CN103752076A - Filtering equipment containing impurities and silver paste and filtering method thereof - Google Patents

Filtering equipment containing impurities and silver paste and filtering method thereof Download PDF

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Publication number
CN103752076A
CN103752076A CN201410042950.0A CN201410042950A CN103752076A CN 103752076 A CN103752076 A CN 103752076A CN 201410042950 A CN201410042950 A CN 201410042950A CN 103752076 A CN103752076 A CN 103752076A
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slurry
container
opening
silver
slurry container
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CN201410042950.0A
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CN103752076B (en
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刘德臣
华永云
李建国
姚雁林
傅建奇
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Beijing Flight Boda Electronics Ltd.
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Beijing Sevenstar Electronics Co Ltd
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Abstract

The invention provides filtering equipment containing impurities and silver paste and a filtering method thereof. The filtering equipment comprises a centrifugal drying device with symmetric inner grooves, an auxiliary device and a plurality of fixed parts, wherein the auxiliary device comprises an impurity-silver paste container, an empty paste container and a connecting device. The impurity-silver paste container is positioned on one sides, near to the center of the centrifugal drying device, of the inner grooves; the empty paste container is positioned on one sides, near to the edge of the centrifugal drying device, of the inner grooves; the connecting device is used for connecting the impurity-silver paste container with the empty paste container; a filtering screen is positioned in the connecting device, and is positioned between the impurity-silver paste container and the empty paste container; the fixed parts are matched with the inner walls of the inner grooves in size for fixing the auxiliary device in the inner grooves; in the centrifugating process, impurities and silver paste are separated from each other; the silver paste is thrown in the empty paste container through the filtering screen, so that the impurities and the silver paste are effectively recovered, the recovery rate is increased, and the cost is reduced.

Description

A kind of filter plant and filter method thereof of impure silver slurry
Technical field
The present invention relates to technical field of semiconductors, particularly a kind of filter plant and filter method thereof of impure silver slurry.
Background technology
Silver slurry is by the thick slurry being mixed into of highly purified argent particulate, adhesive, solvent, cosolvent, it is for the printing of crystal silicon solar batteries positive electrode, match with backplate, electric field, play the electric energy that crystal silicon solar batteries is produced and send extraneous effect to.Positive electrode is formed by printing, oven dry and sintering by silver slurry.In the printing process of positive electrode, owing to sneaking into impurity in silver slurry, will cause occurring serigraphy substandard products, as thin grid line thickness inequality, spillage etc., even can cause the problems such as half tone explosion.These printing substandard products are done after finished product cell piece, mild degree become off standard, serious meeting becomes waste product, thereby has influence on final product percent of pass and conversion efficiency.After half tone explosion, not only cause the loss of half tone, and can cause the serious waste of silver slurry, and then increase production cost.Therefore, after impure silver slurry is recycled, re-use, can effectively improve product percent of pass, and reduce the waste of silver slurry, reduce production costs.
At present, the recycling of impure silver slurry is mainly contained to two schemes: the one, use silver slurry to filter special equipment and recycle, the 2nd, the artificial glue rifle that adds screen cloth that uses recycles.Scheme one is used silver slurry to filter special equipment and is processed, by vibratory sieve and centrifuge, carry out sorting, make silver slurry separated with impurity, advantage is that output is large, efficiency is high, shortcoming is the recycling that equipment investment expense is high, be not suitable for small lot, due in general actual research and production, conventionally needs the silver-colored batch of starching of impurity of recovery less, therefore, the slurry of the silver in scheme one filtration special equipment is not suitable for scientific research and small lot recycling.Scheme two is packed into impure silver slurry in glue rifle, glue rifle muzzle folder one deck screen cloth, mode by manual compression makes silver slurry separated with impurity, advantage is that equipment investment expense is low, simple to operate, be applicable to the recycling of small lot, shortcoming is that efficiency is low, the rate of recovery is low, therefore, be unfavorable for the recycling of silver slurry, be not also suitable for scientific research and small lot recycling.
Therefore, be badly in need of the recovery method that a kind of efficiency applicable small lot impurity silver high and that cost is low is starched, thereby reduce cost and enhance productivity.
Summary of the invention
In order to overcome the problems referred to above, the present invention aims to provide a kind of silver of the impurity to small lot slurry and carries out effectively reclaiming the method for filtering, thereby improves the rate of recovery and reduce costs.
The filter plant of a kind of impure silver slurry of the present invention, comprises the centrifugal drying equipment with symmetrical inside groove, and wherein, the equipment of the impure silver slurry of described filtration also comprises:
Auxiliary equipment, described auxiliary equipment comprises:
Impurity silver slurry slurry container, for splendid attire impurity silver slurry slurry, is positioned at described inside groove near a side of described centrifugal drying equipment center, and it has opening;
Empty slurry container, the silver slurry after filtering for splendid attire, is positioned at described inside groove near a side of described centrifugal drying device end, and it has opening;
Jockey, it has screen pack and attaching parts, and wherein, described attaching parts are connected the described impurity silver slurry opening of slurry container and the opening of described empty slurry container; Described screen pack is arranged in described attaching parts, and between the described impurity silver slurry opening of slurry container and the opening of described empty slurry container;
Some fixed parts, match with the inwall size of described inside groove, and described auxiliary equipment is fixed in described inside groove.
Preferably, described auxiliary equipment comprises:
A described impurity silver slurry slurry container, it has some openings;
Some described empty slurry container, described in each, empty slurry container has an opening, and the opening of described some empty slurry container is corresponding one by one with the opening of described impurity silver slurry slurry container, by described jockey, is connected;
Some described jockeys, described in each, jockey has screen pack and attaching parts, and described attaching parts are connected the described impurity silver slurry opening of slurry container and the opening of described empty slurry container; Described screen pack is arranged in described attaching parts, and between the described impurity silver slurry opening of slurry container and the opening of described empty slurry container.
Preferably, described attaching parts and described screen pack are separate.
Preferably, described attaching parts are comprised of hollow inner cap and adapter sleeve, described hollow inner cap is enclosed in described screen pack on the opening of described impurity silver slurry slurry container, and described adapter sleeve is connected the described impurity silver slurry opening of slurry container and the opening of described empty slurry container.
Preferably, described adapter sleeve is two hollow enclosing covers of bonding back-to-back.
Preferably, the opening of the described impurity silver slurry slurry container distribution that is centrosymmetric.
Preferably, described auxiliary equipment comprises:
Some described impurity silver slurry slurry container, described in each, impurity silver slurry slurry container has an opening;
Some described empty slurry container, described in each, empty slurry container has an opening, and the opening of described some empty slurry container is corresponding one by one with the opening of described some impurity silver slurry slurry container, by described jockey, is connected;
Some described jockeys, have screen pack and attaching parts, and described attaching parts are connected the described impurity silver slurry opening of slurry container and the opening of described empty slurry container; Described screen pack is arranged in described attaching parts, and between the described impurity silver slurry opening of slurry container and the opening of described empty slurry container.
Preferably, described attaching parts and described screen pack are separate.
Preferably, described attaching parts are comprised of hollow inner cap and adapter sleeve, described hollow inner cap is enclosed in described screen pack on the opening of described impurity silver slurry slurry container, and described adapter sleeve is connected the described impurity silver slurry opening of slurry container and the opening of described empty slurry container.
Preferably, described fixed part has an open end and a non-open end, described non-open end is provided with and adds strong hardness parts, described impurity silver slurry slurry container is arranged at described fixed part open end, described empty slurry container is arranged at the hermetic terminal of described fixed part, and described fixed part is fastened on described auxiliary equipment in described inside groove.
Preferably, described attaching parts and described impurity silver are starched the opening of slurry container and are threaded with the opening of described empty slurry container.
The present invention also provides a kind of filter plant of above-mentioned impure silver slurry that adopts to carry out the filter method that impure silver is starched, and it comprises auxiliary equipment assembling process and the pulp centrifuged process of impurity silver slurry, wherein,
Auxiliary equipment assembling process comprises the following steps:
Step S01: impurity silver slurry slurry is packed in some described impurity silver slurry slurry container, utilize some described jockeys respectively some described impurity silver slurry slurry container to be closely connected with some described empty slurry container;
Step S02: the some described impure silver slurry slurry container and the described empty slurry container that are connected are packed in some described fixed parts;
Step S03: some described fixed parts are fixed in described inside groove, wherein, described impure silver slurry slurry container is positioned at described inside groove near a side at the center of described centrifugal drying equipment, and described empty slurry container is positioned at described inside groove near a side at the edge of described centrifugal drying equipment;
The pulp centrifuged process of impurity silver slurry comprises: in described centrifugal drying equipment, carry out centrifugal process, described impure silver slurry slurry gets rid of in described empty slurry container after described screen pack filters.
Preferably, described jockey comprises attaching parts and screen pack, described attaching parts are comprised of hollow inner cap and adapter sleeve, by described hollow inner cap, described screen pack is enclosed on the opening of described impurity silver slurry slurry container, then, described adapter sleeve is connected with the described impurity silver slurry opening of slurry container, the opening of described empty slurry container respectively.
Preferably, described fixed part has an open end and a non-open end, and described non-open end is provided with and adds strong hardness parts; First, the some described impure silver slurry slurry container and the described empty slurry container that are connected are packed in some described fixed parts, make described impurity silver slurry slurry container be positioned at described fixed part open end, described empty slurry container is positioned at the non-open end of described fixed part; Again described fixed part is fastened in described inside groove.
Preferably, in step S03, the distribution that is centrosymmetric of some described fixed parts.
Preferably, the screen cloth order number of described screen pack is 200-400 order, and the time of described centrifugal process is 30-40min, and rotating speed is 200-600r/min, and centrifugal effective radius is 20-25cm, and temperature is room temperature.
Filter plant and the filter method thereof of impurity silver slurry slurry of the present invention, on the centrifugal drying equipment of routine, auxiliary equipment and fixed part are set, by jockey, impurity silver slurry slurry container and empty slurry container are coupled together, recycle fixed part by its sizing and be fixed in the inside groove of centrifugal drying equipment, utilize centrifugal principle that silver slurry is separated with impurity, silver slurry after filtering is got rid of in sky slurry container, simply and effectively impurity silver slurry slurry has been carried out to filtered and recycled, organic efficiency is high, and has effectively saved cost.
Accompanying drawing explanation
Fig. 1 is the structural representation of the impure silver-colored filter plant of starching of embodiments of the invention one
Fig. 2 is the structural representation of the centrifugal drying equipment of embodiments of the invention one
Fig. 3 is the structural representation of the auxiliary equipment of embodiments of the invention one
Fig. 4 is the structural representation of the fixed part of embodiments of the invention one
Fig. 5 is that the fractionation of all parts of the jockey of embodiments of the invention one is related to schematic diagram
Fig. 6 is the structural representation of the impure silver-colored filter plant of starching of embodiments of the invention two
Fig. 7 is the structural representation of the auxiliary equipment of embodiments of the invention two
Fig. 8 is the structural representation of the fixed part of embodiments of the invention two
Fig. 9 is that the fractionation of all parts of the jockey of embodiments of the invention two is related to schematic diagram
Figure 10 is the schematic flow sheet of the impure silver-colored filter method of starching of embodiments of the invention three
The specific embodiment
For making content of the present invention more clear understandable, below in conjunction with Figure of description, content of the present invention is described further.Certainly the present invention is not limited to this specific embodiment, and the known general replacement of those skilled in the art is also encompassed in protection scope of the present invention.
Below with reference to specific embodiments and the drawings 1-10, filter plant and the filter method thereof of impure silver slurry of the present invention are described in further detail.Wherein, Fig. 1 is the structural representation of the impure silver-colored filter plant of starching of embodiments of the invention one, Fig. 2 is the structural representation of the centrifugal drying equipment of embodiments of the invention one, Fig. 3 is the structural representation of the auxiliary equipment of embodiments of the invention one, Fig. 4 is the structural representation of the fixed part of embodiments of the invention one, Fig. 5 is that the fractionation of all parts of the jockey of embodiments of the invention one is related to schematic diagram, Fig. 6 is the structural representation of the impure silver-colored filter plant of starching of embodiments of the invention two, Fig. 7 is the structural representation of the auxiliary equipment of embodiments of the invention two, Fig. 8 is the structural representation of the fixed part of embodiments of the invention two, Fig. 9 is that the fractionation of all parts of the jockey of embodiments of the invention two is related to schematic diagram, Figure 10 is the schematic flow sheet of the impure silver-colored filter method of starching of embodiments of the invention three.It should be noted that, accompanying drawing all adopts very the form simplified, uses non-ratio accurately, and only in order to object convenient, that reach lucidly the aid illustration embodiment of the present invention.
In the present invention, the filter plant of impure silver slurry comprises centrifugal drying equipment, auxiliary equipment and some fixed parts with some symmetrical inside grooves, centrifugal drying equipment of the present invention can be the centrifugal drier of routine, and it can have some symmetrical expression inside grooves; Fixed part matches with inside groove, for auxiliary equipment is fixed on to inside groove, auxiliary equipment is packed in fixed part, then fixed part is fastened in inside groove; The size of fixed part is for just fixing slurry container, and should match with the inwall size of inside groove, can pack in inside groove and firmly be stuck in inside groove.
Auxiliary equipment of the present invention comprises:
Impurity silver slurry slurry container, for splendid attire impurity silver slurry slurry; When filtering, this impurity silver slurry slurry container is positioned over to inside groove near a side of centrifugal drying equipment center; Its shape should match with the size of fixed part, can pack in fixed part, can be, but not limited to as hollow ball-shape, cylindric, rectangular-shaped etc., and the present invention does not impose any restrictions this.
Empty slurry container, the silver slurry after filtering for splendid attire; When filtering, it is positioned at inside groove near a side of centrifugal drying device end; Its shape also should match with the size of fixed part, can pack in fixed part, can be, but not limited to as cylindric, rectangular-shaped etc.
Jockey, it has screen pack and attaching parts; Screen pack is arranged in attaching parts, and between the impurity silver slurry opening of slurry container and the opening of empty slurry container; In the present invention, attaching parts and screen pack can be separate, also can be integrated, and the two ends of attaching parts are connected with the impurity silver slurry opening of slurry container, the opening of empty slurry container respectively, in this way, just impurity silver slurry slurry container and empty slurry container can be coupled together; The mode of its connection can be, but not limited to adopt and is threaded, and also can adopt gummed bonding etc., and certainly, being threaded is modal tight connected mode.If adopted, be threaded, opening part has screw thread, if opening part is internal thread, attaching parts end is external screw thread, if opening part is external screw thread, attaching parts end is internal thread, and the present invention is not restricted this.
It should be noted that, the number of impurity silver slurry slurry container can be one, also can be for a plurality of, in embodiment mono-, the number of impurity silver slurry slurry container is one, in impurity silver slurry slurry container, there are some openings, make these openings can be corresponding one by one with the opening in some empty slurry container in the present invention, simultaneously, when filtering, this impurity silver slurry slurry container is arranged at the center of centrifugal drying equipment, empty slurry container is positioned in inside groove, by jockey, the opening of the opening of empty slurry container and impurity silver slurry slurry container is coupled together.In embodiment bis-, the number of impurity silver slurry slurry container is several, on it, there is an opening, by jockey, the opening in this opening and empty slurry container is coupled together, then one one correspondence is positioned in inside groove, impurity silver slurry slurry container is arranged at inside groove near a side at the center of centrifugal drying equipment, and empty slurry container is arranged at inside groove near a side at the edge of centrifugal drying equipment.
The principle that the filter plant of impure silver slurry of the present invention and filter method thereof adopt is: according to centrifugal principle, be F=m ω 2r, ω=2 π n wherein, F is centrifugal force, ω is angular speed, r is the distance of matter center to center, and n is rotating speed, utilizes the centrifugal action of centrifugal drier that silver slurry is separated with impurity.
Embodiment mono-
Centrifugal drying equipment in the present invention can have some symmetrical expression inside grooves, adopts in the present embodiment the centrifugal drier with symmetrical expression six grooves, but this is not used in and limits the scope of the invention.
Refer to accompanying drawing 1, the structure of the filter plant of the impure silver slurry of the present embodiment comprises:
Centrifugal drying equipment 100, auxiliary equipment 102 and the fixed part 103 with six symmetrical expression inside grooves.
Refer to accompanying drawing 2, the centrifugal drying equipment 100 of structure of the centrifugal drying equipment of the present embodiment has six symmetrical inside grooves 101, and these six inside grooves 101 are equal angles distribution along the pivot of centrifugal drying equipment 100, and the distribution that is centrosymmetric; Certainly, the centrifugal drying equipment 100 adopting can be the centrifugal drier of routine, and can also have other parts, such as sucker etc., here repeats no more.
Auxiliary equipment 102 in the present embodiment, refers to accompanying drawing 3, comprising:
An impurity silver slurry slurry container 1 ', it has several openings, it should be noted that, in the present invention, the number of these openings can be any positive integer, but, in order to make it stressed more even in centrifugal process, thereby raising centrifugal efficiency, in the present embodiment, the arranging of opening of impurity silver slurry slurry container 1 ' should be along the pivot of centrifugal drier 100 equal angles distribution, or can centered by be symmetrical arranged, because above-mentioned symmetrical expression inside groove 101 is six and the distribution that is centrosymmetric, the number of these openings can and be centrosymmetric distribution identical with the number of symmetrical expression inside groove 101, therefore, the opening of impurity silver slurry slurry container 1 ' should be six and the distribution that is centrosymmetric in contrast, certainly, in other embodiments, also can be the two or four that is centrosymmetric and distributes, impurity silver slurry slurry container 1 ' can be, but not limited to as impurity silver slurry slurry bottle.
Some empty slurry container 2 ', each empty slurry container 2 ' has an opening; In the present embodiment, the number of empty slurry container 2 ' should be corresponding with the opening of impurity silver slurry slurry container 1 ', the opening of starching slurry container 1 ' due to impurity silver is six, therefore, the opening of empty slurry container 2 ' is six, and corresponding one by one with six openings of impurity silver slurry slurry container 1 ' respectively, by jockey 3 ', be connected; In the present embodiment, empty slurry container 2 ' can be, but not limited to as empty slurry bottle.
Some jockeys 3 ', each jockey 3 ' all has screen pack 4 ' and attaching parts 5 ', and attaching parts 5 ' are connected the impurity silver slurry opening of slurry container 1 ' and the opening of empty slurry container 2 '; In the present invention, the number of jockey 3 ' should be identical with the number of impurity silver slurry slurry container 1 ', empty slurry container 2 ', in the present embodiment, the number of starching slurry container 1 ' due to impurity silver is six, therefore, the number of jockey 3 ' is six, but this is not used in and limits the scope of the invention.
Fixed part 103 in the present embodiment, refer to accompanying drawing 4, there is an open end and a non-open end, impurity silver slurry slurry container 1 ' is arranged at fixed part 103 open ends, empty slurry container 2 ' is arranged at the hermetic terminal of fixed part 103, and fixed part 103 is fastened on auxiliary equipment 102 in inside groove 101; In addition, at this non-open end, be provided with the parts that add strong hardness, this is in order to improve the shock-resistant ability of non-open end, to be avoided in centrifugal process, compared with large centrifugal force, impacts non-open end and causes non-open end to damage.
In the present embodiment, these fixed parts 103 should be consistent with the distribution of impurity silver slurry slurry container 1 ', and distribution is centrosymmetric; The number of fixed part 103 should be identical with the number of above-mentioned impurity silver slurry slurry container 1 ', empty slurry container 2 ', jockey 3 ', be six, these six fixed parts 103 are positioned over above-mentioned six impurity silver slurry slurry container 1 ' and the empty slurry container 2 ' symmetries that are connected in six inside grooves 101.In the present embodiment, fixed part 103 can be, but not limited to as being foam box, one end perforate of foam box, not perforate of one end, can enter perforate one end by impurity silver slurry slurry is bottled, enters not perforate one end by empty slurry is bottled, wherein, in not perforate one end of foam box, can fix parts that add strong hardness, as hardboard etc., prevent from destroying in centrifugal process foam box.
In the present embodiment, screen pack 4 ' and attaching parts 5 ' are separate, refer to accompanying drawing 5, the fractionation of all parts of jockey 3 ' is closed: attaching parts 5 ' are comprised of hollow inner cap 6 ' and adapter sleeve 7 ', before use, need to assemble jockey 3 ', the process of assembling comprises first utilizes hollow inner cap 6 ' screen pack 4 ' to be sealed on the opening 8 ' of impurity silver slurry slurry container 1 ', then, use adapter sleeve 7 ' that the impurity silver slurry opening 8 ' of slurry container 1 ' and the opening of empty slurry container 2 ' 9 ' are connected.In the present embodiment, preferably, adapter sleeve 5 ' is two hollow enclosing covers of bonding back-to-back, hollow enclosing cover and impurity silver are starched the opening 8 ' of slurry container 1 ' and are threaded with the opening 9 ' of empty slurry container 2 ', such as, hollow covers outward has external screw thread, on the opening being attached thereto, has internal thread.
In the present embodiment, after having assembled, screen pack 4 ' is arranged in attaching parts 5 ', is specifically arranged in adapter sleeve 7 ', and is positioned between the impurity silver slurry opening 8 ' of slurry container 1 ' and the opening 9 ' of empty slurry container 2 '; The screen cloth order number of screen pack 4 ' can be 200-400 order, and preferably, screen cloth order number is 280 orders.
Embodiment bis-
Centrifugal drying equipment in the present invention can have some symmetrical expression inside grooves, adopts in the present embodiment the centrifugal drier with symmetrical expression six grooves, but this is not used in and limits the scope of the invention.
Refer to accompanying drawing 6, the structure of the filter plant of the impure silver slurry of the present embodiment comprises:
The centrifugal drying equipment 200 with six symmetrical expression inside grooves, it has six symmetrical inside grooves 201; Auxiliary equipment 202; And fixed part 203.
Centrifugal drying equipment 200 in the present embodiment centrifugal drying equipment 100 a kind of with above-described embodiment is identical, repeats no more here.
Auxiliary equipment 202 in the present embodiment, refers to accompanying drawing 7, comprising:
Some impurity silver slurry slurry container 1, have an opening on each container 1, it should be noted that, in the present invention, these impurity silver slurry slurry container 1 can be any positive integer, but, in order to make it stressed more even in centrifugal process, thereby raising centrifugal efficiency, in the present embodiment, arranging of impurity silver slurry slurry container 1 should be along the pivot of centrifugal drier 200 equal angles distribution, and can centered by be symmetrical arranged, in the present embodiment, because above-mentioned symmetrical expression inside groove 201 is six, the number of these impurity silver slurry slurry container 1 can and be centrosymmetric distribution identical with the number of symmetrical expression inside groove 201, therefore, the number of impurity silver slurry slurry container 1 should be six and the distribution that is centrosymmetric in contrast, certainly, in other embodiments, impurity silver slurry slurry container can be also the two or four that is centrosymmetric and distributes, impurity silver slurry slurry container 1 can be, but not limited to as impurity silver slurry slurry bottle.
Some empty slurry container 2, each empty slurry container 2 has an opening; In the present embodiment, the number of empty slurry container 2 should be all corresponding with number and the distribution of impurity silver slurry slurry container 1, the number of starching slurry container 1 due to impurity silver is six, therefore, the opening of empty slurry container 2 is also six, and corresponding one by one with the opening of six impurity silver slurry slurry container 1 respectively, the distribution that is centrosymmetric, is connected by jockey 3; In the present embodiment, empty slurry container 2 can be, but not limited to as empty slurry bottle.
Some jockeys 3, each jockey 3 all has screen pack 4 and attaching parts 5, and attaching parts 5 are connected the opening of impurity silver slurry slurry container 1 with the opening of empty slurry container 2; In the present invention, the number of jockey 3 should be identical with the number of impurity silver slurry slurry container 1, empty slurry container 2, in the present embodiment, the number of starching slurry container 1, empty slurry container 2 due to impurity silver is six, therefore, the number of jockey 3 is six, but this is not used in and limits the scope of the invention.
Fixed part 203 in the present embodiment, refer to 8, have and have an open end and a non-open end, impurity silver slurry slurry container 1 is arranged at fixed part 203 open ends, empty slurry container 2 is arranged at the hermetic terminal of fixed part 203, and fixed part 203 is fastened on auxiliary equipment 202 in inside groove 201; In addition, at this non-open end, be provided with the parts that add strong hardness, this is in order to improve the shock-resistant ability of non-open end, to be avoided in centrifugal process, compared with large centrifugal force, impacts non-open end and causes non-open end to damage.
In the present embodiment, these fixed parts 203 should be consistent with the distribution of impurity silver slurry slurry container 1, and distribution is centrosymmetric; The number of fixed part 203 should be identical with the number of above-mentioned impurity silver slurry slurry container 1, empty slurry container 2, jockey 3, be six, these six fixed parts are positioned over above-mentioned six impurity silver slurry slurry container 1 and empty slurry container 2 symmetries that are connected in six inside grooves.In the present embodiment, fixed part 203 can be, but not limited to as foam box, one end perforate of foam box, not perforate of one end, can enter perforate one end by impurity silver slurry slurry is bottled, enters not perforate one end by empty slurry is bottled, wherein, in not perforate one end of foam box, can fix parts that add strong hardness, such as hardboard etc., prevent from destroying in centrifugal process foam box.
In the present embodiment, refer to accompanying drawing 9, the fractionation relation of all parts of jockey 3 can be with above-described embodiment one identical, be: attaching parts 5 and screen pack 4 are separate, attaching parts 5 are comprised of hollow inner cap 6 and adapter sleeve 7, before filtering, need assemble jockey, assembling process comprises: first, utilize hollow inner cap 6 that screen pack 4 is sealed on the opening 8 of impurity silver slurry slurry container 1, adapter sleeve 7 is connected the impurity silver slurry opening 8 of slurry container 1 and the opening 9 of empty slurry container 2.In the present embodiment, preferably, adapter sleeve 7 is two hollow enclosing covers of bonding back-to-back, hollow enclosing cover and impurity silver are starched the opening of slurry container and are threaded with the opening of empty slurry container, such as, hollow covers outward has external screw thread, on the opening being attached thereto, has internal thread.
In the present embodiment, after jockey has been assembled, screen pack 4 is arranged in attaching parts 3, is specifically arranged in adapter sleeve 7, and between the impurity silver slurry opening 8 of slurry container 1 and the opening 9 of empty slurry container 2; The screen cloth order number of screen pack 4 can be 200-400 order, and preferably, screen cloth order number is 280 orders.
Embodiment tri-
Refer to Fig. 3, the filter method of the impure silver slurry of the present embodiment of the present invention, refers to accompanying drawing 10, comprises the following steps, and wherein, step S01-03 is auxiliary equipment assembling process, and step S04 is the pulp centrifuged process of impurity silver slurry:
Step S01: impure silver slurry slurry is packed in impurity silver slurry slurry container, utilize jockey that impure silver slurry slurry container is closely connected with empty slurry container;
Concrete, in the present embodiment, jockey comprises attaching parts and screen pack, attaching parts are comprised of hollow inner cap and adapter sleeve, by hollow inner cap, screen pack is enclosed on the opening of impurity silver slurry slurry container, then, adapter sleeve is connected with the impurity silver slurry opening of slurry container, the opening of empty slurry container respectively.
For example, adapter sleeve can be two hollow enclosing covers that bond back-to-back, first utilize hollow inner cap screen pack to be enclosed in to the opening of impurity silver slurry slurry container, then hollow enclosing cover is starched to the opening of slurry container and is connected with the opening of empty slurry container with impurity silver, connected mode can be screw thread, such as, hollow covers outward has external screw thread, on the opening being attached thereto, there is internal thread, if hollow enclosing cover has internal thread, on the opening being attached thereto, there is external screw thread.
In the present embodiment, the screen cloth order number of screen pack can be 200-400 order, preferably, can select 280 orders.
Step S02: the impure silver slurry slurry container and the empty slurry container that are connected are packed in fixed part;
Concrete, in the present embodiment, fixed part has an open end and a non-open end, and non-open end is provided with and adds strong hardness parts; Impurity silver slurry slurry container is positioned at fixed part open end, and empty slurry container is positioned at the non-open end of fixed part; Again fixed part is fastened in inside groove.The material of fixed part can be foamed material, for example, fixed part can be foam box, one end perforate of foam box, not perforate of one end, can make impurity silver slurry slurry bottle be positioned at perforate one end, empty slurry bottle is positioned at not perforate one end, wherein, in not perforate one end of foam box, can fix a hardboard, such as hardwood plate etc., prevent from destroying in centrifugal process foam box.
Step S03: above-mentioned fixed part is individually fixed in the inside groove of centrifugal drying equipment, wherein, impure silver slurry slurry container is positioned at inside groove near a side at the center of centrifugal drying equipment, and empty slurry container is positioned at inside groove near a side at the edge of described centrifugal drying equipment;
Concrete, in the present embodiment, the center by one end of the opening of fixed part towards centrifugal drying equipment, one end of opening is not towards the edge of centrifugal drying equipment; Fixed part should not produce and rock in centrifugal process, and fixed part can be fastened in inside groove; Thereby in order to make auxiliary equipment stressed centrifugal mass that evenly improves in centrifugal process, fixed part should be along the pivot of centrifugal drier equal angles and distribute, or the distribution that is centrosymmetric.
Step S04: carry out centrifugal process in centrifugal drying equipment, impure silver slurry slurry gets rid of in sky slurry container after net filtration after filtration.
Concrete, in the present embodiment, centrifugal process can adopt room temperature, and centrifugation time can be 30-40min, and rotating speed can be 200-600r/min, and centrifugal effective radius can be 20-25cm.According to such condition, calculate, if the impure silver slurry slurry packing in impurity silver slurry slurry container is 2-2.5Kg, in centrifugal drying equipment, there are 6 inside grooves, in 30-40min, can process the impure silver slurry of 12-15Kg simultaneously, the about 25-30Kg of filtration silver slurry per hour, organic efficiency is higher, can reach more than 99%, thereby improve silver slurry utilization rate.
Owing to can adopting conventional centrifugal drying equipment to carry out the filtered and recycled of impurity silver slurry slurry in the present embodiment, therefore can be on the basis of existing equipment and material enterprising line operate, reduced fund input, and simple to operate, the rate of recovery is high.
In sum, filter plant and the filter method thereof of impurity silver slurry slurry of the present invention, on the centrifugal drying equipment of routine, auxiliary equipment and fixed part are set, by jockey, impurity silver slurry slurry container and empty slurry container are coupled together, recycle fixed part by its sizing and be fixed in the inside groove of centrifugal drying equipment, utilize centrifugal principle that silver slurry is separated with impurity, silver slurry after filtering is got rid of in sky slurry container, simply and effectively impurity silver slurry slurry has been carried out to filtered and recycled, organic efficiency is high, and has effectively saved cost.
Although the present invention discloses as above with preferred embodiment; right described embodiment only gives an example for convenience of explanation; not in order to limit the present invention; those skilled in the art can do some changes and retouching without departing from the spirit and scope of the present invention, and the protection domain that the present invention advocates should be as the criterion with described in claims.

Claims (16)

1. a filter plant for impure silver slurry, comprises the centrifugal drying equipment with symmetrical inside groove, it is characterized in that, the equipment of the impure silver slurry of described filtration also comprises:
* auxiliary equipment, described auxiliary equipment comprises:
Impurity silver slurry slurry container, for splendid attire impurity silver slurry slurry, is positioned at described inside groove near a side of described centrifugal drying equipment center, and it has opening;
Empty slurry container, the silver slurry after filtering for splendid attire, is positioned at described inside groove near a side of described centrifugal drying device end, and it has opening;
Jockey, it has screen pack and attaching parts, and wherein, described attaching parts are connected the described impurity silver slurry opening of slurry container and the opening of described empty slurry container; Described screen pack is arranged in described attaching parts, and between the described impurity silver slurry opening of slurry container and the opening of described empty slurry container;
* some fixed parts, match with the inwall size of described inside groove, and described auxiliary equipment is fixed in described inside groove.
2. the filter plant of impure silver slurry according to claim 1, is characterized in that, described auxiliary equipment comprises:
A described impurity silver slurry slurry container, it has some openings;
Some described empty slurry container, described in each, empty slurry container has an opening, and the opening of described some empty slurry container is corresponding one by one with the opening of described impurity silver slurry slurry container, by described jockey, is connected;
Some described jockeys, described in each, jockey has screen pack and attaching parts, and described attaching parts are connected the described impurity silver slurry opening of slurry container and the opening of described empty slurry container; Described screen pack is arranged in described attaching parts, and between the described impurity silver slurry opening of slurry container and the opening of described empty slurry container.
3. the filter plant of impure silver slurry according to claim 2, is characterized in that, described attaching parts and described screen pack are separate.
4. the filter plant that impure silver according to claim 3 is starched, it is characterized in that, described attaching parts are comprised of hollow inner cap and adapter sleeve, described hollow inner cap is enclosed in described screen pack on the opening of described impurity silver slurry slurry container, and described adapter sleeve is connected the described impurity silver slurry opening of slurry container and the opening of described empty slurry container.
5. the filter plant of impure silver slurry according to claim 4, is characterized in that, described adapter sleeve is two hollow enclosing covers of bonding back-to-back.
6. the filter plant of impure silver slurry according to claim 2, is characterized in that, the distribution that is centrosymmetric of the opening of described impurity silver slurry slurry container.
7. the filter plant of impure silver slurry according to claim 1, is characterized in that, described auxiliary equipment comprises:
Some described impurity silver slurry slurry container, described in each, impurity silver slurry slurry container has an opening;
Some described empty slurry container, described in each, empty slurry container has an opening, and the opening of described some empty slurry container is corresponding one by one with the opening of described some impurity silver slurry slurry container, by described jockey, is connected;
Some described jockeys, have screen pack and attaching parts, and described attaching parts are connected the described impurity silver slurry opening of slurry container and the opening of described empty slurry container; Described screen pack is arranged in described attaching parts, and between the described impurity silver slurry opening of slurry container and the opening of described empty slurry container.
8. the filter plant of impure silver slurry according to claim 7, is characterized in that, described attaching parts and described screen pack are separate.
9. the filter plant that impure silver according to claim 8 is starched, it is characterized in that, described attaching parts are comprised of hollow inner cap and adapter sleeve, described hollow inner cap is enclosed in described screen pack on the opening of described impurity silver slurry slurry container, and described adapter sleeve is connected the described impurity silver slurry opening of slurry container and the opening of described empty slurry container.
10. the filter plant that impure silver according to claim 1 is starched, it is characterized in that, described fixed part has an open end and a non-open end, described non-open end is provided with the parts that add strong hardness, described impurity silver slurry slurry container is arranged at described fixed part open end, described empty slurry container is arranged at the hermetic terminal of described fixed part, and described fixed part is fastened on described auxiliary equipment in described inside groove.
The filter plant of 11. impure silver slurries according to claim 1, is characterized in that, described attaching parts and described impurity silver are starched the opening of slurry container and is threaded with the opening of described empty slurry container.
12. 1 kinds adopt the filter plant of the impure silver slurry described in the claims 1-11 any one to carry out the filter method that impure silver is starched, and it is characterized in that, comprise auxiliary equipment assembling process and the pulp centrifuged process of impurity silver slurry, wherein,
Described auxiliary equipment assembling process comprises the following steps:
Step S01: impurity silver slurry slurry is packed in some described impurity silver slurry slurry container, utilize some described jockeys respectively some described impurity silver slurry slurry container to be closely connected with some described empty slurry container;
Step S02: the some described impure silver slurry slurry container and the described empty slurry container that are connected are packed in some described fixed parts;
Step S03: some described fixed parts are fixed in described inside groove, wherein, described impure silver slurry slurry container is positioned at described inside groove near a side at the center of described centrifugal drying equipment, and described empty slurry container is positioned at described inside groove near a side at the edge of described centrifugal drying equipment;
The pulp centrifuged process of described impurity silver slurry comprises: in described centrifugal drying equipment, carry out centrifugal process, described impure silver slurry slurry gets rid of in described empty slurry container after described screen pack filters.
The filter method of 13. impure silver slurries according to claim 12, it is characterized in that, described jockey comprises attaching parts and screen pack, described attaching parts are comprised of hollow inner cap and adapter sleeve, by described hollow inner cap, described screen pack is enclosed on the opening of described impurity silver slurry slurry container, then, described adapter sleeve is connected with the described impurity silver slurry opening of slurry container, the opening of described empty slurry container respectively.
The filter method of 14. impure silver slurries according to claim 12, is characterized in that, described fixed part has an open end and a non-open end, and described non-open end is provided with and adds strong hardness parts; First, the some described impure silver slurry slurry container and the described empty slurry container that are connected are packed in some described fixed parts, make described impurity silver slurry slurry container be positioned at described fixed part open end, described empty slurry container is positioned at the non-open end of described fixed part; Again described fixed part is fastened in described inside groove.
The filter methods of 15. impure silver slurries according to claim 12, is characterized in that, in step S03, and the distribution that is centrosymmetric of some described fixed parts.
The filter method of 16. impure silver slurries according to claim 12, is characterized in that, the screen cloth order number of described screen pack is 200-400 order, the time of described centrifugal process is 30-40min, rotating speed is 200-600r/min, and centrifugal effective radius is 20-25cm, and temperature is room temperature.
CN201410042950.0A 2014-01-29 2014-01-29 A kind of filter plant of impure silver slurry and filter method thereof Expired - Fee Related CN103752076B (en)

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS61212308A (en) * 1985-03-15 1986-09-20 Toshiba Corp Filter device
US20060207927A1 (en) * 2005-03-18 2006-09-21 Tirakian Edward L Garnet filtration system for use with water jet cutting tools
CN202446892U (en) * 2012-02-20 2012-09-26 深圳顺络电子股份有限公司 Silver paste recycling device
CN202933535U (en) * 2012-12-05 2013-05-15 无锡市儒兴科技开发有限公司 Automatic slurry filter device
CN202983334U (en) * 2012-11-12 2013-06-12 上海超日(洛阳)太阳能有限公司 Slurry filter net

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS61212308A (en) * 1985-03-15 1986-09-20 Toshiba Corp Filter device
US20060207927A1 (en) * 2005-03-18 2006-09-21 Tirakian Edward L Garnet filtration system for use with water jet cutting tools
CN202446892U (en) * 2012-02-20 2012-09-26 深圳顺络电子股份有限公司 Silver paste recycling device
CN202983334U (en) * 2012-11-12 2013-06-12 上海超日(洛阳)太阳能有限公司 Slurry filter net
CN202933535U (en) * 2012-12-05 2013-05-15 无锡市儒兴科技开发有限公司 Automatic slurry filter device

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