily in flask, stops distilling, obtains Jasminum sambac Air essential oil.
Dropper dry for the Jasminum sambac Air essential oil obtained in the pyriform cucurbit of step (4) is sucked in brown vial, seals lid with sealed membrane, tinning foil paper lucifuge, be placed on 4 DEG C, refrigerator, save backup.
Obtain Jasminum sambac Air essential oil by the acquisition method of the Jasminum sambac Air volatile matter described in the present embodiment, detected by gas chromatograph-mass spectrometer.
The model of gas chromatograph-mass spectrometer that arrives when using be AgilenttechnologiesN6890c-5973ineit, gas phase analysis condition: chromatographic column is HP-5MS (30m*0.25mm*0.25mm) capillary column; Sample size 0.5 μ L; Injector temperature: 230 DEG C; Column temperature program: initial temperature 50 DEG C, is warming up to 150 DEG C with 4 DEG C/min, keeps 2min, is warming up to 250 DEG C with 8 DEG C/min, keeps 3min, is warming up to 260 DEG C with 5 DEG C/min.Carrier gas: helium, flow velocity: 0.76mL/min; Mass Spectrometry Conditions: EI source, ionization voltage 70eV; Detector temperature: 250 DEG C.The chromatogram image of gained is shown in Figure 4, and wherein, the horizontal seat in Fig. 4 is retention time, and ordinate is absorption peak strength; The retention time of linalool is 10.55 minutes; The retention time of phenylmethyl acetate is 12.6 minutes, the retention time of cis-3-hexenol benzoic ether is 25.7 minutes, from chromatogram, in the retention time of 40min, absworption peak evenly occurs, and the peak-to-peak retention time of each absorption is shorter, and each absworption peak is more symmetrical, without conditions of streaking, the extraction of essential oil effect of the present embodiment is better.
Contrast test:
1) in refluxing extraction process, adopt low boiling, hypotoxic n-hexane (boiling point is 68.74 DEG C), other steps are all identical with embodiment 2, carry out refluxing extraction, but extraction efficiency comparatively embodiment 2 is lower.
2) in refluxing extraction process, adopt low boiling, hypotoxic benzinum because of (boiling point is at 40-80 DEG C), other steps are all identical with embodiment 2, carry out refluxing extraction, but the aromatic odour of the essential oil extracted is not dense, and fragrance is lighter, and is doped with the smell of some alcohol, ether in aromatic odor, have impact on the fragrance extracting essential oil, also namely have impact on the purity of the essential oil of extraction further.
The deficiency of the method existence of tradition water extraction essential oil: (1) Extracting temperature is high, makes some ingredient breakdown in essential oil, except the composition in original plant, also may comprise the volatile decomposition products produced in some still-process.(2) essential oil fragrance is pure not, and fragrance is mingled with water sulks, and essential oil product is difficult to upper high-grade.Compared with the method for traditional water extraction essential oil, the derived essential oil obtained in the present embodiment 2 is pure, and essential oil purity is high.
The acquisition system of the aromatic plant volatile matter that the present invention relates to, original position, continuous print collection can be carried out to volatile matter, sustainable use natural resources, have continuously, efficiently, original position, natural, the feature of low-carbon (LC), and any impact is not produced on the normal growth of plant, to protection of the environment, maximum resource utilization, use value maximize and the sustainable development of resource utilizes significant; And the use providing a kind of acquisition system of aromatic plant volatile matter of the present invention is simple, easy and simple to handle, uses manpower and material resources sparingly.
The above embodiment only have expressed several embodiment of the present invention, and it describes comparatively concrete and detailed, but therefore can not be interpreted as the restriction to the scope of the claims of the present invention.It should be pointed out that for the person of ordinary skill of the art, without departing from the inventive concept of the premise, can also make some distortion and improvement, these all belong to protection scope of the present invention.Therefore, the protection domain of patent of the present invention should be as the criterion with claims.
Claims (7)
1. an acquisition system for aromatic plant volatile matter, is characterized in that, comprises vasculum, breeding apparatus and adsorbent equipment, and described vasculum has air inlet, gas outlet, water inlet and delivery port, and described breeding apparatus is positioned at described vasculum;
Described breeding apparatus comprises drip irrigation appliance, and described drip irrigation appliance has water-supply-pipe, and described water-supply-pipe one end is communicated in described water inlet, and the other end is toward in described vasculum;
Described adsorbent equipment comprises vavuum pump and activated carbon adsorption layer, described vavuum pump, activated carbon adsorption layer and described gas outlet are communicated with successively by pipeline, between described vavuum pump and described activated carbon adsorption layer, be also communicated with surge flask, between described activated carbon adsorption layer and described gas outlet, between described activated carbon adsorption layer and described vavuum pump, be equipped with packed layer.
2. the acquisition system of aromatic plant volatile matter according to claim 1, is characterized in that, also comprises light supply apparatus, and described light supply apparatus is connected to the top of described vasculum.
3. the acquisition system of aromatic plant volatile matter according to claim 2, is characterized in that, described light supply apparatus adopts LED light source.
4. the acquisition system of the aromatic plant volatile matter according to any one of claims 1 to 3, is characterized in that, one end that described water-supply-pipe is opened in described vasculum is connected with water-dropper.
5. the acquisition system of the aromatic plant volatile matter according to any one of claims 1 to 3, is characterized in that, described water-supply-pipe is arranged at the bottom of described vasculum.
6. the acquisition system of the aromatic plant volatile matter according to any one of claims 1 to 3, is characterized in that, the air inlet of described vasculum is provided with the air filtration layer matched.
7. the acquisition system of the aromatic plant volatile matter according to any one of claims 1 to 3, is characterized in that, described vasculum is provided with case lid, and described case lid is provided with handle.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410030939.2A CN103756788B (en) | 2014-01-07 | 2014-01-22 | The acquisition system of aromatic plant volatile matter |
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2014100075243 | 2014-01-07 | ||
| CN201410007524 | 2014-01-07 | ||
| CN201410007524.3 | 2014-01-07 | ||
| CN201410030939.2A CN103756788B (en) | 2014-01-07 | 2014-01-22 | The acquisition system of aromatic plant volatile matter |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103756788A CN103756788A (en) | 2014-04-30 |
| CN103756788B true CN103756788B (en) | 2016-03-30 |
Family
ID=50524118
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410030939.2A Expired - Fee Related CN103756788B (en) | 2014-01-07 | 2014-01-22 | The acquisition system of aromatic plant volatile matter |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103756788B (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106525512A (en) * | 2016-09-21 | 2017-03-22 | 环境保护部南京环境科学研究所 | VOC collection box in the wild |
| CN107132151A (en) * | 2017-06-22 | 2017-09-05 | 北京建筑大学 | A kind of device for determining vacuum distillation fracturing outlet liquid steam COD value |
| CN107899366A (en) * | 2017-11-24 | 2018-04-13 | 尹大建 | A kind of Jasmine fragrance extracting device |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101234279A (en) * | 2007-11-01 | 2008-08-06 | 浙江大学 | Open type living body plant volatile dynamic high-efficiency collecting device |
| CN102778368A (en) * | 2012-08-09 | 2012-11-14 | 山东省产品质量监督检验研究院 | Sampling method and collector for organic volatile matters in product/sample |
| CN103266015A (en) * | 2013-04-27 | 2013-08-28 | 中南林业科技大学 | Natural aromatic essential oil acquisition apparatus and application method |
| CN203183881U (en) * | 2013-01-14 | 2013-09-11 | 华中农业大学 | Plant volatile collecting device |
| CN103484251A (en) * | 2013-09-05 | 2014-01-01 | 上海交通大学 | Effective collection and storage methods for aromas of aromatic plant living bodies and application of same |
-
2014
- 2014-01-22 CN CN201410030939.2A patent/CN103756788B/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101234279A (en) * | 2007-11-01 | 2008-08-06 | 浙江大学 | Open type living body plant volatile dynamic high-efficiency collecting device |
| CN102778368A (en) * | 2012-08-09 | 2012-11-14 | 山东省产品质量监督检验研究院 | Sampling method and collector for organic volatile matters in product/sample |
| CN203183881U (en) * | 2013-01-14 | 2013-09-11 | 华中农业大学 | Plant volatile collecting device |
| CN103266015A (en) * | 2013-04-27 | 2013-08-28 | 中南林业科技大学 | Natural aromatic essential oil acquisition apparatus and application method |
| CN103484251A (en) * | 2013-09-05 | 2014-01-01 | 上海交通大学 | Effective collection and storage methods for aromas of aromatic plant living bodies and application of same |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103756788A (en) | 2014-04-30 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN203869918U (en) | Plant volatile substance in-situ collection device | |
| CN103756788B (en) | The acquisition system of aromatic plant volatile matter | |
| CN103266015A (en) | Natural aromatic essential oil acquisition apparatus and application method | |
| CN204939435U (en) | A kind of family expenses essential oil distillation extraction device | |
| CN104713965A (en) | Method for extracting tobacco volatile and semi-volatile aroma components | |
| CN101928642B (en) | Method for extracting and separating spice and medicinal components from whole plants of Dendranthema indicum | |
| CN105296163A (en) | Extraction equipment for fragrant plant essential oil and headspace volatile | |
| CN103923748B (en) | A kind of volatile oil extracts collects separation equipment | |
| CN103194312A (en) | Method for extracting essential oil from cypress leaves | |
| CN203360416U (en) | Aromatic plant essential oil extraction device | |
| CN103525556A (en) | Ecological flower planting method before extracting jasmine flower aroma substances | |
| CN105950293A (en) | Extraction method of jasmine essential oil | |
| Shao et al. | Analysis of volatile components extracted from the peels of four different Chinese pomelos using TDS‐GC‐MS | |
| CN203741300U (en) | Collection system of aromatic plant volatiles | |
| CN103756789B (en) | The acquisition method of aromatic plant volatile matter | |
| CN104017651A (en) | Preparation method and preparation device of peony flower and rose flower mixed essential oil | |
| CN204550508U (en) | A kind of volatile oil extractor of ultrasonic assistant | |
| CN204502440U (en) | One Plants sesame oil boiler | |
| CN104531358A (en) | Jasmine flower scented oil collection extraction device and process thereof | |
| EP2163287A4 (en) | Method and device for preparing solution along with equipment for preparing scented tea | |
| CN202148299U (en) | Volatile oil extraction oil-water separator with condensation | |
| CN106390511A (en) | Low-temperature vacuum distillation extraction equipment for preparation of high-purity essential oil | |
| CN205412299U (en) | Multi -functional steam distillation and soxhlet extraction integration experimental apparatus | |
| CN101824366B (en) | Method for extracting absolute oil of lavender by using fixed bed extraction method | |
| CN202543170U (en) | Novel fragrance recovery equipment |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160330 Termination date: 20180122 |